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- Author:
- Zheng-Yu Lin; Kun-Ching Cheng; Huey-Jen Su; Chi-I Chang; Jue-Liang Hsu; Min-fen Hsu; Mei-Chin Lu; Yun-Sheng Lin
- Source:
- Chemistry of natural compounds 2022 v.58 no.4 pp. 659-668
- ISSN:
- 0009-3130
- Subject:
- X-ray diffraction; acylation; corals; cytotoxicity; diterpenoids; humans; mass spectrometry; metabolites; neoplasm cells; spectral analysis
- Abstract:
- ... The xenicane-type diterpene 13-epi-9-deacetylxenicin (1) was isolated from polar extract of the soft coral Asterospicularia laurae. The structure of 13-epi-9-deacetylxenicin was determined by X-ray diffraction analysis, and the absoulte configuration was determined using the modified Mosher′s method. Eleven acylation products of 13-epi-9-deacetylxenicin were prepared: 13-epi-9-O-p-anisoylxenicin ( ...
- DOI:
- 10.1007/s10600-022-03765-z
- https://doi.org/10.1007/s10600-022-03765-z
- Author:
- Niranjan Das; Prashanta Kumar Deb; Eunus S. Ali; Manash C. Das; Biswatrish Sarkar; Siddhartha Kumar Mishra
- Source:
- Chemistry of natural compounds 2022 v.58 no.1 pp. 21-26
- ISSN:
- 0009-3130
- Subject:
- aerial parts; breast neoplasms; chemistry; cytotoxicity; glucosides; humans; naphthalene; neoplasm cells; spectral analysis
- Abstract:
- ... A new bioactive naphthalene glucoside, named neanoside C (1), was isolated from the aerial part of Neanotis wightiana. The structure of neanoside C (1) was elucidated as 1,4-dihydroxy-2-(6′-Omethylglucopyranosyloxymethyl)-naphthalene-3-vinyloxyglucopyranoside by interpretation of the spectroscopic data, including 2D NMR and chemical studies. Neanoside C (1) was further subjected to screening for a ...
- DOI:
- 10.1007/s10600-022-03591-3
- https://doi.org/10.1007/s10600-022-03591-3
- Author:
- Daniel Osei Dankyira; Bin Wang; Jin Cai; Wei-nv Zeng; Guo-Lei Huang; Cai-Juan Zheng
- Source:
- Chemistry of natural compounds 2022 v.58 no.5 pp. 842-844
- ISSN:
- 0009-3130
- Subject:
- Candida albicans; Dothiorella; chemistry; fermentation; fungi; spectral analysis
- Abstract:
- ... A new cytosporone derivative, dothiorelone P (1), and one known analog, dothiorelone E (2), were isolated from fermentation culture of the mangrove-derived fungus Dothiorella sp. ML002. Their structures were identified by comprehensive analyses of 1D and 2D NMR and HR-ESI-MS spectroscopic data. Compound 2 exhibited inhibitory activity against Candida albicans with the MIC value of 6.25 μg/mL. ...
- DOI:
- 10.1007/s10600-022-03812-9
- https://doi.org/10.1007/s10600-022-03812-9
- Author:
- Vu Thi Quyen; Le Thi Hong Minh; Vu Thi Thu Huyen; Nguyen Mai Anh; Nguyen Thi Hue; Phi Thi Dao; Nguyen Thuy Linh; Pham Van Cuong; Doan Thi Mai Huong
- Source:
- Chemistry of natural compounds 2022 v.58 no.4 pp. 704-707
- ISSN:
- 0009-3130
- Subject:
- Nocardiopsis; antimicrobial properties; benzoic acid; chemistry; cinnamic acid; culture media; secondary metabolites; vanillin
- Abstract:
- ... Analysis of an antimicrobial extract prepared from the culture broth of the marine-derived actinomycete Nocardiopsis synnemataformans (HT06 strain) led to the isolation of a new C-glucoside benzoic acid derivative, 4βC-glucopyranosyl-3,5-dihydroxy-2-methoxybenzoic acid (1), along with eight known compounds, norharman (2), (E)-4-(3-hydroxy-4-methoxyphenyl)but-3-en-2-one (3), methyl 2,3,4,9-tetrahyd ...
- DOI:
- 10.1007/s10600-022-03772-0
- https://doi.org/10.1007/s10600-022-03772-0
- Author:
- Jiang Hu; Jiaxun Li; Qiang Li; Xia Mao; Tianfeng Peng; Nianhua Jin; Huiqing Liu; Si Yin; Chong Liu
- Source:
- Chemistry of natural compounds 2022 v.58 no.2 pp. 312-315
- ISSN:
- 0009-3130
- Subject:
- Aconitum; acetaminophen; analgesic effect; aspirin; chemistry; mass spectrometry; nuclear magnetic resonance spectroscopy; phytochemicals
- Abstract:
- ... Phytochemical investigation of the roots of Aconitum pseudostapfianum resulted in the isolation of two new C19-diterpenoid alkaloids, designated as pseudostapines A and B (1 and 2). Their structures were determined by spectral methods such as 1D and 2D (¹H–¹H COSY, HMQC, NOESY, and HMBC) NMR spectroscopy, in addition to high-resolution mass spectrometry. The isolated alkaloids were tested in vivo ...
- DOI:
- 10.1007/s10600-022-03666-1
- https://doi.org/10.1007/s10600-022-03666-1
- Author:
- M. Hojahmat; A. Wali; G. Yanhua; Y. Aili; G. T. Mavlonov; Sh. Ya. Mirzaakhmedov; A. Yili
- Source:
- Chemistry of natural compounds 2022 v.58 no.4 pp. 721-725
- ISSN:
- 0009-3130
- Subject:
- antioxidant activity; blood serum; casein; cattle; cow colostrum; hydrolysis; hydroxyl radicals; pH; papain; peptides; protein hydrolysates; trypsin; ultrafiltration
- Abstract:
- ... Casein was removed from defatted bovine colostrum by precipitation at pH 4.3. Serum proteins were hydrolyzed by trypsin, alkalase, and papain. The degree of hydrolysis (DH) of colostrum serum proteins was determined from the reaction with o-phthalaldehyde (OPA). The obtained fractions were placed in the following order: alkalase > trypsin > papain. The peptides obtained by alkalase treatment were ...
- DOI:
- 10.1007/s10600-022-03776-w
- https://doi.org/10.1007/s10600-022-03776-w
- Author:
- M. Ozer; H. Caliskan; T. Sabudak; H. H. Orak; B. Batar; D. Gulen; E. Serdal
- Source:
- Chemistry of natural compounds 2022 v.58 no.2 pp. 264-268
- ISSN:
- 0009-3130
- Subject:
- Cirsium; antioxidants; phenolic acids; spectroscopy
- Abstract:
- ... In the our ongoing studies on the isolation of new molecules from Cirsium creticum subsp. creticum (Asteraceae), a new phenolic acid derivative 1 was isolated from the plant. Its structure was established on the basis of various spectroscopic methods. As part of our investigations into the biological activities of isolated bioactive compounds, antioxidant, antibacterial, and antiproliferative acti ...
- DOI:
- 10.1007/s10600-022-03656-3
- https://doi.org/10.1007/s10600-022-03656-3
- Author:
- Ya-Ning Zhu; Ming-Xin Liu; Bing-Biao Cai; Yong Li; Man-Fei Li; Hua-Shun Liu; Min Zhou; Guang-Yu Yang; Qiu-Fen Hu; Yin-Ke Li; Xue-Mei Li
- Source:
- Chemistry of natural compounds 2022 v.58 no.4 pp. 712-716
- ISSN:
- 0009-3130
- Subject:
- Aspergillus versicolor; antiviral properties; chemistry; fungi; indoles; spectroscopy; tobacco; viruses
- Abstract:
- ... Two new (1 and 2) and four known (3–6) CPA-type indole alkaloids were isolated from the fungus Aspergillus versicolor. Their structures were determined by means of HR-ESI-MS and extensive 1D and 2D NMR spectroscopic studies. Compounds 1 and 2 were tested for their anti-tobacco mosaic virus (anti-TMV) activity. The results showed that compounds 1 and 2 demonstrated potential anti-TMV activity with ...
- DOI:
- 10.1007/s10600-022-03774-y
- https://doi.org/10.1007/s10600-022-03774-y
9. Asymmetric Synthesis of (S)-14-Methyl-1-Octadecene, the Sex Pheromone of the Peach Leafminer Moth
- Author:
- Guo-Guo He; Chun-Ting He; Bao-Qi Rao; Bei-Bei Chen; Hong-Jin Bai; Tao Zhang; Zhen-Ting Du
- Source:
- Chemistry of natural compounds 2022 v.58 no.2 pp. 320-325
- ISSN:
- 0009-3130
- Subject:
- carbon; chemical reactions; leafminers; moths; peaches; sex pheromones; stereoselective synthesis
- Abstract:
- ... An asymmetric synthesis of 14-methyl-1-octadecene, the sex pheromone of the peach leafminer moth, has been achieved efficiently. From a key intermediate (R)-4-(benzyloxy)-2-methylbutan-1-ol and 1,11-undecanediol, the target molecule was synthesized in 10 linear steps with 34% yield. The key intermediate (R)-4-benzyloxy-2-methylbutan-1-ol was prepared through Evans′ template (R)-4-benzyl-2-oxazolid ...
- DOI:
- 10.1007/s10600-022-03668-z
- https://doi.org/10.1007/s10600-022-03668-z
- Author:
- Saswata Rabi; Md. Nazrul Islam; Md. Din Islam; Ranajit K. Sutradhar
- Source:
- Chemistry of natural compounds 2022 v.58 no.3 pp. 485-490
- ISSN:
- 0009-3130
- Subject:
- Lagerstroemia; antifungal properties; chemistry; spectral analysis
- Abstract:
- ... Bioactive terpenoids 1 and 2 along with a known compound, β-sitosterol, have been isolated from the DCM extract of the fruits of Lagerstroemia speciosa. Structures of 1 and 2 have been established by spectroscopic analysis. In vitro antibacterial and antifungal activity of 1 and 2 have been reported. Compound 1 showed poor activity, but compound 2 exhibited significant antibacterial and antifungal ...
- DOI:
- 10.1007/s10600-022-03716-8
- https://doi.org/10.1007/s10600-022-03716-8
- Author:
- D. N. Olennikov; A. A. Shamilov
- Source:
- Chemistry of natural compounds 2022 v.58 no.2 pp. 269-273
- ISSN:
- 0009-3130
- Subject:
- Vaccinium vitis-idaea; chemistry; chromatography; mass spectrometry; nuclear magnetic resonance spectroscopy
- Abstract:
- ... Chromatographic separation of the Me₂CO extract of Vaccinium vitis-idaea L. (Ericaceae) stems isolated new catechin-O-glycosides that were identified using UV, IR, and NMR spectroscopy and mass spectrometry as (–)-epicatechin-3-O-α-L-rhamnopyranoside (vacciniside D, 1), (+)-catechin-3-O-[4′′-O-(3′′′-hydroxy-3′′′-methylglutaroyl)]-α-L-rhamnopyranoside (vacciniside E, 2), and (+)-catechin-3-O-(2′′,4 ...
- DOI:
- 10.1007/s10600-022-03657-2
- https://doi.org/10.1007/s10600-022-03657-2
- Author:
- Min Guo; Deng-Ji Lou; Lin-Jiao Shao; Yin-Fei Li; Ying-Zhong Liang; Xiao-Yan Yang
- Source:
- Chemistry of natural compounds 2022 v.58 no.4 pp. 656-658
- ISSN:
- 0009-3130
- Subject:
- Antrodiella; chemistry; fungi; sesquiterpenoids; spectroscopy
- Abstract:
- ... A new chamigrane sesquiterpene, antroalbol F (1), along with one known compound, acaciicolinol C (2), were isolated from cultures of the fungus Antrodiella albocinnamomea. The structures were elucidated by extensive spectroscopic methods and comparison with literature data. ...
- DOI:
- 10.1007/s10600-022-03764-0
- https://doi.org/10.1007/s10600-022-03764-0
- Author:
- Ying-Ying Wei; Peng Han; Jia-Qi Yue; Fan Li
- Source:
- Chemistry of natural compounds 2022 v.58 no.4 pp. 610-613
- ISSN:
- 0009-3130
- Subject:
- Eleutherococcus senticosus; chemistry; cytotoxicity; humans; lignans; spectroscopy
- Abstract:
- ... A new lignan, named 1,6-bis-(3-methoxy-4-hydroxyphenyl)hexane-1,6-dione (1), together with seven known compounds (2–8) were isolated from the EtOAc-soluble extract of Acanthopanax senticosus. Their structures were elucidated based on extensive spectroscopic analyses. All isolates were evaluated for in vitro cytotoxic activity against human cancer cells of HepG2, A549, HeLa, and MCF-7. Among them, ...
- DOI:
- 10.1007/s10600-022-03753-3
- https://doi.org/10.1007/s10600-022-03753-3
- Author:
- M. M. Benidze; A. V. Skhirtladze; M. Z. Getia; E. P. Kemertelidze
- Source:
- Chemistry of natural compounds 2022 v.58 no.1 pp. 50-54
- ISSN:
- 0009-3130
- Subject:
- Yucca gloriosa; glycosides; sesquiterpenoids; triterpenoids; Georgia
- Abstract:
- ... Four new sesquiterpene glycosides and one triterpene glycoside were isolated from flowers of Yucca gloriosa L. introduced into Georgia. ...
- DOI:
- 10.1007/s10600-022-03595-z
- https://doi.org/10.1007/s10600-022-03595-z
- Author:
- M. Belguidoum; H. Dendougui; H. Araya; Y. Fujimoto; S. Akkal; C. Bensaci; A. Belfar; K. Bireche; M. Hadjadj
- Source:
- Chemistry of natural compounds 2022 v.58 no.1 pp. 9-13
- ISSN:
- 0009-3130
- Subject:
- Zygophyllum; aerial parts; spectral analysis; sulfates; triterpenoid saponins
- Abstract:
- ... A new megastigman sulfate (1) was isolated from the aerial part of Zygophyllum gaetulum. The structure of 1 was elucidated as (E)-3-sulfooxymegastigm-7-en-9-one by analysis of spectroscopic data. In addition, 22 known compounds were isolated. Triterpenoid saponins 3, 4, 5, 7, 9, 12, and 13, and compounds 17–23 were isolated from Z. gaetulum for the first time. ...
- DOI:
- 10.1007/s10600-022-03588-y
- https://doi.org/10.1007/s10600-022-03588-y
- Author:
- Jia-Rui Jiang; Jian-Duo Zhang; Geng-Yun Yin; Jian-Quan Shi; Bing-Biao Cai; Wen-Wu Yang; Le-Le Deng; Li Xu; Tao Zhou; Qiu-Fen Hu; Min Zhou; Wei-Song Kong
- Source:
- Chemistry of natural compounds 2022 v.58 no.3 pp. 420-423
- ISSN:
- 0009-3130
- Subject:
- Cassia; Staphylococcus aureus; antibacterial properties; chemistry
- Abstract:
- ... Two new chromone derivatives (1 and 2) were isolated from the twigs of Cassia auriculata. Their structures were elucidated by spectroscopic methods, including extensive 1D and 2D NMR techniques. Compounds 1 and 2 were evaluated for their anti-methicillin-resistant Staphylococcus aureus (anti-MRSA) activity. The results revealed that compounds 1 and 2 showed good inhibition with IZD of 12.8 ± 2.2 a ...
- DOI:
- 10.1007/s10600-022-03698-7
- https://doi.org/10.1007/s10600-022-03698-7
17. Comparing the Fatty Acid Composition and Neuroprotective Effects of Some Lamiaceae Taxa from Turkey
- Author:
- Tugce Fafal; Gizem Kaftan; Pelin Tastan; Bijen Kivcak; Guliz Armagan
- Source:
- Chemistry of natural compounds 2022 v.58 no.2 pp. 208-212
- ISSN:
- 0009-3130
- Subject:
- Lamium album; Phlomis; Salvia sclarea; Salvia syriaca; Stachys; cell death; cytotoxicity; fatty acid composition; hydrogen peroxide; methanol; neurons; neuroprotective effect
- Abstract:
- ... This study aims to analyze the fatty acid composition and neuroprotective potential of some selected Lamiaceae taxa from Turkey. For this purpose, methanol extracts of Lamium album L., Lamium garganicum L., Phlomis rigida Labill., Salvia syriaca L., Salvia sclarea L., and Stachys cretica subsp. anatolica Rech. f. were investigated for their activity against hydrogen peroxide induced neuronal cell ...
- DOI:
- 10.1007/s10600-022-03642-9
- https://doi.org/10.1007/s10600-022-03642-9
- Author:
- I. L. Khikmatullaev; O. Sh. Boimatov; N. K. Yuldasheva; D. Sh. Azizova; E. O. Terent’eva; R. K. Rakhmanberdyeva; S. D. Gusakova; S. F. Aripova
- Source:
- Chemistry of natural compounds 2022 v.58 no.4 pp. 596-600
- ISSN:
- 0009-3130
- Subject:
- Physalis angulata; aerial parts; esterification; polysaccharides; seeds; water solubility
- Abstract:
- ... Total alkaloids (0.6%) were isolated from the aerial part of Physalis angulata. The known alkaloids cuscohygrine and tropine were identified for the first time in it. Neutral and polar lipids from seeds and fatty acids from leaves of P. angulata were characterized. Neutral (12.35%) and polar lipids (2.18%) were isolated from seeds. Their fatty-acid compositions (16–17 constituents) were determined ...
- DOI:
- 10.1007/s10600-022-03749-z
- https://doi.org/10.1007/s10600-022-03749-z
- Author:
- Jiu-ming Li; Ting-ting Huang; Ning Xu; Xing-yang Xu; Hong-cui Yu
- Source:
- Chemistry of natural compounds 2022 v.58 no.3 pp. 520-523
- ISSN:
- 0009-3130
- Subject:
- Ostrinia furnacalis; acetates; nitric acid; oxidation; sex pheromones; sodium nitrite; spectral analysis
- Abstract:
- ... The sex pheromones of Ostrinia furnacalis Z/E-isomers of acetate of 12-tetradecene-1-ol were synthesized in an overall yield of 44.5% with 1,12-dodecanediol as a starting material via mono-esterification, PCC oxidation, and the Wittig reaction. The Z/E-isomers ratio was 72:28. Configuration transformation of Z/E-isomers 72:28 mixture treated with sodium nitrite and nitric acid resulted in the prod ...
- DOI:
- 10.1007/s10600-022-03724-8
- https://doi.org/10.1007/s10600-022-03724-8
- Author:
- R. Nuerxiati; C. F. Lu; X. Ning; A. Wubulikasimu; N. Mukhamedov; A. Aierken; Sh. Ya. Mirzaakhmedov; A. Yili
- Source:
- Chemistry of natural compounds 2022 v.58 no.2 pp. 213-216
- ISSN:
- 0009-3130
- Subject:
- Plantago ovata; antioxidants; oleic acid
- Abstract:
- ... The chemical composition of fatty acids in lipids from Plantago ovata Forssk. seeds was studied. The yield of lipids was 6.12%. The lipids consisted mainly of linoleic (41.20%) and 9-octadecenoic acid (26.56%). The antioxidant and antimicrobial activities of the obtained lipids were assessed for the first time. ...
- DOI:
- 10.1007/s10600-022-03643-8
- https://doi.org/10.1007/s10600-022-03643-8
- Author:
- Zengxin Qin; Mengfei Zhao; Kaixin Zhang; Masuo Goto; Kuo-Hsiung Lee; Jizhen Li
- Source:
- Chemistry of natural compounds 2022 v.58 no.3 pp. 398-403
- ISSN:
- 0009-3130
- Subject:
- fluorine; humans; hydrophobicity; neoplasms
- Abstract:
- ... Several neo-tanshinlactone derivatives with fluorine or the trifluoromethyl group were synthesized and their antiproliferative activities were evaluated. Compared with neo-tanshinlactone, fluorinated derivatives showed a broad activity spectrum against human tumor lines. For a neo-tanshinlactone chemical skeleton, these results also indicated that the hydrophobic group (methyl) at C-4 position and ...
- DOI:
- 10.1007/s10600-022-03694-x
- https://doi.org/10.1007/s10600-022-03694-x
- Author:
- Hai-jun Wang; Li-na Qin; Ming-Zhu Li; Xian-you Wang
- Source:
- Chemistry of natural compounds 2022 v.58 no.1 pp. 75-77
- ISSN:
- 0009-3130
- Subject:
- Magnolia hypolampra; glucosides; spectral analysis
- Abstract:
- ... A new phenylpropanoid glucoside, michehedyoside G (1), together with two known compounds, including 9-(β-D-ribofuranosyl)-adenosine (2) and (±)-1,2-methylenedioxy-4-(1,2,3-trihydroxypropyl)-benzene (3), were isolated from the seeds of Michelia hedyosperma Y. W. Law (Magnoliaceae). Their structures were confirmed by comprehensive spectroscopic analysis. ...
- DOI:
- 10.1007/s10600-022-03599-9
- https://doi.org/10.1007/s10600-022-03599-9
- Author:
- N. I. Kashchenko; D. N. Olennikov
- Source:
- Chemistry of natural compounds 2022 v.58 no.2 pp. 274-278
- ISSN:
- 0009-3130
- Subject:
- Nepeta; Schizonepeta; chemistry; glycosides; mass spectrometry; nuclear magnetic resonance spectroscopy; rosmarinic acid
- Abstract:
- ... Roots of Nepeta multifida L. (Schizonepeta multifida (L.) Briq.; Lamiaceae) contained 15 observed compounds including two new rosmarinic acid glycosides 1 and 2. UV and NMR spectroscopy and mass spectrometry showed that the new compounds were rosmarinic acid 3,3′-di-O-methyl ether 4′-O-β-D-glucopyranoside (nepetamultin C, 1) and rosmarinic acid 3′-O-methyl ether 4′-O-β-D-glucopyranoside (nepetamul ...
- DOI:
- 10.1007/s10600-022-03658-1
- https://doi.org/10.1007/s10600-022-03658-1
- Author:
- Farina Aziz; Md Abdullah Al Noman; Choudhury Mahmood Hasan; Monira Ahsan
- Source:
- Chemistry of natural compounds 2022 v.58 no.3 pp. 450-454
- ISSN:
- 0009-3130
- Subject:
- chemistry; cytotoxicity; iridoids; neoplasm cells; stomach neoplasms; triterpenoids
- Abstract:
- ... A new iridoid aglycone, 1-acetylscyphiphin B₂, along with two known iridoid aglycones and three triterpenes, was isolated from the whole plant of Lindenbergia indica. The known compounds were identified as scyphiphin B₁, 1β,6β,7α,8α,10-pentahydroxy-cis-2-oxabicyclo[4.3.0]nonane, salacianol, 20-hydroxylupan-3-one, and acetylursolic acid, all of which constitute the first record of such compounds fr ...
- DOI:
- 10.1007/s10600-022-03706-w
- https://doi.org/10.1007/s10600-022-03706-w
- Author:
- N. Sh. Kavtaradze; M. D. Alaniya; M. Z. Getia; N. M. Gogitidze; N. I. Mushkiashvili; K. G. Mulkijanyan; L. V. Mskhiladze; E. P. Kemertelidze
- Source:
- Chemistry of natural compounds 2022 v.58 no.1 pp. 27-31
- ISSN:
- 0009-3130
- Subject:
- Pueraria montana var. lobata; chemistry; daidzein; daidzin; flora; genistin; glycosides; hepatoprotective effect; liver; models; Georgia
- Abstract:
- ... The new isoflavone glycoside 3′-hydroxydaidzein-7-O-β-D-glucopyranoside and four known isoflavones (daidzin, daidzein, genistin, and ononin) were isolated from Pueraria hirsuta (Thunb.) Matsum. introduced into the flora of Georgia. Total isoflavonoids from the roots exhibited hepatoprotective activity in an in vivo experiment in an acute CCl₄-induced liver injury model in mice. ...
- DOI:
- 10.1007/s10600-022-03634-9
- https://doi.org/10.1007/s10600-022-03634-9
26. Isolation and Characterization of Anti-Inflammatory Chromones from Imperata cylindrica var. major
- Author:
- Hongyu Jiang; Huina Cao; Jingya Ruan; Wei Zhao; Ying Zhang; Yu Han; Qian Chen; Yi Zhang; Tao Wang
- Source:
- Chemistry of natural compounds 2022 v.58 no.4 pp. 623-627
- ISSN:
- 0009-3130
- Subject:
- Imperata cylindrica; anti-inflammatory activity; chemistry; lipopolysaccharides; models
- Abstract:
- ... One new chromone, 5-hydroxy-8-O-β-D-glucopyranosyl-2-(2-phenylethyl)chromone (1), along with 13 known ones (2–14) were obtained and identified from a 70% EtOH extract of Imperata cylindrica var. major (Nees) C. E. Hubb. rhizomes. Among the known isolates, 3, 6, 10, 11, 13, and 14 were gained firstly from the Imperata genus. The lipopolysaccharides (LPS)-induced RAW 264.7 cell model was established ...
- DOI:
- 10.1007/s10600-022-03756-0
- https://doi.org/10.1007/s10600-022-03756-0
- Author:
- Rongrui Wei; Qinge Ma
- Source:
- Chemistry of natural compounds 2022 v.58 no.3 pp. 407-410
- ISSN:
- 0009-3130
- Subject:
- Oenanthe javanica; chemistry; lignans; spectral analysis
- Abstract:
- ... A new lignan, named 1-phenylpropenoate-4,8′-lignan A (1), and three known lignans (2–4) were isolated from Oenanthe javanica (Blume) DC. for the first time. The structures of compounds 1–4 were determined by extensive spectroscopic data analysis and comparison with reported references. Compounds 1–4 were evaluated for their inhibitory activity against LPS-induced NO production in RAW264.7 cells. A ...
- DOI:
- 10.1007/s10600-022-03699-6
- https://doi.org/10.1007/s10600-022-03699-6
- Author:
- Xiaogen Ma; Lin Zhang; Xiaoli Zhang
- Source:
- Chemistry of natural compounds 2022 v.58 no.2 pp. 245-248
- ISSN:
- 0009-3130
- Subject:
- Hovenia acerba; Oriental traditional medicine; cell viability; chemistry; fruits; human cell lines; xanthone
- Abstract:
- ... Hovenia acerba Lindl. is not only a delicious fruit but also a traditional Chinese medicine because of its nutritional and medicinal value. A new xanthone, named 1,3-dihydroxy-2-geranyl-4-isoprenyl-5-prenyl-11,12-dimethylpyranoxanthen-10-one (1), and six known xanthones 2–7 were isolated from H. acerba Lindl. for the first time. Compounds 1–7 were assayed for their hepatoprotective activities in H ...
- DOI:
- 10.1007/s10600-022-03651-8
- https://doi.org/10.1007/s10600-022-03651-8
- Author:
- Ming-Jen Cheng; Ming-Der Wu; Sung-Yuan Hsieh; Chung-Yi Chen; Jih-Jung Chen; Yueh-Hsiung Kuo
- Source:
- Chemistry of natural compounds 2022 v.58 no.4 pp. 653-655
- ISSN:
- 0009-3130
- Subject:
- Curvularia; Oryza sativa; chemistry; endophytes; fungi; sesquiterpenoids; spectral analysis; spectroscopy
- Abstract:
- ... One new natural product, cadinane-type sesquiterpenoid, (±)-(2S*,3S*)-dihydroxy-α-corocalene (1), has been isolated from the endophytic fungus Curvularia intermedia, derived from the plant Oryza sativa. The structure was determined using spectroscopic methods, mainly 1D and 2D NMR, and comparison of the spectroscopic data with those reported for structurally related compounds. ...
- DOI:
- 10.1007/s10600-022-03763-1
- https://doi.org/10.1007/s10600-022-03763-1
- Author:
- J. Dharani; S. Ravi
- Source:
- Chemistry of natural compounds 2022 v.58 no.1 pp. 40-46
- ISSN:
- 0009-3130
- Subject:
- Cyanthillium cinereum; DNA replication; antineoplastic activity; antioxidant activity; antioxidants; cell lines; cytotoxicity; interphase; sesquiterpenoid lactones
- Abstract:
- ... Three sesquiterpene lactones has been isolated from Cyanthillium cinereum (L.) H. Rob. by bioactivity guided assay and characterized by spectral methods as compounds 1, 2, and 3. The in vitro anticancer activity was tested against 786-O, MCF-7, and K562 cells by the MTT assay. Compound 1 showed IC₅₀ values of 12.5 and 10.4 μg/mL against 786-O cell line after 48 and 72 h, respectively, and matches ...
- DOI:
- 10.1007/s10600-022-03593-1
- https://doi.org/10.1007/s10600-022-03593-1
- Author:
- Z. S. Khashimova; K. A. Kakhorova; U. Zh. Ishimov; Yu. I. Oshchepkova; Sh. I. Salikhov
- Source:
- Chemistry of natural compounds 2022 v.58 no.2 pp. 316-319
- ISSN:
- 0009-3130
- Subject:
- Alhagi; Cuscuta; cell division; chemistry; colchicine; cytotoxicity; dose response; etoposide
- Abstract:
- ... Lectin-like proteins (LLP) from Cuscuta europaea parasitizing Alhagi L. were isolated and characterized. They were found to exhibit dose-dependent cytotoxic activity against various passaged cell lines. Combined action of LLP₅₀ and etoposide and colchicine suggested that the LLP₅₀ affected primarily the S-period of cell division. ...
- DOI:
- 10.1007/s10600-022-03667-0
- https://doi.org/10.1007/s10600-022-03667-0
- Author:
- P. Grover; J. Kaur; K. A. Suri; R. Kumar; G. Bansal
- Source:
- Chemistry of natural compounds 2022 v.58 no.2 pp. 193-198
- ISSN:
- 0009-3130
- Subject:
- Nyctanthes arbor-tristis; antineoplastic activity; chemistry; chloroform; fractionation; neoplasm cells
- Abstract:
- ... A new compound, 1,1,2-tris(2′,4′-di-tert-butylphenyl)-4,4-dimethylpent-1-ene, was isolated and characterized from the leaves of Nyctanthes arbor-tristis L. The plant was subjected to bioactivity-guided fractionation, and a compound was isolated from chloroform extract that was found to have potent anticancer activity. The chloroform extract was further fractionated, and a pure compound was isolate ...
- DOI:
- 10.1007/s10600-022-03639-4
- https://doi.org/10.1007/s10600-022-03639-4
- Author:
- D. T. Asilbekova; G. Ozek; T. Ozek; Kh. M. Bobakulov; A. M. Nigmatullaev; Sh. Sh. Sagdullaev
- Source:
- Chemistry of natural compounds 2022 v.58 no.2 pp. 217-221
- ISSN:
- 0009-3130
- Subject:
- Ferula; chemistry; essential oils; fruits; Uzbekistan
- Abstract:
- ... Lipids and essential oils from Ferula prangifolia Korovin (Apiaceae) endemic in Uzbekistan were studied for the first time. The compositions of lipid fatty acids and essential oils of fruit and leaves were established. ...
- DOI:
- 10.1007/s10600-022-03644-7
- https://doi.org/10.1007/s10600-022-03644-7
- Author:
- Ming-Jen Cheng; Ming-Der Wu; Yang-Cheng Kuo; Jih-Jung Chen; Yueh-Hsiung Kuo
- Source:
- Chemistry of natural compounds 2022 v.58 no.5 pp. 822-824
- ISSN:
- 0009-3130
- Subject:
- Monascus; chemistry; red yeast rice; spectroscopy
- Abstract:
- ... A new furan-2-one, namely monafuranone (1), was isolated from the EtOAc-soluble fraction of a 95% EtOH extract of the red mold rice produced by Monascus. sp. BCRC-PINK24. The structure of 1 was elucidated by spectroscopic methods, including UV, IR, HR-ESI-MS, and extensive 1D and 2D NMR techniques. ...
- DOI:
- 10.1007/s10600-022-03806-7
- https://doi.org/10.1007/s10600-022-03806-7
- Author:
- J. F. Wu; A. Turak; R. Rouzimaimaiti; G. A. Zou; H. A. Aisa
- Source:
- Chemistry of natural compounds 2022 v.58 no.1 pp. 32-36
- ISSN:
- 0009-3130
- Subject:
- antioxidant activity; monoterpenoids; planting; testing
- Abstract:
- ... Ten monoterpenoids, including new seritramentol A (1), were isolated from Seriphidium transiliense (Poljakov) Poljakov. Compounds 2, 3, 6, and 7 were isolated from this plant as new natural compounds that were previously synthesized. The structures of the compounds were elucidated by analyzing HR-ESI-MS, UV, IR, and 1D and 2D NMR spectra and calculating ECD spectra. Their absolute configurations w ...
- DOI:
- 10.1007/s10600-022-03635-8
- https://doi.org/10.1007/s10600-022-03635-8
- Author:
- C. Y. Chen; C. L. Kao; S. T. Huang; H. C. Yeh; H. T. Li
- Source:
- Chemistry of natural compounds 2022 v.58 no.3 pp. 418-419
- ISSN:
- 0009-3130
- Subject:
- Michelia; chemistry; rooting; roots
- Abstract:
- ... A new pyran-4-one, figopyrane (2,3-dimethoxy-6-methyl-4H-pyran-4-one) (1), was isolated from the roots of Michelia figo. The structure of the new constituent was essentially elucidated by spectral evidence. ...
- DOI:
- 10.1007/s10600-022-03695-w
- https://doi.org/10.1007/s10600-022-03695-w
- Author:
- Rui-hang Hu; Yong-qiang Zhou; Chuan-wen Lei; Chang-bin Wang; Wei-qian Zhu; Xin Yin; Ying Zhou
- Source:
- Chemistry of natural compounds 2022 v.58 no.4 pp. 593-595
- ISSN:
- 0009-3130
- Subject:
- Ardisia crispa; chemistry; spectral analysis
- Abstract:
- ... A new alkyl polyglycoside, together with two known compounds (2 and 3), was isolated from the roots of Ardisia crispa (Thunb.) A. DC. Structures of these compounds were identified by 1D, 2D NMR, and HR-ESI-MS spectral data analysis. ...
- DOI:
- 10.1007/s10600-022-03748-0
- https://doi.org/10.1007/s10600-022-03748-0
- Author:
- Ni Ma; Hong-Mei Lei; Pei-Ji Zhao; Guo-Hong Li
- Source:
- Chemistry of natural compounds 2022 v.58 no.1 pp. 82-85
- ISSN:
- 0009-3130
- Subject:
- Colletotrichum; Huperzia serrata; adenosine; chemistry; endophytes; internal transcribed spacers; mycelium; nuclear magnetic resonance spectroscopy
- Abstract:
- ... An endophytic strain F169 was isolated from the plant Huperzia serrata. It was identified as Colletotrichum sp. based on the sequence at the internal transcribed spacer (ITS) region. Two new alkylated purine derivatives colletotrichadenines A (1) and B (2), as well as one known adenosine (3), were isolated from mycelia extract of the strain cultured on SDA solid medium. Their structures were eluci ...
- DOI:
- 10.1007/s10600-022-03601-4
- https://doi.org/10.1007/s10600-022-03601-4
- Author:
- Zhongyan Tang; Zhengxiang Xia
- Source:
- Chemistry of natural compounds 2022 v.58 no.5 pp. 870-873
- ISSN:
- 0009-3130
- Subject:
- carcinoma; cell lines; chemistry; cytotoxicity; diterpenoids; endometrium; glucosides; humans; inhibitory concentration 50; spectral analysis
- Abstract:
- ... A new diterpenoid glucoside, 15,16-dihydroxy-4-formyl-neo-clerodane-3,13 (Z)-dien-17-O-β-Dglucopyranosyl (1), was isolated from Sheareria nana S. Moore. The structure was elucidated by spectroscopic data. 1 was evaluated for cytotoxic activities against human endometrial carcinoma cells (Ishikawa and ECC-1). The results suggested that 1 exhibited moderate cytotoxic activity against Ishikawa and EC ...
- DOI:
- 10.1007/s10600-022-03819-2
- https://doi.org/10.1007/s10600-022-03819-2
- Author:
- C. Y. Chen; C. L. Kao; H. C. Yeh; H. T. Li; M. D. Wu; M. J. Cheng; W. J. Li
- Source:
- Chemistry of natural compounds 2022 v.58 no.3 pp. 387-389
- ISSN:
- 0009-3130
- Subject:
- 4-hydroxybenzoic acid; Liriodendron; chemistry; lignans; syringic acid; vanillic acid; vanillin
- Abstract:
- ... A new benzenoid, liriodenchic acid (1), along with nine known compounds that include two aporphine alkaloids, liriodenine (2) and (–)-anonaine (3); two lignans, (+)-syringaresinol (4) and (+)-yangambin (5); and five benzenoids, p-hydroxybenzoic acid (6), vanillic acid (7), vanillin (8), syringic acid (9), and syringaldehyde (10), were isolated from the leaves of Liriodendron chinense (Magnoliaceae ...
- DOI:
- 10.1007/s10600-022-03692-z
- https://doi.org/10.1007/s10600-022-03692-z
- Author:
- Fu-Sen Wu; I-Chou Wang; Chia-Ching Liaw; Hsueh-Yang Huang; Tsung-Hsien Chang; Chun-Lin Chen; Ping-Jyun Sung; Ming-Jen Cheng; Chu-Wen Kuo; Jih-Jung Chen
- Source:
- Chemistry of natural compounds 2022 v.58 no.5 pp. 833-838
- ISSN:
- 0009-3130
- Subject:
- Hypericum; aerial parts; benzophenones; cell lines; chemistry; spectroscopy
- Abstract:
- ... A new benzophenone derivative, hyperinagasone (1), has been isolated from the aerial part of Hypericum nagasawae together with six known compounds, trichadonic acid (2), norathyriol (3), euxanthone (4), subalatin (5), hyperielliptone D (6), and 1,4-O-diferuloylsecoisolariciresinol (7). The structure of new compound 1 was determined through spectroscopic and MS analyses. Among the isolates, compoun ...
- DOI:
- 10.1007/s10600-022-03810-x
- https://doi.org/10.1007/s10600-022-03810-x
- Author:
- C. Y. Chen; J. J. Wang; C. L. Kao; H. T. Li; M. D. Wu; M. J. Cheng
- Source:
- Chemistry of natural compounds 2022 v.58 no.4 pp. 614-616
- ISSN:
- 0009-3130
- Subject:
- Polyporaceae; Taiwanofungus camphoratus; benzoquinones; chemistry; lignans
- Abstract:
- ... A new benzoquinone, 2-hydroxy-3-methoxy-5-methyl-p-benzoquinone (1), along with 11 known compounds including three benzoquinones, 2-methoxy-6-methyl-p-benzoquinone (2), 2,3-dimethoxy-5-methyl-pbenzoquinone (3), and 2-hydroxy-5-methoxy-3-methyl-p-benzoquinone (4); three lignans, 4-hydroxysesamin (5), (+)-sesamin (6), and aptosimon (7); five benzenoids, 2,4-dimethoxy-6-methylbenzene-1,3-diol (8), be ...
- DOI:
- 10.1007/s10600-022-03754-2
- https://doi.org/10.1007/s10600-022-03754-2
- Author:
- Shuang Yang; Shuang Su; Rong-Huan Cen; Li-Jingfei Sun; Xue-Qiong Yang; Ya-Bin Yang; Zhong-Tao Ding
- Source:
- Chemistry of natural compounds 2022 v.58 no.3 pp. 404-406
- ISSN:
- 0009-3130
- Subject:
- Aspergillus; Dendrobium officinale; Irpex lacteus; Khuskia oryzae; antifungal properties; chemistry; coculture; endophytes; host plants; metabolites; spectral analysis
- Abstract:
- ... In this research, the co-culture of the host plant Dendrobium officinale, the endophyte Irpex lacteus, and the pathogenic Nigrospora oryzae was examined to study the interaction of host and endophytes by the production of metabolite. A rare butenolide, named nigrolactin (1), was isolated and its structure determined by spectral analysis. Compound 1 showed significant antifungal activity against As ...
- DOI:
- 10.1007/s10600-022-03693-y
- https://doi.org/10.1007/s10600-022-03693-y
- Author:
- Rongrui Wei; Lihua Chen; Qinge Ma
- Source:
- Chemistry of natural compounds 2022 v.58 no.3 pp. 516-519
- ISSN:
- 0009-3130
- Subject:
- alkaloids; cell death; chemistry; curcumin; neuroprotective effect
- Abstract:
- ... A new C₁₉-diterpenoid alkaloid, named 17-acetylaconitine A (1), was isolated from salted Aconiti lateralis Radix Praeparata. The structure of compound 1 was elucidated by 1D and 2D NMR, HR-ESI-MS, IR, and related references. Compound 1 exhibited moderate neuroprotective activity with IC₅₀ value of 4.51 μM, which was evaluated for its neuroprotective activity against 6-OHDA-induced cell death in SH ...
- DOI:
- 10.1007/s10600-022-03721-x
- https://doi.org/10.1007/s10600-022-03721-x
- Author:
- Dam Phuc Nguyen; Y Kieu Le; Nhung Thi Tuyet Thai; Tuan Trong Nguyen; Nhat Vu Pham; Phuoc Huu Le; Tram Thi Thu Nguyen
- Source:
- Chemistry of natural compounds 2022 v.58 no.3 pp. 459-463
- ISSN:
- 0009-3130
- Subject:
- Escherichia coli; Thespesia populnea; acetone; antifungal properties; bark; betulinic acid; chemistry; ethyl acetate; glycosides; hexane; methylene chloride; oleanolic acid; sesquiterpenoids
- Abstract:
- ... One new calamenene sesquiterpene glycoside, (1R,2R,3S,4S)-4-isopropyl-1,6-dimethyl-1,2,3,4- tetrahydronaphthalene-2,7-diol 3-O-β-D-glucopyranoside (1), along with five known compounds including betulinic acid (2), oleanolic acid (3), maslinic acid (4), daucosterol (5), and 6′-O-acetyl-β-daucosterol (6), was isolated from the bark of Thespesia populnea. The n-hexane, dichloromethane, and ethyl acet ...
- DOI:
- 10.1007/s10600-022-03707-9
- https://doi.org/10.1007/s10600-022-03707-9
- Author:
- Guang-Hua Huo; Chao-Yu Cui; Tian He; Jun-Qing Yan; Wen-Wen Peng
- Source:
- Chemistry of natural compounds 2022 v.58 no.3 pp. 468-470
- ISSN:
- 0009-3130
- Subject:
- Penicillium citrinum; Penicillium italicum; antifungal properties; chemistry; culture media; fungi; sesquiterpenoids; spectral analysis
- Abstract:
- ... A new carotane sesquiterpenoid, methyl gymnabloate (1), was isolated from the fermentation broth of the wild macrofungus Gymnopus sp. 0612-9. Its structure was elucidated by analysis of extensive spectroscopic data. The antifungal activity against Penicillium italicum and Penicillium citrinum were evaluated. Compound 1 showed moderate activities against the pathogens P. italicum and P. citrinum. ...
- DOI:
- 10.1007/s10600-022-03711-z
- https://doi.org/10.1007/s10600-022-03711-z
- Author:
- Yongsoo Kwon; Heejung Yang; Wanjoo Chun; Myong Jo Kim; Jinfeng Yang
- Source:
- Chemistry of natural compounds 2022 v.58 no.3 pp. 424-425
- ISSN:
- 0009-3130
- Subject:
- Angelica; chemistry; phytochemicals
- Abstract:
- ... Phytochemical investigation of the MeOH extract of Angelica polymorpha stem led to the isolation of a new chromone (compound 9, named polymorphachromic acid). Based on various spectral analyses, including CD spectrum, the structure of the newly identified compound was deduced to be (7S)-5,7-dihydroxy-8,8-dimethyl-4-oxo-6,7-dihydro-4H,8H-pyrano[3,2-g]chromene-2-carboxylic acid. ...
- DOI:
- 10.1007/s10600-022-03700-2
- https://doi.org/10.1007/s10600-022-03700-2
- Author:
- Liu-Bin Wei; Si-Yuan Ma; Zheng-Bing Gu; Qi-Qiu Wei
- Source:
- Chemistry of natural compounds 2022 v.58 no.2 pp. 230-232
- ISSN:
- 0009-3130
- Subject:
- Saposhnikovia divaricata; breast neoplasms; chemistry; circular dichroism spectroscopy; cytotoxicity; human cell lines; humans; prostatic neoplasms
- Abstract:
- ... One new chromone, (2′S,4′S)-5′-hydroxy-5-O-methylvisamminol (1), was isolated from the roots of Saposhnikovia divaricata. The structure of compound 1 was identified by spectroscopic methods including 1D, 2D NMR, and HR-ESI-MS data. The absolute configuration of compound 1 was elucidated by electronic circular dichroism (ECD) calculation. Compound 1 showed moderate cytotoxic activity against human ...
- DOI:
- 10.1007/s10600-022-03647-4
- https://doi.org/10.1007/s10600-022-03647-4
- Author:
- D. N. Olennikov; A. A. Shamilov
- Source:
- Chemistry of natural compounds 2022 v.58 no.2 pp. 240-244
- ISSN:
- 0009-3130
- Subject:
- Vaccinium vitis-idaea; chemistry; mass spectrometry; nuclear magnetic resonance spectroscopy
- Abstract:
- ... The new compounds vaccinisides A–C (1–3) were isolated from leaves of Vaccinium vitis-idaea (Ericaceae) and identified using chemical transformations; UV, IR, and NMR spectroscopy; and mass spectrometry as 2′ ,6′-di-O-caffeylarbutin (1), quercetin-3-O-[2′′-O-(3′′′-hydroxy-3′′′-methylglutaroyl)]-α-L-rhamnopyranoside (2), and quercetin-3-O-[2′′-O-(3′′′-hydroxy-3′′′-methylglutaroyl)-4′′-O-(3′′′′-hydr ...
- DOI:
- 10.1007/s10600-022-03650-9
- https://doi.org/10.1007/s10600-022-03650-9
- Author:
- D. N. Olennikov
- Source:
- Chemistry of natural compounds 2022 v.58 no.5 pp. 816-821
- ISSN:
- 0009-3130
- Subject:
- Peucedanum; amine oxidase (flavin-containing); chemistry; cholinesterase; chromatography; coumarins; fruits; glycosides; mass spectrometry; nuclear magnetic resonance spectroscopy; roots
- Abstract:
- ... Chromatographic separation of constituents from roots and fruit of Peucedanum morisonii Besser (Apiaceae) isolated 30 compounds, including four new coumarins 1–4. UV and NMR spectroscopy and mass spectrometry established that the new compounds were officinalin isovalerate (1), umbelliferone-6-carboxylic acid 7-O-β-D-glucopyranoside (peumoriside I, 2), umbelliferone-6-carboxylic acid 7-O-(6′-O-β-D- ...
- DOI:
- 10.1007/s10600-022-03805-8
- https://doi.org/10.1007/s10600-022-03805-8
- Author:
- Shameem A. Shameem; Abid H. Banday; Khaliquz Zaman Khan; Mudasir A. Tantry; Bashir A. Ganai
- Source:
- Chemistry of natural compounds 2022 v.58 no.1 pp. 71-74
- ISSN:
- 0009-3130
- Subject:
- Astragalus; aerial parts; chemistry; glycosides; spectral analysis
- Abstract:
- ... A new 9,19-cyclolanostane type arabinoside, 16,23;22,25-diepoxy-3β,22,23,24-tetrahydroxy-9,19-cyclolanostane-3-O-α-L-arabinopyranoside (1), together with two known compounds (2 and 3), was isolated from the aerial part of Astragalus grahamianus. The structures of these compounds were characterized and identified by 1D and 2D NMR spectroscopic techniques and HR-ESI-MS and by comparison of their spe ...
- DOI:
- 10.1007/s10600-022-03598-w
- https://doi.org/10.1007/s10600-022-03598-w
- Author:
- Yahong Xiong; Nannan Feng; Shengquan Liu; Junjie Zhu; Chunyuan Li; Weijia Ding
- Source:
- Chemistry of natural compounds 2022 v.58 no.3 pp. 394-397
- ISSN:
- 0009-3130
- Subject:
- Colletotrichum musae; Escherichia coli; Fusarium oxysporum; Phoma; antifungal properties; chemistry; endophytes; fungi; serotypes; spectral analysis
- Abstract:
- ... A new derivative of barceloneic acid A, named phomaspether J (1), was isolated from the mangrove endophytic fungus Phoma herbarum L28. Its structure was elucidated by comprehensive spectroscopic analysis. It displayed strong antifungal activity against Colletotrichum musae and Fusarium oxysporum, and weak activity towards two serotypes of Escherichia coli (O6 and O78). ...
- DOI:
- 10.1007/s10600-022-03690-1
- https://doi.org/10.1007/s10600-022-03690-1
- Author:
- Ying-Nan Zhao; Ming Zhao; Jun Li; Zhi-Chun Shi; Dan Wang; Li-Qiu Sun; Jin-Lan Wang; Shu-Jun Zhang
- Source:
- Chemistry of natural compounds 2022 v.58 no.5 pp. 845-847
- ISSN:
- 0009-3130
- Subject:
- Betula pendula subsp. mandshurica; chemistry; ethyl acetate; spectroscopy
- Abstract:
- ... A new diarylheptanoid, 3,4-dihydroxy-1,7-bis(4′ ,4′′-dihydroxyphenyl)-heptane (1), was isolated from the ethyl acetate extract of Betula platyphylla. Its structure was established by spectroscopic analyses, including 1D and 2D NMR (¹H, ¹³C, COSY, HMBC, and HSQC) and HR-ESI-TOFMS, and comparison with the data of known analogs. ...
- DOI:
- 10.1007/s10600-022-03813-8
- https://doi.org/10.1007/s10600-022-03813-8
- Author:
- Mohamed A. El-Ansari; Rasha R. Abdel-Latif; Katarzyana Baczek; Hanem M. Awad; Mohamed Sharaf
- Source:
- Chemistry of natural compounds 2022 v.58 no.3 pp. 433-437
- ISSN:
- 0009-3130
- Subject:
- Filipendula vulgaris; chemistry; cytotoxicity; doxorubicin; glucosides; humans; neoplasm cells; quercetin; spectroscopy; Poland
- Abstract:
- ... From the methanolic extract of the flowers of Filipendula vulgaris, a new dimeric flavonol is isolated and identified as quercetinyl 3-O-glucoside-4′-O-4′′′′-quercetin (QI 3-O-glucoside-4′-O-4′′′′-QII) by chemical and spectroscopic methods. Also, six known flavonoids were isolated from the flowers for the first time and identified. The methanolic extract of the flowers (F) and quercetin (7), which ...
- DOI:
- 10.1007/s10600-022-03703-z
- https://doi.org/10.1007/s10600-022-03703-z
- Author:
- Shuang Yang; Wen-Zhi Shi; Xing Long; Shi-Yu Li; Li-Jingfei Sun; Rong-Huang Ceng; Shuang Su; Xue-Qiong Yang; Ya-Bin Yang; Zhong-Tao Ding
- Source:
- Chemistry of natural compounds 2022 v.58 no.2 pp. 261-263
- ISSN:
- 0009-3130
- Subject:
- Boletus edulis; Epicoccum sorghinum; Glomerella cingulata; Khuskia oryzae; biphenyl; chemistry; metabolites; mushrooms; phytotoxins; plant pathogens
- Abstract:
- ... An endogenous fungus was isolated from the edible mushroom Boletus edulis and determined as Phoma sp. The metabolites from Phoma sp. NM-46 were investigated. A new diphenyl derivative and two known phytotoxins were found from Phoma sp. NM-46, and their structures were determined by 1D NMR, 2D NMR, and HR-ESI-MS. The phytotoxins (2, 3) indicated obvious antifungal activities against phytopathogens, ...
- DOI:
- 10.1007/s10600-022-03654-5
- https://doi.org/10.1007/s10600-022-03654-5
- Author:
- C. Y. Chen; C. L. Kao; S. T. Huang; H. C. Yeh; H. T. Li; M. D. Wu; W. J. Li; M. J. Cheng
- Source:
- Chemistry of natural compounds 2022 v.58 no.4 pp. 634-636
- ISSN:
- 0009-3130
- Subject:
- Aquilaria sinensis; chemistry; diphenyl ethers
- Abstract:
- ... A new diphenyl ether, 3,3′-dihydroxy-2,2′,4,4′-tetramethoxy-6,6′-dimethyldiphenyl ether (1) was isolated from the woods of Aquilaria sinensis (Lour.) Spreng. (Thymelaeaceae). The structure of the new diphenyl ether was elucidated by chemical and physical evidence. ...
- DOI:
- 10.1007/s10600-022-03758-y
- https://doi.org/10.1007/s10600-022-03758-y
- Author:
- Lin-Jiao Shao; Deng-Ji Lou; Yin-Fei Li; Ying-Zhong Liang; Wan-Rong Niu; Min Guo; Xiao-Yan Yang
- Source:
- Chemistry of natural compounds 2022 v.58 no.3 pp. 464-467
- ISSN:
- 0009-3130
- Subject:
- Pholiota microspora; chemistry; circular dichroism spectroscopy; fungi; sesquiterpenoids; spectral analysis
- Abstract:
- ... A new eremophilane sesquiterpene (1), together with four known sesquiterpenes, donacinol B (2), donacinol C (3), trichapargin A (4), and trichapargin B (5), were isolated from cultures of the fungus Pholiota nameko. The structure of compound 1 was elucidated by extensive spectroscopic analysis and electronic circular dichroism (ECD) calculations. The known compounds (2–5) were determined by compar ...
- DOI:
- 10.1007/s10600-022-03710-0
- https://doi.org/10.1007/s10600-022-03710-0
- Author:
- Muhammad S. Ali; Aqsa Sultan; Mehreen Lateef; Ayesha Ashfaq
- Source:
- Chemistry of natural compounds 2022 v.58 no.2 pp. 233-236
- ISSN:
- 0009-3130
- Subject:
- Alstonia scholaris; Proteus mirabilis; acetates; antibacterial properties; chemistry; dicoumarol; flavones; urease
- Abstract:
- ... 5,6-Benzoflavone (1), a new natural product, has been isolated from the EtOH extract of the flowers of Alstonia scholaris (L.) R. Br. (Apocynaceae), along with the known compound dicoumarol (2). Phytochemical studies on the fruits also provided bergenin (3), 9,19-cycloart-23-ene-3,25-diol (4), 11-oxo-α-amyrin acetate (5), and marsformoxide B (6). Compounds 2–6 have been isolated for the first time ...
- DOI:
- 10.1007/s10600-022-03648-3
- https://doi.org/10.1007/s10600-022-03648-3
- Author:
- Rongrui Wei; Zhipei Sang; Qinge Ma
- Source:
- Chemistry of natural compounds 2022 v.58 no.5 pp. 808-811
- ISSN:
- 0009-3130
- Subject:
- Oenanthe javanica; anti-inflammatory activity; chemistry; lignans; spectral analysis
- Abstract:
- ... A new geranylated lignan, named 8′-geranylated lignan A (1), and a known lignan (2) were isolated from Oenanthe javanica (Blume) DC., to our knowledge, for the first time. Compounds 1 and 2 were determined by analyzing their extensive spectral data and comparing them with related references. Compounds 1 and 2 exhibited anti-inflammatory activities with IC₅₀ values of 15.24 ± 0.39 μM and 20.07 ± 0. ...
- DOI:
- 10.1007/s10600-022-03803-w
- https://doi.org/10.1007/s10600-022-03803-w
- Author:
- C. Y. Chen; C. L. Kao; M. H. Huang; H. T. Li
- Source:
- Chemistry of natural compounds 2022 v.58 no.3 pp. 438-441
- ISSN:
- 0009-3130
- Subject:
- 4-hydroxybenzoic acid; Michelia; caffeic acid; chemistry; glycosides; hydroxybenzaldehyde; stigmasterol; vanillic acid
- Abstract:
- ... Fuscatin B (1), liriodenine, (–)-anonaine, northalifoline, thalifoline, p-hydroxybenzoic acid, p-hydroxybenzaldehyde, vanillic acid, isovanillic acid, β-sitosterol, stigmasterol, 11,13-dehydrolanuginolide, and costunolide were isolated from the unripe flowers of Michelia fuscata (Magnoliaceae). Among them, fuscatin B is a new glycoside (caffeic acid phenethyl ester 3-O-4′′-rhamnosyl-(1′′→3′′′)-glu ...
- DOI:
- 10.1007/s10600-022-03704-y
- https://doi.org/10.1007/s10600-022-03704-y
61. A New Icetexane Diterpenoid from the Endophytic Fungus Annulohypoxylon multiforme var. alaskense
- Author:
- Ming-Jen Cheng; Ming-Der Wu; Sung-Yuan Hsieh; Chung-Yi Chen; Jih-Jung Chen; Yueh-Hsiung Kuo
- Source:
- Chemistry of natural compounds 2022 v.58 no.3 pp. 471-473
- ISSN:
- 0009-3130
- Subject:
- Alnus formosana; chemistry; diterpenoids; endophytes; fungi; medicinal plants; spectral analysis
- Abstract:
- ... An icetexane diterpenoid, 9(10→20)-abeo-abietane diterpenoid, annlomultialaskoside (1), has been isolated from the endophytic fungus Annulohypoxylon multiforme var. alaskense, derived from the medicinal plant Alnus formosana. The structure was determined by spectroscopic methods, mainly 1D and 2D NMR, and comparison of the spectroscopic data with those reported for structurally related compounds. ...
- DOI:
- 10.1007/s10600-022-03713-x
- https://doi.org/10.1007/s10600-022-03713-x
- Author:
- C. Y. Chen; C. L. Kao; H. C. Yeh; H. T. Li; M. D. Wu; M. J. Cheng; W. J. Li
- Source:
- Chemistry of natural compounds 2022 v.58 no.3 pp. 385-386
- ISSN:
- 0009-3130
- Subject:
- Nymphaeaceae; chemistry; ketones; leaves
- Abstract:
- ... A new ketone, vicamazone (4-(2-butoxyethoxy)-4-methylpentan-2-one) (1), was isolated from the leaves of Victoria amazonica (Nymphaeaceae). The structure of the new 4-methylpentan-2-one derivative was elucidated by chemical and physical evidences. ...
- DOI:
- 10.1007/s10600-022-03691-0
- https://doi.org/10.1007/s10600-022-03691-0
- Author:
- Jin-Lan Wang; Zhi-Hua Liu; Ying-Nan Zhao; Jun Li; Zhi-Chun Shi; Xin-Rui Liang; Ming Zhao; Shu-Jun Zhang
- Source:
- Chemistry of natural compounds 2022 v.58 no.4 pp. 601-603
- ISSN:
- 0009-3130
- Subject:
- Cannabis sativa; chemistry; ethyl acetate; lactams; spectroscopy
- Abstract:
- ... A new lactam, 5-hydroxy-1-[(4-hydroxyphenyl)methyl]-2-pyrrolidinone (1), was isolated from the ethyl acetate extract of Cannabis sativa L. The structure was established by spectroscopic analyses, including 1D and 2D NMR (¹H, ¹³C, COSY, HMBC, HSQC) and EI-MS, and comparison with the data of known analogs. ...
- DOI:
- 10.1007/s10600-022-03750-6
- https://doi.org/10.1007/s10600-022-03750-6
- Author:
- Dao-Wang Lu; Xun Zhang; Mei-Hang Chen
- Source:
- Chemistry of natural compounds 2022 v.58 no.3 pp. 411-413
- ISSN:
- 0009-3130
- Subject:
- Gymnotheca involucrata; chemistry; lignans; medicinal plants
- Abstract:
- ... A new lignan, named gymnotheinvolin (1), and three known compounds (2–4) were isolated from the Chinese medicinal plant Gymnotheca involucrata. The structure of the new compound was established on the basis of 1D and 2D NMR experiments. ...
- DOI:
- 10.1007/s10600-022-03697-8
- https://doi.org/10.1007/s10600-022-03697-8
- Author:
- Nguyen Thanh Tra; Nguyen Ngoc Nhu Thuy; Nguyen Van Tuyen; Nguyen Thi Thu Ha; Le Thi Tu Anh; Ninh The Son
- Source:
- Chemistry of natural compounds 2022 v.58 no.4 pp. 607-609
- ISSN:
- 0009-3130
- Subject:
- Styrax; chemistry; ethyl acetate; lignans; phytochemicals
- Abstract:
- ... Phytochemical investigation of the ethyl acetate extract of Styrax annamensis leaves has led to the isolation and determination of a new lignan, 7R,8S,7′S,8′R-3,4,3′-trimethoxy-9,4′,7′-trihydroxy-8.8′,7.O.9′-lignan (1), together with a known compound, 4-ketopinoresinol (2). Compound 2 was isolated from the genus Styrax for the first time, and showed moderate activity to capture the DPPH radical wi ...
- DOI:
- 10.1007/s10600-022-03752-4
- https://doi.org/10.1007/s10600-022-03752-4
- Author:
- Yu-Xin Yan; Li-Jun Yan; Yong-Chao Wang; Ming-Hua Qiu
- Source:
- Chemistry of natural compounds 2022 v.58 no.3 pp. 482-484
- ISSN:
- 0009-3130
- Subject:
- Azadirachta indica; chemistry; leaves; stems
- Abstract:
- ... A new limonoid, 3-acetoxy-7-(2′-methylpropenoyl)-vilasinin lactone (1), together with a known analogue, 3-acetoxy-7-tigloylvilasinin lactone (2), was isolated from the leaves and stems of Azadirachta indica. Their structures were elucidated based on spectral methods and by comparison with the literature. ...
- DOI:
- 10.1007/s10600-022-03715-9
- https://doi.org/10.1007/s10600-022-03715-9
- Author:
- Jih-Jung Chen; Ming-Jen Cheng; Ming-Der Wu; Nanthaphong Khamthong
- Source:
- Chemistry of natural compounds 2022 v.58 no.2 pp. 287-289
- ISSN:
- 0009-3130
- Subject:
- Monascus; chemistry; diterpenoids; fungi; metabolites; mutants; phytochemicals; red yeast rice; spectral analysis
- Abstract:
- ... Phytochemical investigation of the CH₂Cl₂-soluble fraction of the EtOH extract of red mold rice fermented with the white mutant of the fungus Monascus argentinensis BCRC 33998 (Eurotiaceae) led to the isolation and characterization of a new diterpenoid, monascusargentinoic acid (1). The structure of the new compound was elucidated by analysis of its spectroscopic data, including MS, 1D, and 2D NMR ...
- DOI:
- 10.1007/s10600-022-03661-6
- https://doi.org/10.1007/s10600-022-03661-6
- Author:
- Ming-Jen Cheng; Ming-Der Wu; Chung-Yi Chen; Wen-Huang Peng; Jih-Jung Chen
- Source:
- Chemistry of natural compounds 2022 v.58 no.2 pp. 283-286
- ISSN:
- 0009-3130
- Subject:
- Monascus; chemistry; fungi; metabolites; mutants; red yeast rice; sesquiterpenoids
- Abstract:
- ... Careful examination of the hexane-soluble fraction of the ethanolic extract of red mold rice fermented with the yellow mutant of the fungus Monascus lunisporas BCRC 33640 (Eurotiaceae) led to the isolation of a new sesquiterpenoid derivative, namely monasuslunin (1) together with nine known compounds (2–10). Their structures were elucidated on the basis of extensive 1D and 2D NMR as well as HR-ESI ...
- DOI:
- 10.1007/s10600-022-03660-7
- https://doi.org/10.1007/s10600-022-03660-7
- Author:
- Yu-Peng Li; Ya-Ping Chen; Xing-Long Chen; Yong-Sheng Tao; Rong-Ping Zhang
- Source:
- Chemistry of natural compounds 2022 v.58 no.1 pp. 6-8
- ISSN:
- 0009-3130
- Subject:
- Pleione; acarbose; chemistry; phenanthrenes
- Abstract:
- ... A new phenanthrene, 2,3,7-trihydroxy-4,8-dimethoxyphenanthrene (1), was isolated from Pleione maculata. Its structure was determined on the basis of NMR (1D and 2D) and HR-ESI-MS data. The new compound was also evaluated for its α-glucosidase inhibitory activity. Compared with the positive control, the new compound even slightly exceeded the effect of acarbose. ...
- DOI:
- 10.1007/s10600-022-03587-z
- https://doi.org/10.1007/s10600-022-03587-z
- Author:
- Man Wang; Yan Wang; Lei Shi; Yi’an Lu; Haiying Zhu; Lin Liang; Zhen-Liang Sun
- Source:
- Chemistry of natural compounds 2022 v.58 no.2 pp. 237-239
- ISSN:
- 0009-3130
- Subject:
- Mentha longifolia; aerial parts; chemistry; circular dichroism spectroscopy; lipopolysaccharides; nitric oxide; spectral analysis
- Abstract:
- ... One new phenylpropanoid-substituted flavan-3-ol, named longifoin A, together with five known compounds, was isolated from the aerial part of Mentha longifolia. Their structures were elucidated on the basis of spectral analysis, including 1D and 2D NMR and electronic circular dichroism calculations. Compound 1 significantly inhibited nitric oxide production in lipopolysaccharide induced RAW 264.7 c ...
- DOI:
- 10.1007/s10600-022-03649-2
- https://doi.org/10.1007/s10600-022-03649-2
- Author:
- Yun-Yun Zhou; Chen-Zhong Jin; Ying-Qun Ma; Xue-Jiao Zhang; Xiu Liu; Shun-Li Xiao
- Source:
- Chemistry of natural compounds 2022 v.58 no.1 pp. 47-49
- ISSN:
- 0009-3130
- Subject:
- Inula britannica; chemical structure; lettuce; phytotoxicity; sesquiterpenoids
- Abstract:
- ... A new eudesmane sesquiterpene, 12-acetoxy-1β,2α-dihydroxyeudesma-4(15),11(13)-diene (1), was isolated from Inula japonica. The chemical structure of compound 1 was elucidated by advanced spectroscopy techniques, such as ¹H, ¹³C NMR, HMBC, HSQC, COSY, and NOESY. The compound 1 presented phytotoxic effect on the growth of lettuce at 250 ppm. ...
- DOI:
- 10.1007/s10600-022-03594-0
- https://doi.org/10.1007/s10600-022-03594-0
- Author:
- Hyeon Seok Jang; Seong Yeon Choi; Birang Jeong; Jiho Lee; Yongsoo Kwon; Heejung Yang
- Source:
- Chemistry of natural compounds 2022 v.58 no.5 pp. 866-869
- ISSN:
- 0009-3130
- Subject:
- Stapelia; chemistry; glycosides; pregnanes; spectral analysis
- Abstract:
- ... Two new pregnane glycosides (1 and 2) were isolated from Stapelia gigantea. The structures were determined by 1D and 2D NMR spectral analysis. The absolute configurations of compounds 1 and 2 were determined by NOESY and coupling constants analyses. ...
- DOI:
- 10.1007/s10600-022-03818-3
- https://doi.org/10.1007/s10600-022-03818-3
- Author:
- Jun Li; Dayong Zheng; Ning Wei; Yunfeng Sun; Li Liu; Yuan Yuan; Qinghua Jiang
- Source:
- Chemistry of natural compounds 2022 v.58 no.4 pp. 650-652
- ISSN:
- 0009-3130
- Subject:
- Brucea javanica; chemistry; macrophages; nitric oxide
- Abstract:
- ... A new quassinoid, dehydrobruceantinol B (1), was isolated from the seeds of Brucea javanica, together with two known compounds, bruceantinol (2) and bruceine A (3). The structure of the new compound 1 was elucidated by advanced spectrometric methods, including HR-MS, UV, IR, 1D and 2D NMR experiments. The inhibitory effects of 1–3 on nitric oxide production in lipopolysaccharide-activated macropha ...
- DOI:
- 10.1007/s10600-022-03762-2
- https://doi.org/10.1007/s10600-022-03762-2
- Author:
- Lien T. M. Do; Tuyet T. A. Nguyen; Phung K. P. Nguyen; Truong L. Tuong; Toan N. Vo; Jirapast Sichaem
- Source:
- Chemistry of natural compounds 2022 v.58 no.2 pp. 227-229
- ISSN:
- 0009-3130
- Subject:
- Boerhavia erecta; aerial parts; chemistry; spectral analysis
- Abstract:
- ... A previously unreported rotenoid derivative, boeractanone (1), along with four known compounds, isobavachalcone (2), syringaresinol (3), 4-hydroxy-3-methoxybenzoic acid (4), and 3,4-dihydroxybenzoic acid (5), was isolated from the aerial part of Boerhavia erecta L. Their structures were elucidated by spectroscopic data analysis (1D and 2D NMR and HR-ESI-MS) and comparison with published NMR data. ...
- DOI:
- 10.1007/s10600-022-03646-5
- https://doi.org/10.1007/s10600-022-03646-5
- Author:
- Hoang-Thuy-Tien Le; Thuc-Huy Duong; Quyen-Thien-Phuc Tran; Nguyen-Kim-Tuyen Pham; Ngoc-Hong Nguyen; Minh-Hiep Dinh; Van-Son Dang; Jirapast Sichaem
- Source:
- Chemistry of natural compounds 2022 v.58 no.5 pp. 853-856
- ISSN:
- 0009-3130
- Subject:
- Bombax ceiba; Staphylococcus aureus; antibacterial properties; chemistry; glycosides; kaempferol; naringenin; procyanidins; quercetin; sesquiterpenoids
- Abstract:
- ... A new sesquiterpene glycoside, ceibanoside (1), was isolated from the leaves of Bombax ceiba, together with the previously-reported quercetin (2), kaempferol (3), naringenin (4), (+)-epicatechin (5), and procyanidin B2 (6). The structure of the new sesquiterpene glycoside was elucidated using chemical and physical evidence. Compound 2 showed antibacterial activity against Staphylococcus aureus, pr ...
- DOI:
- 10.1007/s10600-022-03815-6
- https://doi.org/10.1007/s10600-022-03815-6
- Author:
- Dekun Chen; Kai Zhang; Jianbing Tan; Sha Zhang; Kangping Xu; Wenxuan Wang; Fenghua Kang; Zhenxing Zou; Guishan Tan
- Source:
- Chemistry of natural compounds 2022 v.58 no.2 pp. 199-202
- ISSN:
- 0009-3130
- Subject:
- Caryopteris incana; apigenin; caffeic acid; chemistry; cytotoxicity; hepatoma; humans; luteolin; quercetin
- Abstract:
- ... A new stilbenoid, methyl 2,4-dihydroxy-6-(4-hydroxyphenethyl)-3-methylbenzoate (1), along with 11 known compounds, cirsimaritin (2), cirsiliol (3), quercetin (4), apigenin (5), acacetin (6), genkwanin (7), luteolin (8), caffeic acid (9), esculetin (10), alternariol (11), and alternariol-5-O-methyl ether (12), was isolated from the 70% EtOH extract of Caryopteris incana. The structures of these com ...
- DOI:
- 10.1007/s10600-022-03640-x
- https://doi.org/10.1007/s10600-022-03640-x
- Author:
- Bin-Bin Fan; Jia-Xiang Liu; Hai-Jun Hu; Yu-Mei Zhang
- Source:
- Chemistry of natural compounds 2022 v.58 no.2 pp. 297-300
- ISSN:
- 0009-3130
- Subject:
- adipocytes; chemistry; glucose; triterpenoids
- Abstract:
- ... One new triterpene, 6α-hydroxyilexosapogenin A (1), and nine known compounds were isolated from Metadina trichotoma. Their structures were mainly elucidated by NMR and MS spectra. As evidenced by a glucose concentration assay, compound 2 can stimulate glucose uptake in 3T3-L1 adipocytes and is the first pyrocincholic acid type triterpenoid that shows promoting glucose uptake activity. ...
- DOI:
- 10.1007/s10600-022-03663-4
- https://doi.org/10.1007/s10600-022-03663-4
- Author:
- Hui-Ming Chen; Chien-Ming Huang; Li-Chai Chen; Chang-Syun Yang; Tsung-Hsien Chang; Chun-Lin Chen; Ping-Jyun Sung; Wen-Lung Kuo; Ming-Jen Cheng; Jen-Wen Hsiao; Jih-Jung Chen
- Source:
- Chemistry of natural compounds 2022 v.58 no.3 pp. 496-500
- ISSN:
- 0009-3130
- Subject:
- Eriobotrya deflexa; chemistry; kaempferol; naringenin; quercetin; spectroscopy; ursolic acid
- Abstract:
- ... A new triterpenoid, methyl 2α-(4-hydroxybenzoyl)oxy-3β-hydroxy-urs-12-en-28-oate (1), has been isolated from the leaves of Eriobotrya deflexa f. deflexa, together with five known compounds, quercetin (2), kaempferol 3-O-β-glucoside (3), naringenin (4), ursolic acid (5), and euscaphic acid (6). The structure of new compound 1 was determined through spectroscopic and MS analyses. Among the isolates, ...
- DOI:
- 10.1007/s10600-022-03718-6
- https://doi.org/10.1007/s10600-022-03718-6
- Author:
- C. Y. Chen; C. M. Liu; H. C. Yeh; W. J. Li; H. T. Li; M. J. Cheng
- Source:
- Chemistry of natural compounds 2022 v.58 no.5 pp. 830-832
- ISSN:
- 0009-3130
- Subject:
- Epimedium; chemistry; spectral analysis
- Abstract:
- ... A new β-ionone, episagittatone (1), and eight known compounds were isolated from the stems of Epimedium sagittatum (Berberidaceae). The structure of 1 was determined by interpretation of the spectroscopic data. ...
- DOI:
- 10.1007/s10600-022-03809-4
- https://doi.org/10.1007/s10600-022-03809-4
- Author:
- C. Y. Chen; C. M. Liu; H. C. Yeh; W. J. Li; H. T. Li; M. J. Cheng; P. C. Hsieh; H. M. Wang
- Source:
- Chemistry of natural compounds 2022 v.58 no.3 pp. 455-458
- ISSN:
- 0009-3130
- Subject:
- Liriodendron tulipifera; antineoplastic activity; chemistry; dose response
- Abstract:
- ... A new β-ionone, litulipiferic acid (12), was isolated from the leaves of Liriodendron tulipifera (Magnoliaceae). The structure of the new β-ionone was elucidated by chemical and physical evidence. The anticancer effect of compounds 1–3, 5, 6, and 8 on A375 cells exhibit a dose-dependent behavior. When cells were exposed to epitulipinolide diepoxide (8) at 100 μM, the data exhibited viabilities of ...
- DOI:
- 10.1007/s10600-022-03708-8
- https://doi.org/10.1007/s10600-022-03708-8
- Author:
- T. L. Yang; C. L. Kao; C. E. Kuo; H. C. Yeh; W. J. Li; H. T. Li; C. Y. Chen
- Source:
- Chemistry of natural compounds 2022 v.58 no.5 pp. 825-827
- ISSN:
- 0009-3130
- Subject:
- Hydrangea; chemistry; spectral analysis
- Abstract:
- ... A novel bibenzyl derivative, hydrangchinenin (1), was isolated from the stems of Hydrangea chinensis Maxim. (Hydrangeaceae). Its structure was determined on the basis of spectral analysis. ...
- DOI:
- 10.1007/s10600-022-03807-6
- https://doi.org/10.1007/s10600-022-03807-6
- Author:
- C. Y. Chen; C. L. Kao; H. C. Yeh; H. T. Li; M. J. Cheng; W. J. Li
- Source:
- Chemistry of natural compounds 2022 v.58 no.5 pp. 793-795
- ISSN:
- 0009-3130
- Subject:
- Cinnamomum osmophloeum; chemistry; spectroscopy
- Abstract:
- ... Cinnamosmophin (1), along with 12 known compounds, was isolated from the barks of Cinnamomum osmophloeum (Lauraceae). Their structures were unambiguously elucidated by NMR spectroscopic analyses. ...
- DOI:
- 10.1007/s10600-022-03799-3
- https://doi.org/10.1007/s10600-022-03799-3
- Author:
- C. Y. Chen; M. D. Wu; H. C. Yeh; H. M. Wu; H. T. Li; M. J. Cheng
- Source:
- Chemistry of natural compounds 2022 v.58 no.1 pp. 18-20
- ISSN:
- 0009-3130
- Subject:
- Cinnamomum; biphenyl; chemistry; spectral analysis
- Abstract:
- ... A novel biphenyl derivative, insularione (3,3′,4,4′,6-pentahydroxy-3,4-dihydro-[1,1′-biphenyl]-2,5-dione) (1), was isolated from the stems of Cinnamomum insulari-montanum Hayata (Lauraceae) along with six known compounds. The structure of the novel biphenyl derivative was characterized on the basis of spectral analysis. ...
- DOI:
- 10.1007/s10600-022-03590-4
- https://doi.org/10.1007/s10600-022-03590-4
- Author:
- Iman Sedighimehr; Bahador Karami; Mahnaz Farahi
- Source:
- Chemistry of natural compounds 2022 v.58 no.2 pp. 249-253
- ISSN:
- 0009-3130
- Subject:
- acids; aldehydes; condensation reactions; methodology; nanocatalysts; solids; synthesis
- Abstract:
- ... In this paper, a novel and efficient method for the preparation of new indeno[1,2-b]chromene derivatives is reported. This synthetic method comprises one-pot and three-component condensation reaction between various aryl aldehydes, indane-1,3-dione and 4-hydroxychromen-2-one in the presence of Fe₃O₄@SiO₂@(CH₂)₃OPO₃H₂ as novel solid acid nanocatalyst. The structures of the synthesized products were ...
- DOI:
- 10.1007/s10600-022-03652-7
- https://doi.org/10.1007/s10600-022-03652-7
- Author:
- Kh. A. Rasulova; Kh. M. Bobakulov; Z. Ch. Abraeva; N. D. Abdullaev
- Source:
- Chemistry of natural compounds 2022 v.58 no.5 pp. 892-894
- ISSN:
- 0009-3130
- Subject:
- Haplophyllum acutifolium; aerial parts; alkaloids; chemistry; quinoline; spectral analysis; Uzbekistan
- Abstract:
- ... Alkaloids from the aerial part, seeds, and roots of the plant Haplophyllum perforatum collected in Kashkadarya Region, Republic of Uzbekistan, were studied. The new quinoline alkaloid perfirine in addition to known alkaloids (evoxine, skimmianine, glycoperine, methylevoxine, evodine, flindersine, haplamine, dictamnine, robustine, perfamine) were isolated from the seeds. Perfirine was a modified fu ...
- DOI:
- 10.1007/s10600-022-03823-6
- https://doi.org/10.1007/s10600-022-03823-6
- Author:
- Muhammad Ismail; Salma Javed; Muhammad Kazim; Abdur Razaq; Ejaz Hussain; Attia-tul-Wahab; Sajjad Ali; Muhammad Iqbal Choudhary
- Source:
- Chemistry of natural compounds 2022 v.58 no.4 pp. 637-643
- ISSN:
- 0009-3130
- Subject:
- Meloidogyne incognita; Sitophilus oryzae; Tanacetum; chemistry; insect pests; insecticidal properties; juveniles; larvae; mortality; nematicidal properties; phenylpropanoids; secondary metabolites; spectroscopy
- Abstract:
- ... One new and seven known secondary metabolites 1–8 were isolated, and the nematocidal and insecticidal activities of major compounds from Tanacetum baltistanicum Podlech (Asteraceae) were studied. The structures of these compounds were deduced based on various spectroscopic methods. Nematocidal activity was assayed by using second-stage juvenile (J2) of Meloidogyne incognita, whereas insecticidal a ...
- DOI:
- 10.1007/s10600-022-03759-x
- https://doi.org/10.1007/s10600-022-03759-x
- Author:
- D. Z. Azizov; R. K. Rakhmanberdieva; H. A. Elova
- Source:
- Chemistry of natural compounds 2022 v.58 no.4 pp. 589-592
- ISSN:
- 0009-3130
- Subject:
- Bacillus subtilis; Escherichia coli; Ferula; Klebsiella; Staphylococcus aureus; antimicrobial properties; esterification; polysaccharides; water solubility
- Abstract:
- ... Various groups of polysaccharides were isolated from roots of Ferula tenuisecta. Their monosaccharide compositions were established. Pectinic substances were determined to have a degree of esterification of 56.25%. Antimicrobial activity was found for water-soluble polysaccharides against Gram-positive (Staphylococcus aureus) and Gram-negative (Escherichia coli and Klebsiella oxitoca 1) and spore- ...
- DOI:
- 10.1007/s10600-022-03747-1
- https://doi.org/10.1007/s10600-022-03747-1
- Author:
- D. N. Olennikov; N. I. Kashchenko; A. I. Gadimli; D. I. Isaev
- Source:
- Chemistry of natural compounds 2022 v.58 no.5 pp. 799-803
- ISSN:
- 0009-3130
- Subject:
- Gentiana; aerial parts; polysaccharides; water solubility; Azerbaijan
- Abstract:
- ... Polysaccharide constituents from the aerial part of three species of Gentiana (Gentianaceae) growing in Azerbaijan were characterized for the first time. Neutral and acidic polymers and water-soluble polyphenol– polysaccharide conjugates containing fragments of phenolic acids and possessing antiradical activity were observed in G. asclepiadea L., G. cruciata L., and G. septemfida Pall. ...
- DOI:
- 10.1007/s10600-022-03801-y
- https://doi.org/10.1007/s10600-022-03801-y
- Author:
- E. V. Ermolenko; T. V. Sikorskaya
- Source:
- Chemistry of natural compounds 2022 v.58 no.5 pp. 804-807
- ISSN:
- 0009-3130
- Subject:
- Apostichopus japonicus; chemistry; integument; lipidomics; triacylglycerols
- Abstract:
- ... The Apostichopus japonicus (Selenka) is the most valuable commercial species of sea cucumbers. The profile of triacylglycerides (TAG) from the body wall of the sea cucumber has been determined for the first time. A total of 46 molecular species of TAG, the main ones of which were 16:1/16:1/16:1, 20:5/16:0/20:5, and 20:5/16:1/20:5, were identified in sea-cucumber lipids. The composition of A. japon ...
- DOI:
- 10.1007/s10600-022-03802-x
- https://doi.org/10.1007/s10600-022-03802-x
- Author:
- Chunshi Li; Tianyi Zhang; Qiaosi Zhang; Xin Liu; Jixin Zou; Xueqian Bai
- Source:
- Chemistry of natural compounds 2022 v.58 no.5 pp. 882-887
- ISSN:
- 0009-3130
- Subject:
- bioactive properties; moieties; nitroimidazoles; prostaglandin synthase; ursolic acid
- Abstract:
- ... Three novel series of derivatives by introducing a 1,2,3-triazoles moiety, 1,2,4-triazoles moiety or a nitroimidazoles ring to the ursolic acid (UA) nucleus were designed and synthesized. The biological activity of these compounds was evaluated to assess their hypoxia-inducible factor-1α (HIF-1α) and cyclooxygenase-2 (COX-2) inhibitory activities along with HIF-1α inhibitory and anti-inflammatory ...
- DOI:
- 10.1007/s10600-022-03821-8
- https://doi.org/10.1007/s10600-022-03821-8
91. Seco-Abietanoids from Cryptomeria japonica and Their Inhibitory Activity Toward Xanthine Oxidase
- Author:
- Chi-I Chang; Cheng-Chi Chen; Horng-Huey Ko; Jih-Jung Chen; Ming-Jen Cheng; Che-Yi Chao; Yueh-Hsiung Kuo
- Source:
- Chemistry of natural compounds 2022 v.58 no.3 pp. 478-481
- ISSN:
- 0009-3130
- Subject:
- Cryptomeria japonica; bark; chemistry; methanol; xanthine oxidase
- Abstract:
- ... A new seco-abietanoid, 12-methoxy-7-oxo-6,7-secoabieta-8,11,13-trien-6-oic acid (1), and a known seco-abietanoid,12-hydroxy-6,7-secoabieta-8,11,13-triene-6,7-dial (2), were isolated from the methanol extract of the bark of Cryptomeria japonica. Structure determination of the two compounds was accomplished by spectroscopic analyses including 1D and 2D NMR (¹H, ¹³C, COSY, HMQC, HMBC, and NOESY) and ...
- DOI:
- 10.1007/s10600-022-03714-w
- https://doi.org/10.1007/s10600-022-03714-w
- Author:
- Zhen-Cheng Lv; Xiang-Lu Zhou; Jia-Hui Yan; Yong-Hong Peng; Liang-Xiong Xu
- Source:
- Chemistry of natural compounds 2022 v.58 no.3 pp. 390-393
- ISSN:
- 0009-3130
- Subject:
- Castanea; Fusarium verticillioides; Phytophthora infestans; Streptomyces humidus; antifungal properties; chemistry; endophytes; fungi; macrolides; secondary metabolites; spectral analysis
- Abstract:
- ... A new macrolide, named concanamycin H (1), together with 12 known compounds (2–13), was isolated from the endophytic Streptomyces humidus SCB0232 for the first time. Compounds 1–13 were identified by analysis of spectroscopic data. Compounds trienomycin A (2) and trienomycin E (3) exhibited moderate inhibitory activities against Fusarium verticillioides and Phytophthora infestans with IC₅₀ values ...
- DOI:
- 10.1007/s10600-022-03689-8
- https://doi.org/10.1007/s10600-022-03689-8
- Author:
- Thuc-Huy Duong; Thi-Minh-Dinh Tran; Nguyen-Kim Tuyen Pham; Tri-Dinh Mai; Huu-Hung Nguyen; Ngoc-Hong Nguyen; Jirapast Sichaem
- Source:
- Chemistry of natural compounds 2022 v.58 no.5 pp. 862-865
- ISSN:
- 0009-3130
- Subject:
- Parmotrema; betulin; chemistry; ergosterol; lichens; secondary metabolites; spectroscopy; thallus
- Abstract:
- ... A new C₄₁-spiroterpenoid, norreticulatin (1), has been isolated from the thalli of Parmotrema cristiferum together with four known compounds, anadensin (2), fusicoauritone (3), ergosterol (4), and betulin (5). The structure of the new compound 1 was determined through spectroscopic and MS analyses. Compound 1 exhibited potent inhibition, with an IC₅₀ value of 8.8 μM, much lower than that of the ac ...
- DOI:
- 10.1007/s10600-022-03817-4
- https://doi.org/10.1007/s10600-022-03817-4
- Author:
- Jian-Hai Ding; Xin-Ning Han; Shi-Wei Liu; Zheng-Hui Li; Tao Feng; Ji-Kai Liu
- Source:
- Chemistry of natural compounds 2022 v.58 no.1 pp. 37-39
- ISSN:
- 0009-3130
- Subject:
- 11-beta-hydroxysteroid dehydrogenase; Pleurotus nebrodensis; humans; isozymes; mushrooms; neoplasm cells; sesquiterpenoids; spectroscopy
- Abstract:
- ... Pleunebron A (1), a new cadinane sesquiterpenoid, together with three known drimane sesquiterpenoids (2–4), was isolated from cultures of the edible mushroom Pleurotus nebrodensis. Their structures were elucidated on the basis of extensive spectroscopic methods. Compounds 1 and 2 were tested for their cytotoxicities against five human cancer cell lines and for their inhibitory activity against iso ...
- DOI:
- 10.1007/s10600-022-03592-2
- https://doi.org/10.1007/s10600-022-03592-2
- Author:
- Meili Wang; Nabuqi Bao; Qinghu Wang; Guojun Zhang; Aorigele Chen; Ying Xin
- Source:
- Chemistry of natural compounds 2022 v.58 no.3 pp. 429-432
- ISSN:
- 0009-3130
- Subject:
- Lomatogonium; chemistry; flavones; glycosides
- Abstract:
- ... A new flavone C-glycoside, named lomarotatoside A (1), together with two known ones, was isolated from Lomatogonium rotatum (L.) Fr.ex Fernald. The structure of 1 was elucidated by spectroscopic methods, including UV, IR, and HR-ESI-MS and extensive 1D and 2D NMR techniques. ...
- DOI:
- 10.1007/s10600-022-03702-0
- https://doi.org/10.1007/s10600-022-03702-0
- Author:
- Yingcai Bao; Guojun Zhang; Aorigele Chen; Biligetu Pa; Ying Xin; Qinghu Wang
- Source:
- Chemistry of natural compounds 2022 v.58 no.2 pp. 258-260
- ISSN:
- 0009-3130
- Subject:
- Artemisia; chemistry; glycosides
- Abstract:
- ... A new diphenylethane glycoside, namely artemongosid A (1), together with two known ones, were isolated from Artemisia mongolica (Fisch. ex Besser) Fisch. ex Nakai (A. mongolica). The structure of 1 was elucidated by spectroscopic methods, including UV, IR, HR-ESI-MS, and extensive 1D and 2D NMR techniques. ...
- DOI:
- 10.1007/s10600-022-03655-4
- https://doi.org/10.1007/s10600-022-03655-4
- Author:
- R. K. Rakhmanberdyeva; L. I. Shevchenko; O. Sh. Boimatov; Zh. D. Khuzhakhmedov
- Source:
- Chemistry of natural compounds 2022 v.58 no.2 pp. 203-207
- ISSN:
- 0009-3130
- Subject:
- Gleditsia triacanthos; antioxidant activity; blood; galactomannans; hemodynamics; methylation; nuclear magnetic resonance spectroscopy; water solubility
- Abstract:
- ... A water-soluble depolymerized galactomannan (DGM) polysaccharide with MM 18 kDa and Gal–Man monosaccharide ratio 1:2.1 was obtained from Gleditsia triacanthos seeds. The structure of DGM was established using methylation and ¹H and ¹³C NMR spectroscopy as (1→6)-α-D-galactopyranosyl-(1→4)-β-D-mannan. Pharmacological studies showed that the galactomannan was a constituent of the polyfunctional hemod ...
- DOI:
- 10.1007/s10600-022-03641-w
- https://doi.org/10.1007/s10600-022-03641-w
- Author:
- Bin Wang; Xu-Hua Nong; Wei-Nv Zeng; Shan-Shan Li; Gao-Yu Li; Jing Liu; Guo-Lei Huang; Cai-Juan Zheng
- Source:
- Chemistry of natural compounds 2022 v.58 no.5 pp. 812-815
- ISSN:
- 0009-3130
- Subject:
- Bacillus cereus; Escherichia coli; Penicillium; Staphylococcus aureus; Talaromyces verruculosus; antioxidant activity; circular dichroism spectroscopy; culture media; fungi; secondary metabolites; spectral analysis
- Abstract:
- ... A new compound, named penicillquei C (1), and eight known compounds (2–9), were isolated from the fermentation broth of mangrove-derived fungus Penicillium verruculosum TGM14. The structure of compound 1 was identified by comprehensive analyses of 1D and 2D NMR and HR-ESI-MS spectroscopic data, and calculated electronic circular dichroism (ECD) spectra. Compound 2 was isolated from the genus Penic ...
- DOI:
- 10.1007/s10600-022-03804-9
- https://doi.org/10.1007/s10600-022-03804-9
- Author:
- D. V. Reshetnikov; L. G. Burova; T. V. Rybalova; E. A. Bondareva; S. S. Patrushev; A. N. Evstropov; E. E. Shults
- Source:
- Chemistry of natural compounds 2022 v.58 no.5 pp. 908-915
- ISSN:
- 0009-3130
- Subject:
- Bacillus cereus; Staphylococcus aureus; amino acids; antibacterial properties; caffeine; cross-coupling reactions; microwave treatment; toluene; xanthine
- Abstract:
- ... Cross-coupling of 8-bromocaffeine, 8-bromo-1-butyltheobromine, or 8-bromo-7-butyltheophylline with α-, β-, or ω-amino-acid methyl or t-butyl ester hydrochlorides in toluene in the presence of the catalytic system Pd(OAc)₂·XantPhos and Cs₂CO₃ with microwave activation led to the formation of xanthine derivatives containing amino-acid fragments in the C-8 position. The antibacterial activity against ...
- DOI:
- 10.1007/s10600-022-03826-3
- https://doi.org/10.1007/s10600-022-03826-3
- Author:
- G. V. Giniyatullina
- Source:
- Chemistry of natural compounds 2022 v.58 no.4 pp. 684-692
- ISSN:
- 0009-3130
- Subject:
- antineoplastic activity; betulin; chemistry; colorectal neoplasms; doxorubicin; humans; neoplasm cells; ovarian neoplasms
- Abstract:
- ... O- and N-propylamino-derivatives of betulin and betulonic acid oxime and methyl ester were synthesized. Their antitumor activity against a panel of 60 human cancer cell lines was studied. Two betulin derivatives, 3β-hydroxy- 4 and 3β-O-(3-propylamino)-28-O-(3,6-diaminohexyl)lupa-20(29)-ene 5, exhibited antitumor activity against most of 60 cancer cell lines of nine different human tumor types. The ...
- DOI:
- 10.1007/s10600-022-03769-9
- https://doi.org/10.1007/s10600-022-03769-9