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- Author:
- Ahmadi, Shahin; Rahdar, Somayeh; Igwegbe, Chinenye Adaobi; Rahdar, Abbas; Shafighi, Nahid; Sadeghfar, Fardin
- Source:
- MethodsX 2019 v.6 pp. 98-106
- ISSN:
- 2215-0161
- Subject:
- Fourier transform infrared spectroscopy; adsorbents; adsorption; aqueous solutions; fluorides; fluorosis; ions; models; nanoparticles; pH
- Abstract:
- ... High concentration of fluoride above the optimum level can lead to dental and skeletal fluorosis. The data presents a method for its removal from fluoride-containing water. P/γ-Fe2O3 nanoparticles was applied as an adsorbent for the removal of fluoride ions from its aqueous solution. The structural properties of the P/γ-Fe2O3 nanoparticles before and after fluoride adsorption using the Fourier tra ...
- DOI:
- 10.1016/j.mex.2018.12.009
- https://dx.doi.org/10.1016/j.mex.2018.12.009
- Author:
- Fan, Ruemei; Chen, Ching-lung; Lin, Jui-yen; Tzeng, Jing-hua; Huang, Chih-pin; Dong, Chengdi; Huang, C.P.
- Source:
- Bioresource technology 2019 v.272 pp. 465-472
- ISSN:
- 0960-8524
- Subject:
- Fourier transform infrared spectroscopy; adsorption; ammonium; aqueous solutions; bamboos; biochar; heat production; ionic strength; moieties; nitrogen; pH; slow-release fertilizers
- Abstract:
- ... This research aims at studying the characteristics of ammonium adsorption onto hydrous bamboo biochar. Results showed that pH played the most important role in ammonium adsorption. High ionic strength enhanced the ammonium adsorption capacity of bamboo biochar. Ammonium adsorption was exothermic and spontaneous. FTIR results showed shift, disappearance, or appearance of specific functional groups ...
- DOI:
- 10.1016/j.biortech.2018.10.064
- https://dx.doi.org/10.1016/j.biortech.2018.10.064
- Author:
- Movasaghi, Zahra; Yan, Bei; Niu, Catherine
- Source:
- Industrial crops and products 2019 v.127 pp. 237-250
- ISSN:
- 0926-6690
- Subject:
- Fourier transform infrared spectroscopy; adsorbents; adsorption; agricultural industry; byproducts; cellulosic materials; ciprofloxacin; endothermy; kinetics; moieties; oat hulls; pH; pollutants; porosity; scanning electron microscopy; sorption isotherms; surface area; temperature; thermodynamics; water pollution
- Abstract:
- ... In this work, a novel and environmentally friendly adsorbent was developed from oat hulls, representative of cellulosic materials abundantly generated as by-products in agriculture industry, for removal ciprofloxacin (CIP) from water. Results of various characterization techniques (e.g. SEM, FTIR, and BET) showed substantial enhancement in porosity, surface functional groups and surface area of th ...
- DOI:
- 10.1016/j.indcrop.2018.10.051
- https://dx.doi.org/10.1016/j.indcrop.2018.10.051
- Author:
- Gadisa, Bekelcha Tesfaye; Appiah-Ntiamoah, Richard; Kim, Hern
- Source:
- Environmental science and pollution research international 2019 v.26 no.3 pp. 2734-2746
- ISSN:
- 0944-1344
- Subject:
- Fourier transform infrared spectroscopy; X-ray diffraction; X-ray photoelectron spectroscopy; adsorbents; adsorption; effluents; energy-dispersive X-ray analysis; iron; methylene blue; models; nanowires; pH; remediation; scanning electron microscopy; toxicity; zeta potential
- Abstract:
- ... Environmental and health concerns arising from the toxicity of organic dye effluents is still the issue of the twenty-first century. In that regard, this study presents iron sulfide (FeS₂) for its use in environmental remediation application. Amorphous phase FeS₂ nanowires were synthesized by PVP-assisted solvothermal reaction and were characterized using XRD, XPS, BET, FE-SEM, and EDS techniques. ...
- DOI:
- 10.1007/s11356-018-3811-3
- https://dx.doi.org/10.1007/s11356-018-3811-3
- Author:
- Jin, Jiafeng; Wang, Haoyu; Jing, Yannan; Liu, Min; Wang, Daigang; Li, Yiming; Bao, Mutai
- Source:
- Chemosphere 2019 v.215 pp. 241-247
- ISSN:
- 0045-6535
- Subject:
- Fourier transform infrared spectroscopy; biodegradation; cations; decane; dispersants; droplets; electrostatic interactions; emulsifying; emulsifying properties; emulsions; environmental impact; fluorescence microscopy; lecithins; moieties; oil spills; oil-water interface; oils; pH; polysorbates; remediation; soybeans; surface tension; surfactants; temperature
- Abstract:
- ... Eliminating the adverse environmental impact of chemical dispersants for oil spill has been a significant challenge since decades ago. Here, we prepared an effective and environmentally-friend dispersant with stable emulsifying capacity by the soybean lecithin and Tween 80. The mean droplet diameters of emulsions prepared by decane decreased from 11.3 to 4.1 μm, the emulsification index of emulsio ...
- DOI:
- 10.1016/j.chemosphere.2018.09.159
- https://dx.doi.org/10.1016/j.chemosphere.2018.09.159
- Author:
- Lassouane, Fatiha; Aït-Amar, Hamid; Amrani, Saïd; Rodriguez-Couto, Susana
- Source:
- Bioresource technology 2019 v.271 pp. 360-367
- ISSN:
- 0960-8524
- Subject:
- Fourier transform infrared spectroscopy; Trametes pubescens; adsorption; aqueous solutions; biocatalysts; bisphenol A; calcium alginate; crosslinking; glutaraldehyde; laccase; pH
- Abstract:
- ... The immobilization of crude laccase from Trametes pubescens by glutaraldehyde crosslinking prior to entrapment into Ca-alginate beads increased the immobilization yield by 30% and reduced the leaking by 7-fold compared to the immobilization with no crosslinking. The performance of the newly developed biocatalyst to degrade Bisphenol A (BPA) from aqueous solutions was tested. Thus, operating at opt ...
- DOI:
- 10.1016/j.biortech.2018.09.129
- https://dx.doi.org/10.1016/j.biortech.2018.09.129
- Author:
- Białkowska, A.; Bakar, M.; Marchut-Mikołajczyk, O.
- Source:
- Polymer degradation and stability 2019 v.159 pp. 98-106
- ISSN:
- 0141-3910
- Subject:
- crosslinking; Achromobacter xylosoxidans; emulsifying; urethane; phenol; differential scanning calorimetry; pH; Fourier transform infrared spectroscopy; biodegradation; formaldehyde; scanning electron microscopy; sulfonic acids; polyurethanes; urea; tensile strength; bacteria
- Abstract:
- ... The present work investigates the biodegradation of nonisocyanate condensation polyurethanes (NIPU) by aerobic bacterial strains (Achromobacter xylosoxidans G21). The study was conducted on linear and branched polyurethanes prepared from oligoetherol, urea, phenolsulfonic acid, 2-hydroxynaphthalene-6-sulfonic acid and various amounts of formaldehyde. The tensile strength, pH, emulsification and pr ...
- DOI:
- 10.1016/j.polymdegradstab.2018.11.011
- https://dx.doi.org/10.1016/j.polymdegradstab.2018.11.011
- Author:
- Arunprasath, T.; Sudalai, S.; Meenatchi, R.; Jeyavishnu, K.; Arumugam, A.
- Source:
- Biocatalysis and agricultural biotechnology 2019 v.17 pp. 672-679
- ISSN:
- 1878-8181
- Subject:
- Fourier transform infrared spectroscopy; Lasiodiplodia; X-ray diffraction; adsorption; adverse effects; alkanes; alkenes; amides; biodegradation; carboxylic acids; decolorization; fungi; industrial effluents; laccase; malachite green; mineralization; mutagens; mycelium; oxidation; pH; temperature; textile industry; toxicity; xenobiotics
- Abstract:
- ... Malachite green (MG) is a synthetic cationic dye widely used in the textile industry as a coloring agent. It is reported to be a potential carcinogenic and mutagenic agent for the living organisms in nature. Hence, it is essential to treat and release the industrial effluents containing MG to avoid serious and irreversible effects to both the natural environment and living organisms. An effective ...
- DOI:
- 10.1016/j.bcab.2019.01.030
- https://dx.doi.org/10.1016/j.bcab.2019.01.030
- Author:
- Toledo, Paulo V. O.; Limeira, Diego P. C.; Siqueira, Nicolas C.; Petri, Denise F. S.
- Source:
- Cellulose 2019 v.26 no.1 pp. 597-615
- ISSN:
- 0969-0239
- Subject:
- Fourier transform infrared spectroscopy; adsorbents; adsorption; carboxymethylcellulose; citric acid; copper; crosslinking; equations; freeze drying; hydrogels; ions; macropores; methylene blue; micro-computed tomography; mixing; models; pH; polyacrylic acid; reflectance; scanning electron microscopy; thermal properties
- Abstract:
- ... Interpenetrating polymer network (IPN) hydrogels were prepared by mixing carboxymethyl cellulose (CMC) solution and crosslinked poly(acrylic acid) (cPAA) single IPN hydrogel at mass ratios 100:0, 25:75, 50:50, 75:25 and 0:100 and subsequent crosslinking of CMC chains with citric acid, aimed towards the creation of full IPN hydrogels. The resulting CMC:cPAA hydrogels were freeze-dried for the deter ...
- DOI:
- 10.1007/s10570-018-02232-9
- https://dx.doi.org/10.1007/s10570-018-02232-9
- Author:
- Kaur, Kuljit; Jindal, Rajeev; Tanwar, Riteeka
- Source:
- Journal of polymers and the environment 2019 v.27 no.1 pp. 19-36
- ISSN:
- 1566-2543
- Subject:
- Fourier transform infrared spectroscopy; X-ray diffraction; adsorbents; adsorption; cation exchange; cations; chitosan; composite polymers; energy-dispersive X-ray analysis; fabrics; gelatin; heavy metals; industrial effluents; ion exchange capacity; lead; metal ions; methylene blue; models; nanocomposites; pH; remediation; scanning electron microscopy; temperature; thermal stability; tin; titration; toxicity; transmission electron microscopy
- Abstract:
- ... The present study reported the synthesis of novel organic–inorganic hybrid nanocomposite by incorporating tin (IV) based ion exchanger into the hybrid polymer network of chitosan and gelatin prepared under vacuum for the efficient removal of heavy metal ions and toxic dyes from an aqueous fluid. The physicochemical studies such as ion exchange capacity (IEC), chemical stability, thermal stability, ...
- DOI:
- 10.1007/s10924-018-1321-5
- http://dx.doi.org/10.1007/s10924-018-1321-5
- Author:
- Ibrahim, Ahmed G.; Saleh, Alaaeldine Sh.; Elsharma, Emad M.; Metwally, Essam; Siyam, Tharwat
- Source:
- International journal of biological macromolecules 2019 v.121 pp. 1287-1294
- ISSN:
- 0141-8130
- Subject:
- Fourier transform infrared spectroscopy; absorbed dose; acetic acid; adsorption; chitosan; composite polymers; copper; equations; gamma radiation; heavy metals; kinetics; metal ions; nickel; pH; pollution; sorption isotherms; thermogravimetry
- Abstract:
- ... Pollution of the environment associated with discharging the toxic heavy metals in water makes us focus the light to solve this problem. In continuation of our efforts, we aim in this work to utilize the graft copolymer (chitosan‑g‑maleic acid) to purify water from copper and nickel ions. The graft copolymer has been synthesized using gamma radiation and the grafting conditions have been optimized ...
- DOI:
- 10.1016/j.ijbiomac.2018.10.107
- https://dx.doi.org/10.1016/j.ijbiomac.2018.10.107
- Author:
- Zhao, Yiguo; Khalid, Nauman; Shu, Gaofeng; Neves, Marcos A.; Kobayashi, Isao; Nakajima, Mitsutoshi
- Source:
- Food hydrocolloids 2019 v.86 pp. 70-77
- ISSN:
- 0268-005X
- Subject:
- Fourier transform infrared spectroscopy; Pueraria montana var. lobata; anhydrides; astaxanthin; differential scanning calorimetry; electrostatic interactions; endothermy; gelatin; hydrocolloids; liquids; moieties; pH; polymers; scanning electron microscopy; separation; starch; storage time; temperature
- Abstract:
- ... The formulation of complex coacervates between gelatin and octenyl succinic anhydride (OSA) modified kudzu starch was investigated by turbidimetric analysis as a function of pH and ratio of gelatin and OSA-modified kudzu starch. The interaction between gelatin and OSA-modified kudzu starch yielded a dense liquid coacervate phase, leading to phase separation, and the optimum conditions for their co ...
- DOI:
- 10.1016/j.foodhyd.2018.01.040
- https://dx.doi.org/10.1016/j.foodhyd.2018.01.040
- Author:
- Butt, Atiya; Jabeen, Sehrish; Nisar, Numrah; Islam, Atif; Gull, Nafisa; Iqbal, Sadia Sagar; Khan, Shahzad Maqsood; Yameen, Basit
- Source:
- International journal of biological macromolecules 2019 v.121 pp. 104-112
- ISSN:
- 0141-8130
- Subject:
- Fourier transform infrared spectroscopy; biodegradability; biopolymers; chitosan; crosslinking; drugs; hydrogels; hydrophilicity; mixing; pH; scanning electron microscopy; silane; thermogravimetry
- Abstract:
- ... The novel silane crosslinked (TEOS) hydrogels based on eco-friendly biodegradable chitosan/guargum were prepared by blending with PEG to develop pH sensitive hydrogels (CGP) and achieved its hydrophilicity and target specificity for controlled release of drug. The crosslinker amount was varied to analyze its effect on the hydrogel properties and were characterized using FTIR, SEM, TGA, swelling st ...
- DOI:
- 10.1016/j.ijbiomac.2018.10.018
- https://dx.doi.org/10.1016/j.ijbiomac.2018.10.018
- Author:
- Saha, Nepu; Saba, Akbar; Reza, M. Toufiq
- Source:
- Journal of analytical and applied pyrolysis 2019 v.137 pp. 138-145
- ISSN:
- 0165-2370
- Subject:
- Fourier transform infrared spectroscopy; cellulose; dissociation; hydrochars; hydrothermal carbonization; moieties; pH; pyrolysis; temperature; titration; wood
- Abstract:
- ... The aims of this work were to quantify chemical states associated with the pH, dissociation constants, and pH at point of zero charge (pHPZC) of hydrochar and to quantify the acidic functional groups on hydrochar surface. Hydrochars from cellulose and wood treated at 180, 220, and 260 °C with 30 min residence time were produced. Boehm titration was applied to analyze acidic functional groups and d ...
- DOI:
- 10.1016/j.jaap.2018.11.018
- https://dx.doi.org/10.1016/j.jaap.2018.11.018
- Author:
- Samuel, Melvin S.; Bhattacharya, Jayanta; Raj, Sankalp; Santhanam, Needhidasan; Singh, Hemant; Pradeep Singh, N.D.
- Source:
- International journal of biological macromolecules 2019 v.121 pp. 285-292
- ISSN:
- 0141-8130
- Subject:
- Fourier transform infrared spectroscopy; X-ray diffraction; adsorbents; adsorption; aqueous solutions; chitosan; chromium; graphene oxide; models; nanocomposites; pH; scanning electron microscopy; sorption isotherms; ultrasonic treatment
- Abstract:
- ... The present study involves the adsorption of hexavalent Chromium(Cr(VI)) using chitosan grafted graphene oxide (CS-GO) nanocomposite in batch mode. The CS-GO nanocomposite material was prepared by ultrasonic irradiation technique. The CS-GO adsorbent was characterized by X-ray diffraction (XRD), Fourier transform infrared (FTIR) spectroscopy, scanning electron microscopy (SEM) and Tunnelling elect ...
- DOI:
- 10.1016/j.ijbiomac.2018.09.170
- http://dx.doi.org/10.1016/j.ijbiomac.2018.09.170
16. Efficient removal of ethidium bromide from aqueous solution by using DNA-loaded Fe3O4 nanoparticles
- Author:
- Ge, Zhiqiang; Sun, Tingting; Xing, Jinfeng; Fan, Xuejiao
- Source:
- Environmental science and pollution research international 2019 v.26 no.3 pp. 2387-2396
- ISSN:
- 0944-1344
- Subject:
- DNA; Fourier transform infrared spectroscopy; X-ray diffraction; adsorbents; adsorption; aqueous solutions; batch systems; carcinogens; chemical bonding; crystal structure; dyes; ethidium; heat production; iron oxides; magnetism; models; mutagens; nanoparticles; pH; reaction kinetics; scanning electron microscopy; sorption isotherms; temperature; transmission electron microscopy; zeta potential
- Abstract:
- ... Ethidium bromide (EtBr) is widely used as DNA-staining dyes for the detection of nucleic acids in laboratories and known to be powerful mutagens and carcinogens. In the present paper, the removal of EtBr from aqueous solutions in a batch system using DNA-loaded Fe₃O₄ nanoparticles as a simple and efficient method was investigated. DNA was covalently loaded on the surface of Fe₃O₄ magnetic nanopart ...
- DOI:
- 10.1007/s11356-018-3747-7
- https://dx.doi.org/10.1007/s11356-018-3747-7
- Author:
- Amarathunga, Udara; Diyabalanage, Saranga; Bandara, U.G.C.; Chandrajith, Rohana
- Source:
- Applied geochemistry 2019 v.100 pp. 152-159
- ISSN:
- 0883-2927
- Subject:
- Fourier transform infrared spectroscopy; aluminum; aquifers; arsenic; barium; calcium; carbonate minerals; coatings; desorption; environmental factors; geochemistry; groundwater; iron; magnesium; organic matter; oxygen; pH; potassium; rain; sediments; sodium; water table; wells; Sri Lanka
- Abstract:
- ... Elevated levels of arsenic (As) have been reported in groundwater from sandy aquifer systems in the Mannar Island, located in the northwest of Sri Lanka. As a result of serious health concerns, this study aims to investigate groundwater aquifers in order to trace the different As sources and mechanisms involved in its release from aquifer sediments. A piezometer was constructed in an As contaminat ...
- DOI:
- 10.1016/j.apgeochem.2018.11.011
- https://dx.doi.org/10.1016/j.apgeochem.2018.11.011
- Author:
- Xiong, Wei; Hu, Dongying
- Source:
- Environmental science and pollution research international 2019 v.26 no.2 pp. 1880-1891
- ISSN:
- 0944-1344
- Subject:
- Fourier transform infrared spectroscopy; activation energy; adsorbents; adsorption; aqueous solutions; bamboos; biomass; cellulose; chemical structure; dyes; endothermy; models; pH; purification methods; scanning electron microscopy; sorption isotherms; temperature
- Abstract:
- ... Cellulose from bamboo shavings (BC) separated and modified by grafting triphenylphosphine, which was used as an adsorbent for the removal of Acid Black 24 from aqueous solution. The quaternary phosphonium-based bamboo cellulose (PBC) was characterized by FTIR and SEM measurements. The FTIR studies showed that the quaternary phosphonium group was successfully grafted onto the BC molecular structure ...
- DOI:
- 10.1007/s11356-018-3711-6
- https://dx.doi.org/10.1007/s11356-018-3711-6
- Author:
- Zhang, Juan; Khan, Muhammad Asim; Xia, Mingzhu; Abdo, Abdelnasir Mahmoud; Lei, Wu; Liao, Chuan; Wang, Fengyun
- Source:
- Environmental science and pollution research international 2019 v.26 no.1 pp. 215-226
- ISSN:
- 0944-1344
- Subject:
- Fourier transform infrared spectroscopy; X-ray diffraction; adsorbents; adsorption; antibiotics; ciprofloxacin; harvesting; hot water treatment; kinetics; magnetism; montmorillonite; pH; pollutants; scanning electron microscopy; sorption isotherms; thermodynamics
- Abstract:
- ... A highly resourceful, eco-friendly, and recyclable magnetic adsorbent based on montmorillonite (CoFe₂O₄/MMT) was fabricated via a facile hydrothermal method to harvest tetracycline (TC) and ciprofloxacin (CIP) from pollutant water. The prepared adsorbent was characterized by XRD, FT-IR, SEM, and VSM methods to comprehend its structure, morphology, and magnetism. Effects of experimental parameters ...
- DOI:
- 10.1007/s11356-018-3452-6
- http://dx.doi.org/10.1007/s11356-018-3452-6
- Author:
- Chauhan, Moondeep; Sharma, Bindu; Kumar, Rajeev; Chaudhary, Ganga Ram; Hassan, Ashraf Aly; Kumar, Sandeep
- Source:
- Environmental research 2019 v.168 pp. 85-95
- ISSN:
- 0013-9351
- Subject:
- Fourier transform infrared spectroscopy; Staphylococcus aureus; X-ray diffraction; adsorbents; adsorption; animal pathogenic bacteria; antibacterial properties; chemical precipitation; copper nanoparticles; cupric oxide; dyes; energy-dispersive X-ray analysis; hot water treatment; inorganic ions; kinetics; microwave radiation; organic wastes; pH; pollution; sorption isotherms; surface area; transmission electron microscopy; virulent strains
- Abstract:
- ... Copper oxide (CuO) nanomaterials (NMs) of different size and morphology were synthesized by Chemical precipitation, Microwave irradiation and Hydrothermal method and characterized by TEM, BET, FTIR, XRD and EDX analysis. As synthesized CuO NMs were utilized for elimination of harmful dyes viz. Direct Red 81 (DR-81) and Coomassie Brilliant blue R-250 (BBR-250) and pathogenic bacteria (Staphylococcu ...
- DOI:
- 10.1016/j.envres.2018.09.024
- https://dx.doi.org/10.1016/j.envres.2018.09.024
- Author:
- Xu, Jian; Zhang, Xueliang; Sun, Cheng; Wan, Jinzhong; He, Huan; Wang, Fei; Dai, Yuxuan; Yang, Shaogui; Lin, Yusuo; Zhan, Xinhua
- Source:
- Environmental science and pollution research international 2019 v.26 no.3 pp. 2820-2834
- ISSN:
- 0944-1344
- Subject:
- Fourier transform infrared spectroscopy; X-ray diffraction; X-ray photoelectron spectroscopy; anions; aqueous solutions; bicarbonates; biochar; catalysts; chlorides; copper; energy-dispersive X-ray analysis; free radicals; hydroxyl radicals; iron; iron oxyhydroxides; nitrates; pH; peanut hulls; phosphates; pollutants; scanning electron microscopy; spectrometers; sulfates; tetracycline; wastewater
- Abstract:
- ... Peanut shell biochar (BC) supported on Cu-doped FeOOH composite (Cu–FeOOH/BC) was synthesized using a facile and scalable method. The Cu–FeOOH/BC samples were characterized by Fourier transform infrared spectroscopy (FTIR), x-ray diffraction (XRD), scanning electron microscopy equipped with an energy-dispersive spectrometer (SEM-EDS), x-ray photoelectron spectroscopy (XPS), and Brunauer-Emmett-Tel ...
- DOI:
- 10.1007/s11356-018-3777-1
- https://dx.doi.org/10.1007/s11356-018-3777-1
- Author:
- Shi, Yongli; Xue, Jintao; Sang, Yajun; Xu, Xiaoqing; Shang, Qing
- Source:
- International journal of biological macromolecules 2019 v.121 pp. 1346-1353
- ISSN:
- 0141-8130
- Subject:
- Fourier transform infrared spectroscopy; Raman spectroscopy; animal disease models; animal experimentation; blood glucose; cell viability; cytotoxicity; diabetes; glycemic effect; hydrogels; insulin; pH; photographs; polymerization; rats; scanning electron microscopes; scanning electron microscopy
- Abstract:
- ... The purpose of this study was developing a novel hydroxypropyl methyl cellulose-co-polyacrylamide-co-methacrylic acid (HPMC-co-PAM-co-PMAA) hydrogel, which was used as rectal suppository to regulate the blood glucose of diabetes. HPMC-co-PAM-co-PMAA hydrogel was fabricated via free-radical polymerization. Fourier transform infrared spectroscopy (FTIR) and Raman spectra were used to confirm the fab ...
- DOI:
- 10.1016/j.ijbiomac.2018.09.044
- http://dx.doi.org/10.1016/j.ijbiomac.2018.09.044
- Author:
- Manzoor, Muhammed A.P.; Mujeeburahiman, M.; Duwal, Surya Ram; Rekha, P.D.
- Source:
- Biocatalysis and agricultural biotechnology 2019 v.17 pp. 566-570
- ISSN:
- 1878-8181
- Subject:
- Fourier transform infrared spectroscopy; X-ray diffraction; bacteria; biomineralization; crystallization; crystals; differential scanning calorimetry; gels; magnesium ammonium phosphate; pH; scanning electron microscopy; thermogravimetry; urinary tract diseases
- Abstract:
- ... Struvite stones develop as a result of urinary tract infections by urease-producing bacteria. Here, we report the dynamics of in vitro crystallization of struvite at various pH using single diffusion gel growth technique. Sodium metasilicate gel and ammonium dihydrogen phosphate were used as a medium for growing the struvite crystals. The composition, crystalline nature, and surface morphology of ...
- DOI:
- 10.1016/j.bcab.2019.01.023
- https://dx.doi.org/10.1016/j.bcab.2019.01.023
- Author:
- Xiao, Zuobing; Liu, Min; Niu, Yunwei; Zhu, Guangyong; Deng, Juan; Liu, Sihong
- Source:
- Flavour and fragrance journal 2019 v.34 no.1 pp. 21-27
- ISSN:
- 0882-5734
- Subject:
- Fourier transform infrared spectroscopy; Lavandula; cetyltrimethylammonium bromide; dispersibility; encapsulation; ethanol; home furnishings; nanospheres; odors; pH; polymers; scanning electron microscopes; scanning electron microscopy; silane; silica; strength (mechanics); surfactants; thermal stability; thermogravimetry
- Abstract:
- ... Lavender fragrance (LF) was encapsulated successfully in ORMOSIL (organically modified silica) via the sol‐gel approach. Silane precursor‐ethylsilicate (TEOS) was modified with methyltrimethoxysilane (MTMS) to enhance the mechanical strength and compatibility of the wall material. Hexadecyl trimethyl ammonium bromide (CTAB) was added as surfactant and polymer for the formation of nanospheres. An e ...
- DOI:
- 10.1002/ffj.3474
- http://dx.doi.org/10.1002/ffj.3474
- Author:
- Yi, Xiangzhou; Zheng, Quanhui; Ding, Baomiao; Pan, Min-hsiung; Chiou, Yi-shiou; Li, Li; Li, Zhenshun
- Source:
- Lebensmittel-Wissenschaft + [i.e. und] Technologie 2019 v.99 pp. 505-512
- ISSN:
- 0023-6438
- Subject:
- Fourier transform infrared spectroscopy; circular dichroism spectroscopy; electrostatic interactions; emulsifying; emulsifying properties; fluorescence; gels; hydrogen bonding; hydrophobicity; pH; particle size; polyacrylamide; sodium dodecyl sulfate; temperature; turbidity; whey protein; zeta potential
- Abstract:
- ... The interactions between liposomes and whey proteins (WP) were investigated using sodium dodecyl sulfate polyacrylamide gel electropheresis, intrinsic fluorescence, Fourier transform infrared spectroscopy, circular dichroism spectroscopy, turbidity, particle size, and zeta potential. These results indicated that WP interacted with liposomes via electrostatic force, hydrophobic force, and hydrogen ...
- DOI:
- 10.1016/j.lwt.2018.10.002
- https://dx.doi.org/10.1016/j.lwt.2018.10.002
- Author:
- Bedade, Dattatray K.; Muley, Abhijeet B.; Singhal, Rekha S.
- Source:
- Bioresource technology 2019 v.272 pp. 137-145
- ISSN:
- 0960-8524
- Subject:
- Cupriavidus; Fourier transform infrared spectroscopy; X-ray diffraction; acetone; acrylamides; batch systems; biodegradation; carcinogens; crosslinking; enzymes; heat inactivation; industrial wastes; magnetism; models; nanoparticles; pH; particle size; scanning electron microscopy; temperature; thermal stability; wastewater
- Abstract:
- ... Acrylamidase from Cupriavidus oxalaticus ICTDB921 was immobilized on magnetic nanoparticles (MNPs) for degradation of acrylamide (a group 2A carcinogen and an environmental contaminant) from industrial waste water. Acrylamidase-MNPs were prepared (maximum recovery ∼94%) at optimized process parameters viz. 1.5:1 (v/v) of acetone: crude acrylamidase/5 mM of glutaraldehyde/90 min/1.5:1 of enzyme: MN ...
- DOI:
- 10.1016/j.biortech.2018.10.015
- https://dx.doi.org/10.1016/j.biortech.2018.10.015
- Author:
- Arab, Masoumeh; Hosseini, Seyede Marzieh; Nayebzadeh, Kooshan; Khorshidian, Nasim; Yousefi, Mojtaba; Razavi, Seyed Hadi; Mortazavian, Amir Mohammad
- Source:
- International journal of biological macromolecules 2019 v.121 pp. 691-698
- ISSN:
- 0141-8130
- Subject:
- 2,2-diphenyl-1-picrylhydrazyl; Dietzia; Fourier transform infrared spectroscopy; alginates; antioxidant activity; antioxidants; canthaxanthin; dyes; emulsions; fermented milk; gelation; heat; microencapsulation; microparticles; milk; oxygen; pH; pectins
- Abstract:
- ... Canthaxanthin (CX) is an orange-red keto-carotenoid with high antioxidant activity. This functional pigment is sensitive to oxygen, light, pH and heat. In this study, CX was produced by the Dietzia natronolimnaea HS-1 and was encapsulated in Alginate (Alg) and Alg-high methoxyl pectin (HMP) through O/W/O multiple emulsion/external gelation method to developed resistant microparticles among acidic ...
- DOI:
- 10.1016/j.ijbiomac.2018.10.114
- https://dx.doi.org/10.1016/j.ijbiomac.2018.10.114
- Author:
- Xue, Heng-Yue; Li, Jing-Ru; Liu, Yan-Geng; Gao, Qi; Wang, Xiao-Wen; Zhang, Jun-Wei; Tanokura, Masaru; Xue, You-Lin
- Source:
- International journal of biological macromolecules 2019 v.121 pp. 1186-1193
- ISSN:
- 0141-8130
- Subject:
- 2,2-diphenyl-1-picrylhydrazyl; Dioscorea oppositifolia; Dioscorea polystachya; Fourier transform infrared spectroscopy; absorption; anion exchange; antioxidant activity; cell growth; experimental design; free radicals; galactose; glucose; hydroxyl radicals; mannose; microstructure; pH; polysaccharides; powders; raw materials; regression analysis; response surface methodology; temperature; ultrafiltration; yams
- Abstract:
- ... Ultrafiltration is a separation process for purifying and concentrating macromolecular solutions. Using Baiyu yam (Dioscorea opposita Thunb) as the raw material, single-factor experiments, Box–Behnken design (BBD) and response surface methodology (RSM) were employed to investigate the effects of the ultrafiltration pH, temperature and pressure on the extraction rate of Chinese yam polysaccharide ( ...
- DOI:
- 10.1016/j.ijbiomac.2018.10.126
- https://dx.doi.org/10.1016/j.ijbiomac.2018.10.126
- Author:
- Wu, Yumeng; Jiang, Yihua; Li, Yuejun; Wang, Rong
- Source:
- Cellulose 2019 v.26 no.2 pp. 805-821
- ISSN:
- 0969-0239
- Subject:
- Fourier transform infrared spectroscopy; X-ray diffraction; X-ray photoelectron spectroscopy; adsorbents; adsorption; cellulose; copper; corn stover; emulsifiers; metal ions; moieties; pH; pollution control; potassium persulfate; scanning electron microscopes; secondary amines; sorption isotherms; thermogravimetry; toxicity; wastewater; water pollution
- Abstract:
- ... An amino functionalized microcrystalline cellulose from corn stalk was prepared and its synthesis and operation conditions were optimized to remove Cu²⁺ from wastewater. To prepare this adsorbent, cellulose was grafted by glycidyl methacrylate in the presence of OP-10 as emulsifiers and potassium persulfate as initiators, then the grafted cellulose was aminated by diethylenetriamine. Batch experim ...
- DOI:
- 10.1007/s10570-018-2113-8
- https://dx.doi.org/10.1007/s10570-018-2113-8
- Author:
- Seremeta, Daniele Cristina Hass; da Silva, Cleber Pinto; Zittel, Rosimara; de Campos, Sandro Xavier
- Source:
- Environmental science and pollution research international 2019 v.26 no.1 pp. 797-805
- ISSN:
- 0944-1344
- Subject:
- Fourier transform infrared spectroscopy; adsorbents; adsorption; cigarettes; composts; energy-dispersive X-ray analysis; equations; lead; models; organometallic compounds; pH; sewage sludge
- Abstract:
- ... The adsorption of Pb²⁺ by a compost obtained from the treatment of tobacco from smuggled cigarettes (SCT) and industrial sewage sludge (ISS) was investigated. The Pb²⁺ adsorption process was evaluated as function of different concentrations of adsorbent and adsorbate, pH variations, and contact time. Fourier transformed infrared spectroscopy (FTIR) and energy dispersive X-ray spectrometry (EDX) we ...
- DOI:
- 10.1007/s11356-018-3655-x
- http://dx.doi.org/10.1007/s11356-018-3655-x
- Author:
- Roșu, Crăița Maria; Vochița, Gabriela; Mihășan, Marius; Avădanei, Mihaela; Mihai, Cosmin Teodor; Gherghel, Daniela
- Source:
- Environmental science and pollution research international 2019 v.26 no.1 pp. 431-445
- ISSN:
- 0944-1344
- Subject:
- Candida tropicalis; Cyberlindnera saturnus; DNA damage; Fourier transform infrared spectroscopy; Pichia kudriavzevii; Trifolium pratense; Triticum aestivum; ammonium sulfate; aquatic organisms; azo dyes; biodegradation; biomarkers; bioremediation; cell viability; chromosome aberrations; comet assay; cytotoxicity; decolorization; genotoxicity; germination; glucose; high performance liquid chromatography; kidney cells; metabolites; monkeys; pH; phytotoxicity; roots; seedlings; shoots; soil; spectral analysis; toxic substances; viability assays; wastewater; yeast extract; yeasts
- Abstract:
- ... The aim of this study was to evaluate the performances of Pichia kudriavzevii CR-Y103 yeast strain for the decolorization, biodegradation, and detoxification of cationic dye C.I. Basic Blue 41, a toxic compound to aquatic life with long-lasting effects. Under optimized cultural conditions (10.0-g L⁻¹ glucose, 0.2-g L⁻¹ yeast extract, and 1.0-g L⁻¹ (NH₄)₂SO₄), the yeast strain was able to decoloriz ...
- DOI:
- 10.1007/s11356-018-3651-1
- http://dx.doi.org/10.1007/s11356-018-3651-1
- Author:
- Omran, B.A.; Nassar, H.N.; Younis, S.A.; Fatthallah, N.A.; Hamdy, A.; El‐Shatoury, E.H.; El‐Gendy, N.Sh.
- Source:
- Journal of applied microbiology 2019 v.126 no.1 pp. 138-154
- ISSN:
- 1364-5072
- Subject:
- Fourier transform infrared spectroscopy; Trichoderma longibrachiatum; X-ray diffraction; absorbance; antibacterial properties; cell membranes; cell walls; corrosion; crystal structure; filtrates; fungal biomass; industry; ions; light scattering; mixed culture; mixing; mycelium; nanoparticles; nanosilver; oils; pH; plankton; salt tolerance; scanning electron microscopes; scanning electron microscopy; silver; silver nitrate; sulfate-reducing bacteria; temperature; transmission electron microscopes; transmission electron microscopy; zeta potential
- Abstract:
- ... AIMS: In order to efficiently control the corrosive sulphate‐reducing bacteria (SRB), the main precursor of the microbial influenced corrosion (MIC) in oil industry, the ability of Trichoderma longibrachiatumDSMZ 16517 to synthesize silver nanoparticles (AgNPs) was investigated and their biocidal activity against halotolerant SRB was tested. METHODS AND RESULTS: The mycelial cell‐free filtrate (MC ...
- DOI:
- 10.1111/jam.14102
- http://dx.doi.org/10.1111/jam.14102
- Author:
- Hu, Huigang; Zhao, Qiaoli; Xie, Jianghui; Sun, Dequan
- Source:
- International journal of biological macromolecules 2019 v.121 pp. 1213-1226
- ISSN:
- 0141-8130
- Subject:
- Fourier transform infrared spectroscopy; arabinose; cellulose; dose response; endo-1,4-beta-glucanase; fucose; functional foods; galactose; galacturonic acid; gel chromatography; glucose; glucuronic acid; glycemic effect; high performance liquid chromatography; human cell lines; hydrolysis; hypoglycemic agents; insulin; insulin resistance; mannose; models; molecular weight; pH; pineapples; pomace; response surface methodology; rhamnose; scanning electron microscopy; temperature; ultrasonics; ultraviolet-visible spectroscopy; xylose
- Abstract:
- ... This study determined the optimal extraction conditions for ultrasonic-cellulase synergistic extraction of polysaccharides from pineapple pomace (PPP) using Plackett–Burman design and response surface methodology. The optimal hydrolysis temperature, ratio of material to water, pH value, hydrolysis time, ultrasonic power and the additive quantity of cellulase were 50 °C, 1:45 g/mL, 6.0, 100 min, 16 ...
- DOI:
- 10.1016/j.ijbiomac.2018.10.054
- https://dx.doi.org/10.1016/j.ijbiomac.2018.10.054
- Author:
- Sebeia, Nouha; Jabli, Mahjoub; Ghith, Adel; El Ghoul, Yassine; Alminderej, Fahad M.
- Source:
- International journal of biological macromolecules 2019 v.121 pp. 655-665
- ISSN:
- 0141-8130
- Subject:
- Fourier transform infrared spectroscopy; Nerium oleander; Pergularia; Populus tremula; X-ray diffraction; adsorbents; biosorption; cellulose; differential thermal analysis; lignin; methylene blue; nitrogen; pH; pollutants; scanning electron microscopy; sulfur; temperature; thermogravimetry
- Abstract:
- ... Cellulose-based substrates could represent potential funds for the sorption of pollutants. Herein, methylene blue was selected for demonstrating the bio-sorption efficiency of Nerium oleander, Pergularia tomentosa and Populus tremula seed fibers. Their cellulose contents were 45%, 43.8% and 60%. Their lignin amounts were 21%, 8.6% and 12%, respectively. Fourier Transform InfraRed suggested that th ...
- DOI:
- 10.1016/j.ijbiomac.2018.10.070
- https://dx.doi.org/10.1016/j.ijbiomac.2018.10.070
- Author:
- He, Hong; An, Fengping; Teng, Hui; Huang, Qun; Song, Hongbo
- Source:
- International journal of food science & technology 2019 v.54 no.1 pp. 170-182
- ISSN:
- 0950-5423
- Subject:
- Fourier transform infrared spectroscopy; Raman spectroscopy; X-ray diffraction; agar; ions; iron; iron deficiency anemia; nuclear magnetic resonance spectroscopy; nutrient deficiencies; oligosaccharides; pH; sugar content; temperature
- Abstract:
- ... This study aimed to synthesise a complex of agar oligosaccharides (AOS) with ferric iron and to evaluate its physicochemical and structural characteristics. Based on single factor, Plackett–Burman and response surface optimal experiments of three factors at three levels, the optimised chelate conditions of the AOS‐iron (III) complex were mass ratio of AOS to iron ions of 4.5:1 g:g, reaction temper ...
- DOI:
- 10.1111/ijfs.13921
- http://dx.doi.org/10.1111/ijfs.13921
- Author:
- Gurunathan, Padmalaya; Hari, Sivaram; Suseela, Sreeja Balakrishnapillai; Sankararajan, Radha; Mukannan, Arivanandan
- Source:
- Environmental science and pollution research international 2019 v.26 no.1 pp. 528-543
- ISSN:
- 0944-1344
- Subject:
- Fourier transform infrared spectroscopy; X-ray diffraction; adsorbents; adsorption; anions; aqueous solutions; cellulose acetate; chlorides; crystallites; fluorides; mass transfer; models; nanocomposites; nanoparticles; pH; pollutants; pollution control; scanning electron microscopy; selenium; sodium hydroxide; sulfates; surface area; temperature; water treatment; zeta potential; zinc oxide
- Abstract:
- ... In this study, ZnO functionalized cellulose acetate nanocomposite (ZnO/CA NC) was synthesized using a simple chemical approach found to have a high surface area of 657.34 m²/g and utilized as adsorbents for the removal of Se (VI) from aqueous solutions. Investigations on X-ray diffraction (XRD) revealed that ZnO nanocomposite has a smaller crystallite size compared to ZnO nanoparticles which facil ...
- DOI:
- 10.1007/s11356-018-3472-2
- http://dx.doi.org/10.1007/s11356-018-3472-2
- Author:
- Hu, Yan; Kou, Guangning; Chen, Qiyang; Li, Yan; Zhou, Zhiqin
- Source:
- Lebensmittel-Wissenschaft + [i.e. und] Technologie 2019 v.99 pp. 24-33
- ISSN:
- 0023-6438
- Subject:
- 2,2-diphenyl-1-picrylhydrazyl; Citrus reticulata; Fourier transform infrared spectroscopy; antioxidant activity; bioavailability; citrus peels; encapsulation; flavonoids; hydrophobic bonding; intestines; nanoparticles; pH; transmission electron microscopes; whey protein concentrate; China
- Abstract:
- ... Flavonoids rich in citrus peels have poor stability and bioavailability, which limits their commercial applications. In present study, citrus peel extracts were obtained from four citrus types and their stability and antioxidant activity were investigated in terms of pH conditions. Then, the extracts were encapsulated and protected by whey protein concentrate nanoparticles (WPC NPs). The results s ...
- DOI:
- 10.1016/j.lwt.2018.09.044
- https://dx.doi.org/10.1016/j.lwt.2018.09.044
- Author:
- Finger, Sebastian; Godoy, Félix A.; Wittwer, Geraldine; Aranda, Carlos P.; Calderón, Raúl; Miranda, Claudio D.
- Source:
- Journal of industrial microbiology & biotechnology 2019 v.46 no.1 pp. 101-111
- ISSN:
- 1367-5435
- Subject:
- Artemia; Fourier transform infrared spectroscopy; bacteria; color; culture media; high performance liquid chromatography; isomers; lakes; lethal dose 50; methanol; natural dyes; pH; resins; ribosomal RNA; sequence analysis; solubility; solvents; temperature; ultraviolet-visible spectroscopy; Chile
- Abstract:
- ... The interest in and demand for natural dyes has increased significantly in recent years; however, very few natural blue dyes are commercially available, because blue colored compounds in nature are relatively rare. In this study, a blue pigment-producing bacteria from Lake Chungará (Atacama Desert, Chile) was isolated, and its blue pigment was purified and chemically characterized. The pigment-pro ...
- DOI:
- 10.1007/s10295-018-2088-3
- http://dx.doi.org/10.1007/s10295-018-2088-3
- Author:
- Gao, Li-Yang; Deng, Jin-Huan; Huang, Guo-Fu; Li, Kai; Cai, Kun-Zheng; Liu, Yan; Huang, Fei
- Source:
- Bioresource technology 2019 v.272 pp. 114-122
- ISSN:
- 0960-8524
- Subject:
- Fourier transform infrared spectroscopy; X-ray diffraction; adsorption; aqueous solutions; biochar; cadmium; cation exchange; electrons; energy-dispersive X-ray analysis; pH; rice straw; scanning electron microscopy; sewage sludge; temperature; titration
- Abstract:
- ... Qualitative and quantitative characterization of Cd2+ adsorption mechanisms was performed with rice-straw and sewage-sludge biochars produced at different temperature (300–700 °C), respectively. The pH effect, adsorption kinetics and isotherms were investigated, and chemical analyses of Cd2+-loaded biochars were conducted by SEM-EDS, XRD, FTIR and Boehm titration. This demonstrated that rice-straw ...
- DOI:
- 10.1016/j.biortech.2018.09.138
- https://dx.doi.org/10.1016/j.biortech.2018.09.138
- Author:
- Krishna Mohan, G. V.; Naga Babu, A.; Kalpana, K.; Ravindhranath, K.
- Source:
- International journal of environmental science and technology 2019 v.16 no.1 pp. 101-112
- ISSN:
- 1735-1472
- Subject:
- Fourier transform infrared spectroscopy; X-ray diffraction; adsorbents; adsorption; chromium; endothermy; energy-dispersive X-ray analysis; ions; pH; scanning electron microscopy; sorption isotherms; temperature; thermodynamics; water pollution
- Abstract:
- ... An acid-treated adsorbent derived from spent coffee grounds is investigated for its adsorption toward chromium (VI) ions from polluted water by optimizing various physicochemical parameters such as pH, time of equilibration, initial concentration of Cr(VI), adsorbent dosage, temperature and interfering co-ions. 91.0% of removal is observed at optimum conditions, and the adsorption capacity is foun ...
- DOI:
- 10.1007/s13762-017-1593-7
- https://dx.doi.org/10.1007/s13762-017-1593-7
- Author:
- Mekhamer, Waffa; Al-Tamimi, Salma
- Source:
- Environmental science and pollution research international 2019 v.26 no.3 pp. 2297-2304
- ISSN:
- 0944-1344
- Subject:
- Fourier transform infrared spectroscopy; adsorbents; adsorption; aqueous solutions; batch systems; ciprofloxacin; equations; kinetics; pH; pomegranate peels; regression analysis; scanning electron microscopy; sorption isotherms; wastewater
- Abstract:
- ... The adsorption of Ciprofloxacin (CPX) from aqueous solution by Pomegranate peels (POP) was investigated in a batch process. The influence of time (5–60 min) and CPX concentration (100–10,000 mg/L) on the adsorption ability of POP was studied. The POP was characterized by FTIR, scanning electron microscopy (SEM), and Zeta sizer. The kinetic of adsorption was analyzed by the pseudo-first-order and t ...
- DOI:
- 10.1007/s11356-018-3639-x
- https://dx.doi.org/10.1007/s11356-018-3639-x
- Author:
- Li, Xinlong; Hiroyoshi, Naoki; Tabelin, Carlito Baltazar; Naruwa, Kosuke; Harada, Chie; Ito, Mayumi
- Source:
- Chemosphere 2019 v.214 pp. 70-78
- ISSN:
- 0045-6535
- Subject:
- Fourier transform infrared spectroscopy; acid mine drainage; aluminum; coal; coatings; dissolved oxygen; energy-dispersive X-ray analysis; finishes; ions; iron; iron oxyhydroxides; leachates; leaching; ligands; oxidation; pH; pyrite; scanning electron microscopy; silicon; thermodynamics; titanium
- Abstract:
- ... Pyrite, a common gangue mineral in complex sulfide ores and coals, is rapidly oxidized in water by ferric ions and dissolved oxygen to form a very acidic and heavy metal-laden leachate called acid mine drainage (AMD). Carrier-microencapsulation (CME) using Ti4+, Si4+, and Al3+ was reported as a promising new approach to prevent pyrite oxidation by forming a passivating barrier on the pyrite surfac ...
- DOI:
- 10.1016/j.chemosphere.2018.09.086
- https://dx.doi.org/10.1016/j.chemosphere.2018.09.086
- Author:
- Sahu, Uttam Kumar; Sahu, Sumanta; Mahapatra, Siba Sankar; Patel, Raj Kishore
- Source:
- Environmental science and pollution research international 2019 v.26 no.1 pp. 946-958
- ISSN:
- 0944-1344
- Subject:
- Aegle marmelos; Fourier transform infrared spectroscopy; X-ray diffraction; adsorbents; adsorption; ambient temperature; aqueous solutions; arsenic; electrostatic interactions; endothermy; ions; leaves; ligands; magnetism; models; moieties; nanocomposites; nanoparticles; pH; pyrolysis; scanning electron microscopy; sodium hydroxide; sorption isotherms; thermodynamics; transmission electron microscopy; trees; wastewater; zeta potential
- Abstract:
- ... A novel magnetic bio-adsorbent was prepared from the leaves of Aegle marmelos tree (Indian bael) and Fe₂O₃ nanoparticles. The AMP@Fe₂O₃ nanocomposite (Aegle marmelos leaf powder) was synthesized by pyrolysis process and applied for As(V) removal through batch adsorption process. The synthesized AMP@Fe₂O₃ nanocomposite was analyzed by several instrumental techniques like XRD, FESEM, TEM, HRTEM, FTI ...
- DOI:
- 10.1007/s11356-018-3643-1
- http://dx.doi.org/10.1007/s11356-018-3643-1
- Author:
- Hosseinzadeh, Soleyman; Hosseinzadeh, Hossein; Pashaei, Shahryar; Khodaparast, Zahra
- Source:
- International journal of biological macromolecules 2019 v.121 pp. 677-685
- ISSN:
- 0141-8130
- Subject:
- Fourier transform infrared spectroscopy; X-ray diffraction; acrylamides; acrylic acid; chitosan; copolymerization; doxorubicin; drug carriers; hydrogels; iron oxides; magnetism; nanocomposites; nanoparticles; pH; scanning electron microscopy; temperature; transmission electron microscopy
- Abstract:
- ... In this study, a unique stimuli-responsive hydrogel nanocomposite was prepared via surface reversible addition fragmentation chain transfer (RAFT) copolymerization of acrylic acid and N‑isopropyl acrylamide onto chitosan and subsequent in situ synthesis of magnetic Fe3O4 nanoparticles. In the next age, the structure and morphology of synthetic magnetic nanocomposite were characterized by FTIR, XRD ...
- DOI:
- 10.1016/j.ijbiomac.2018.10.106
- https://dx.doi.org/10.1016/j.ijbiomac.2018.10.106
- Author:
- Çelebi, H.
- Source:
- International journal of environmental science and technology 2019 v.16 no.1 pp. 135-146
- ISSN:
- 1735-1472
- Subject:
- Fourier transform infrared spectroscopy; Gibbs free energy; adsorbents; adsorption; aqueous solutions; dyes; egg shell; energy-dispersive X-ray analysis; enthalpy; entropy; heat production; hulls; models; pH; pumpkins; scanning electron microscopy; sorption isotherms; temperature; wastes
- Abstract:
- ... In this study, it is proposed that pumpkin seed hulls and eggshells that are household wastes are low-cost materials to remove the Reactive Black 5 from water media. Through a number of experiments, the influences of the contact time, adsorption quantity, temperature, and pH of the solution were studied. Characterization of pumpkin seed hulls and eggshells was done by using Fourier transform infra ...
- DOI:
- 10.1007/s13762-018-1969-3
- https://dx.doi.org/10.1007/s13762-018-1969-3
- Author:
- Pawar, Vaishali; Dhanka, Mukesh; Srivastava, Rohit
- Source:
- Colloids and surfaces 2019 v.173 pp. 776-787
- ISSN:
- 0927-7765
- Subject:
- Fourier transform infrared spectroscopy; antibacterial properties; biocompatibility; buffers; cefuroxime; cell lines; cell viability; chemical bonding; chitosan; colloids; drug delivery systems; drugs; esterases; fibroblasts; hemolysis; hydrogels; hydrolysis; osteosarcoma; pH; phosphates; polymers
- Abstract:
- ... Hydrogels are excellent drug delivery systems for the treatment of chronic wound infections. However, the problem of high burst release still remains a challenge that needs to be tackled. In terms of antibiotic release from the hydrogels, as the drug payload depletes it could act as a substrate for bacterial seeding which can create a life-threatening condition. Therefore, to provide the sustained ...
- DOI:
- 10.1016/j.colsurfb.2018.10.034
- https://dx.doi.org/10.1016/j.colsurfb.2018.10.034
- Author:
- Pietraszek, Aneta; Karewicz, Anna; Widnic, Marta; Lachowicz, Dorota; Gajewska, Marta; Bernasik, Andrzej; Nowakowska, Maria
- Source:
- Colloids and surfaces 2019 v.173 pp. 1-8
- ISSN:
- 0927-7765
- Subject:
- Fourier transform infrared spectroscopy; X-ray diffraction; alkaline phosphatase; aluminum oxide; bioactive compounds; bones; calcium hydroxide; colloids; encapsulation; energy-dispersive X-ray analysis; enzyme activity; halloysite; heat; hydroxyapatite; nanocomposites; nanotubes; pH; scanning electron microscopy; thermal stability; tissue engineering
- Abstract:
- ... Alkaline phosphatase (ALP) was sucessfully incorporated into the halloysite (HAL) nanotubes, as confirmed by FTIR-ATR and XRD analyses. The loading efficiency (LE) of ALP was found to be 13.5%, while its encapsulation efficiency (EE) was estimated to be around 27%, as determined using the Bradford test. The influence of the immobilization in HAL on the enzyme activity was measured using standard A ...
- DOI:
- 10.1016/j.colsurfb.2018.09.040
- https://dx.doi.org/10.1016/j.colsurfb.2018.09.040
- Author:
- Yang, Li; Song, Yonghai; Zeng, Mulan; Du, Yue; Peng, Bingxian; Huang, Zhenzhong; Wang, Li
- Source:
- Talanta 2019 v.191 pp. 74-80
- ISSN:
- 0039-9140
- Subject:
- Fourier transform infrared spectroscopy; buffers; coordination polymers; luminescence; nanoparticles; pH; scanning electron microscopy; silica; superoxide anion; transmission electron microscopy; zeta potential
- Abstract:
- ... It is of great significance for superoxide anion (O2•⁻) detection due to its important role in regulation of biological function. The nanoscale coordination polymers (NCPs) core-shell nanostructures have attracted increasing interests for their nanosized-dependent properties. In this study, SiO2@Tb/guanosine 5′-monophosphate (GMP) NCPs with core-shell nanostructures was designed for O2•⁻ detection ...
- DOI:
- 10.1016/j.talanta.2018.08.041
- https://dx.doi.org/10.1016/j.talanta.2018.08.041
- Author:
- Hu, Yongxing; Cai, Tianpei; Zhang, Haijuan; Chen, Jia; Li, Zuguang; Qiu, Hongdeng
- Source:
- Talanta 2019 v.191 pp. 265-271
- ISSN:
- 0039-9140
- Subject:
- Fourier transform infrared spectroscopy; acetonitrile; amino acids; ginsenosides; hydrophilic interaction chromatography; hydrophilicity; nucleobases; nucleosides; pH; polar compounds; polyacrylic acid; salt concentration; scanning electron microscopy; silica; solvents; temperature
- Abstract:
- ... In this study, a new stationary phase based on poly(itaconic acid)-grafted silica (Sil-PIA) were synthesized in deep eutectic solvents (DESs) and characterized in detail. Itaconic acid was homopolymerized on silica via surface radical chain-transfer reaction using DESs as a new kind of green solvents. Sil-PIA were obtained and characterized by Fourier transform infrared spectroscopy, elemental ana ...
- DOI:
- 10.1016/j.talanta.2018.08.072
- https://dx.doi.org/10.1016/j.talanta.2018.08.072
- Author:
- Zhou, Yaoyu; He, Yangzhuo; Xiang, Yujia; Meng, Sijun; Liu, Xiaocheng; Yu, Jiangfang; Yang, Jian; Zhang, Jiachao; Qin, Pufeng; Luo, Lin
- Source:
- The Science of the total environment 2019 v.646 pp. 29-36
- ISSN:
- 0048-9697
- Subject:
- Fourier transform infrared spectroscopy; X-ray photoelectron spectroscopy; adsorption; aquatic environment; aqueous solutions; carbon nanotubes; copper; copper nanoparticles; electrostatic interactions; ions; models; oxidation; pH; scanning electron microscopy; sorption isotherms; thermodynamics; transmission electron microscopy; zeta potential
- Abstract:
- ... In this study, the oxidized multiwalled carbon nanotube (O-MWCNTs) was obtained by a simple method, and investigated by various techniques (SEM, TEM, FT-IR, XPS and zeta potential) for the removal of pefloxacin and Cu(II). The mutual effects of their adsorption onto O-MWCNTs were comprehensively clarified with sole and binary systems with adsorption kinetics, sorption thermodynamic and sorption is ...
- DOI:
- 10.1016/j.scitotenv.2018.07.267
- https://dx.doi.org/10.1016/j.scitotenv.2018.07.267
- Author:
- Rasool, Atta; Ata, Sadia; Islam, Atif
- Source:
- Carbohydrate polymers 2019 v.203 pp. 423-429
- ISSN:
- 0144-8617
- Subject:
- Escherichia coli; Fourier transform infrared spectroscopy; antibacterial properties; antibiotics; biocompatibility; biodegradation; biopolymers; chitosan; drugs; hydrogels; moieties; pH; phosphates; silver; sulfadiazine; thermal analysis; tissue repair
- Abstract:
- ... Stimuli responsive chitosan (CS) and poly (N-vinyl-2-pyrrolidone) (PVP) have attained hydrogel properties in the presence of 74% neutralized poly acrylic acid (PAA) which can be exploited for wound healing applications. The FTIR spectra confirmed the presence of all specific functional groups and the developed interactions in the hydrogels. The thermal analysis explained that the hydrogel samples ...
- DOI:
- 10.1016/j.carbpol.2018.09.083
- https://dx.doi.org/10.1016/j.carbpol.2018.09.083
- Author:
- Shehzad, Khurram; Ahmad, Mukhtar; He, Junyong; Liu, Tao; Xu, Weihong; Liu, Jinhuai
- Source:
- Journal of colloid and interface science 2019 v.533 pp. 588-597
- ISSN:
- 0021-9797
- Subject:
- Fourier transform infrared spectroscopy; World Health Organization; X-ray photoelectron spectroscopy; adsorbents; adsorption; aqueous solutions; arsenic; arsenites; binding capacity; drinking water; graphene oxide; humans; ions; moieties; nanosheets; pH; surface area; water pollution; water treatment; zeta potential; zirconium oxide
- Abstract:
- ... Consumption of water having excessive arsenic (As) contamination can cause adverse health effects on human beings. In this study, novel ultra-large zirconium oxide (ZrO2) nanosheets were successfully synthesized using graphene oxide (GO) templates and their adsorption-ability was studied for arsenite (As(III)). Owing to higher values of surface area, numbers of available hydroxyl groups and strong ...
- DOI:
- 10.1016/j.jcis.2018.08.079
- http://dx.doi.org/10.1016/j.jcis.2018.08.079
- Author:
- Rehman, Rabia; Farooq, Siddra; Mahmud, Tariq
- Source:
- Journal of cleaner production 2019 v.206 pp. 819-826
- ISSN:
- 0959-6526
- Subject:
- Fourier transform infrared spectroscopy; Musa acuminata; Solanum tuberosum; adsorption; biosorbents; dyes; kinetics; moieties; pH; porosity; scanning electron microscopy; streams; temperature; wastewater
- Abstract:
- ... In this work, the efficiency of Musa acuminata and Solanum tuberosum peels was evaluated and compared for removal of Emerald green dye from water in batch mode. Optimized conditions of temperature, pH and biosorbent dosage were used for isothermal and kinetic investigations; which revealed that more Emerald green dye was adsorbed by Musa acuminata peels (qm (maximum adsorption capacity) = 10.75 mg ...
- DOI:
- 10.1016/j.jclepro.2018.09.226
- https://dx.doi.org/10.1016/j.jclepro.2018.09.226
- Author:
- Patil, Chandrashekhar S.; Gunjal, Datta B.; Naik, Vaibhav M.; Harale, Namdev S.; Jagadale, Suryabala D.; Kadam, Abhijit N.; Patil, Pramod S.; Kolekar, Govind B.; Gore, Anil H.
- Source:
- Journal of cleaner production 2019 v.206 pp. 407-418
- ISSN:
- 0959-6526
- Subject:
- Fourier transform infrared spectroscopy; adsorbents; adsorption; cost effectiveness; drugs; hospitals; kitchen waste; models; pH; pollutants; remediation; rivers; scanning electron microscopy; surveys; tea; wastewater; wastewater treatment; water pollution
- Abstract:
- ... Herein, we introduced simple, cheap, cost-effective and sustainable kitchen waste tea residue as an adsorbent. As per the literature survey, all the adsorbents have been used for wastewater treatment only as activated form. The first time, we have used similar material without any complicated activation process for the removal of pharmaceutical pollutant and it shows superior results than the exis ...
- DOI:
- 10.1016/j.jclepro.2018.09.140
- https://dx.doi.org/10.1016/j.jclepro.2018.09.140
- Author:
- Bary, E. M. Abdel; Fekri, Ahmed; Soliman, Yaser A.; Harmal, Ammar N.
- Source:
- TheInternational journal of environmental studies 2019 v.76 no.1 pp. 118-135
- ISSN:
- 1029-0400
- Subject:
- Bacillus subtilis; Candida albicans; Fourier transform infrared spectroscopy; Pectobacterium carotovorum; Proteus vulgaris; Staphylococcus aureus; absorbents; antimicrobial properties; biodegradability; cellulose; chemical treatment; crosslinking; differential scanning calorimetry; fungi; glutaraldehyde; glycerol; hydrogels; mechanical testing; nanocrystals; pH; polyvinyl alcohol; rice hulls; scanning electron microscopy; swelling (materials); virulent strains; water reservoirs
- Abstract:
- ... Novel superabsorbent membranes (SMs) consisting of polyvinyl alcohol (PVA), cellulose nanocrystals (CNCs) originated from rice husk (RH), glutaraldehyde (GLA) and glycerine (G) were manufactured by a compression moulding process. RHs were used to isolate pure CNCs via mechanical and chemical treatments. RHs were used to improve water-retention. Glycerine was used to increase the elasticity of the ...
- DOI:
- 10.1080/00207233.2018.1496607
- http://dx.doi.org/10.1080/00207233.2018.1496607
56. Functionalized biochar-supported magnetic MnFe₂O₄ nanocomposite for the removal of Pb(ii) and Cd(ii)
- Author:
- Zhang, Lianke; Guo, Jinyue; Huang, Xuemin; Wang, Weida; Sun, Peng; Li, Yumei; Han, Jianhong
- Source:
- RSC advances 2019 v.9 no.1 pp. 365-376
- ISSN:
- 2046-2069
- Subject:
- Fourier transform infrared spectroscopy; X-ray diffraction; X-ray photoelectron spectroscopy; adsorbents; adsorption; biochar; cadmium; corn straw; egg albumen; energy-dispersive X-ray analysis; heat production; ion exchange; kinetics; lead; magnetism; models; moieties; nanocomposites; pH; scanning electron microscopy; surface area; wastewater
- Abstract:
- ... In this study, a novel magnetic biochar-MnFe₂O₄ nanocomposite (BC/FM) was prepared using low-cost corn straw and MnFe₂O₄ by sol–gel/pyrolyzing route using egg white, which has abundant functional groups (–NH₂ and –COOH). Following that, its composition, morphology and structure was characterized by various techniques including SEM-EDX, BET, XRD, and VSM. Batch experiment of the adsorption for Pb(i ...
- DOI:
- 10.1039/c8ra09061k
- http://dx.doi.org/10.1039/c8ra09061k
- Author:
- Dutta, Raj Kumar; Shaida, Md. Azfar; Singla, Kirti; Das, Dipika
- Source:
- Journal of materials chemistry A 2019 v.7 no.2 pp. 664-678
- ISSN:
- 2050-7496
- Subject:
- Fourier transform infrared spectroscopy; Raman spectroscopy; X-ray photoelectron spectroscopy; adenosine monophosphate; adsorbents; adsorption; aluminum; cadmium; carboxylic acids; cations; chelation; chemical reduction; cobalt; copper; endothermy; energy-dispersive X-ray analysis; graphene oxide; iron; kinetics; lead; manganese; mercury; nickel; nitrogen; oxygen; pH; phosphates; scanning electron microscopy; sorption isotherms; surface area; thermodynamics; uranyl ions; zeta potential; zinc
- Abstract:
- ... Graphene oxide reduced by adenosine 5′-monophosphate (RGO-AMP) has been developed as a smart nanoscale adsorbent for unprecedented high removal of uranyl ions from aqueous medium. The amine/amide and phosphate groups of AMP are grafted in the graphene oxide structure by reducing the carboxylic acid groups of GO to facilitate a stronger affinity for interaction with uranyl ions. An array of charact ...
- DOI:
- 10.1039/c8ta09746a
- http://dx.doi.org/10.1039/c8ta09746a
- Author:
- Abdel Bary, E. M.; Fekri, Ahmed; Soliman, Yaser A.; Harmal, Ammar N.
- Source:
- TheInternational journal of environmental studies 2019 v.76 no.1 pp. 150-167
- ISSN:
- 1029-0400
- Subject:
- Bacillus subtilis; Candida albicans; Fourier transform infrared spectroscopy; Pectobacterium carotovorum; Proteus vulgaris; Staphylococcus aureus; absorbents; antimicrobial properties; biodegradability; cellulose; chemical treatment; crosslinking; differential scanning calorimetry; fungi; glutaraldehyde; glycerol; horticulture; manufacturing; mechanical testing; nanocrystals; pH; polyvinyl alcohol; rice hulls; scanning electron microscopy; silica; swelling (materials); virulent strains; water reservoirs
- Abstract:
- ... Novel superabsorbent membranes (SMs) consisting of polyvinyl alcohol (PVA), cellulose nanocrystals (CNCs) originated from rice husk (RH), nanosilica, glutaraldehyde and glycerine (G) were manufactured by a compression moulding process. RHs were used to isolate pure CNCs via mechanical and chemical treatments. RHs were used to improve water retention. These SMs were characterised by Fourier-transfo ...
- DOI:
- 10.1080/00207233.2018.1550966
- http://dx.doi.org/10.1080/00207233.2018.1550966
- Author:
- Jiang, Hong-Liu; Lin, Jie-Ci; Hai, Wei; Tan, Hong-Wei; Luo, Yu-Wei; Xie, Xiao-Lin; Cao, Yao; He, Fu-An
- Source:
- Colloids and surfaces 2019 v.560 pp. 59-68
- ISSN:
- 0927-7757
- Subject:
- Fourier transform infrared spectroscopy; absorption; adsorbents; adsorption; aqueous solutions; carbon; carboxylic acids; colloids; crosslinking; electrostatic interactions; methylene blue; nuclear magnetic resonance spectroscopy; pH; polymers; scanning electron microscopy; sorption isotherms; stable isotopes; thermogravimetry
- Abstract:
- ... In this work, a novel crosslinked porous β-cyclodextrin-based polymer containing carboxylic acid groups (CT-β-CD) was synthesized successfully and characterized by SEM, FTIR, 13C solid-state NMR, water-contact-angle measurement, and TGA. The resultant CT-β-CD with triple absorption effects including inclusion complextion, porous network capture, and electrostatic interaction was employed as an ads ...
- DOI:
- 10.1016/j.colsurfa.2018.10.004
- https://dx.doi.org/10.1016/j.colsurfa.2018.10.004
60. A novel magnetic MIL-101(Fe)/TiO2 composite for photo degradation of tetracycline under solar light
- Author:
- He, Lei; Dong, Yanan; Zheng, Yane; Jia, Qingming; Shan, Shaoyun; Zhang, Yaqin
- Source:
- Journal of hazardous materials 2019 v.361 pp. 85-94
- ISSN:
- 0304-3894
- Subject:
- Fourier transform infrared spectroscopy; X-ray diffraction; X-ray photoelectron spectroscopy; coordination polymers; energy-dispersive X-ray analysis; free radicals; hydroxyl radicals; iron; irradiation; magnetic materials; magnetism; pH; photolysis; scanning electron microscopy; solar radiation; superoxide anion; tetracycline; thermogravimetry; titanium dioxide; transmission electron microscopy; ultraviolet radiation; wastewater
- Abstract:
- ... A novel magnetic MIL-101(Fe)/TiO2 composite was synthesized for photo degradation of tetracycline (TC) under solar light. The composite was characterized by XRD, TGA, SEM, TEM, EDS, BET, FTIR, XPS, VSM, ESR, and PL. The resultant composite was environment friendly material, which exhibited high TC degradation efficiency and excellent reusability. In the meantime, it could be separated easily from ...
- DOI:
- 10.1016/j.jhazmat.2018.08.079
- http://dx.doi.org/10.1016/j.jhazmat.2018.08.079
- Author:
- Najafian, Hassan; Manteghi, Faranak; Beshkar, Farshad; Salavati-Niasari, Masoud
- Source:
- Journal of hazardous materials 2019 v.361 pp. 210-220
- ISSN:
- 0304-3894
- Subject:
- Fourier transform infrared spectroscopy; X-ray diffraction; acids; azo dyes; bismuth; copper; elemental composition; energy-dispersive X-ray analysis; free radicals; gelation; gelling agents; irradiation; light; nanocomposites; nanomaterials; pH; particle size distribution; photocatalysis; photocatalysts; photolysis; pollutants; pollution control; scanning electron microscopy; sol-gel processing; superoxide anion; transmission electron microscopy; ultraviolet-visible spectroscopy
- Abstract:
- ... In the present study, CuBi2O4/Bi3ClO4 nanocomposites have been fabricated via an improved Pechini sol-gel process using the mixtures of various gelling agents and polybasic acids. This work shows that by controlling the reaction conditions such as kind of polybasic acids, gelling agents, pH and mole ratio of polybasic acid to total metals, the CuBi2O4/Bi3ClO4 nanocomposites with ultrafine sphere-l ...
- DOI:
- 10.1016/j.jhazmat.2018.08.092
- http://dx.doi.org/10.1016/j.jhazmat.2018.08.092
- Author:
- Lu, Jiwei; Sun, Mingjun; Yuan, Zhitao; Qi, Shengliang; Tong, Zhongyun; Li, Lixia; Meng, Qingyou
- Source:
- Colloids and surfaces 2019 v.560 pp. 35-41
- ISSN:
- 0927-7757
- Subject:
- Fourier transform infrared spectroscopy; adsorption; colloids; dispersants; electrostatic interactions; ions; magnesium; magnesium silicates; molecular dynamics; pH; serpentine; silicon; sodium; zeta potential
- Abstract:
- ... Serpentine, as a common magnesium silicate mineral found in many ores around the world, is usually dispersed/depressed with the dispersants/depressants by adsorbing on the surface of serpentine. Therefore, in this work, the interaction mechanism of the dispersant of sodium hexametaphosphate (SHMP) was investigated in detail though solution chemistry calculations, Fourier transform infrared spectro ...
- DOI:
- 10.1016/j.colsurfa.2018.09.076
- https://dx.doi.org/10.1016/j.colsurfa.2018.09.076
- Author:
- Li, Jian-Rong; Wang, Feng-Kang; Xiao, Hang; Xu, Lei; Fu, Ming-Lai
- Source:
- Colloids and surfaces 2019 v.560 pp. 306-314
- ISSN:
- 0927-7757
- Subject:
- Fourier transform infrared spectroscopy; X-ray diffraction; X-ray photoelectron spectroscopy; adsorption; calcium; colloids; hydrochloric acid; ion exchange; kinetics; lanthanum; magnesium; pH; phosphates; potassium hydroxide; scanning electron microscopy; sewage; surface area; zeta potential
- Abstract:
- ... The layered chalcogenide KMS-1 was modified by La/Ca/Mg via a simple ion exchange process for the removal of phosphate from water. La-modified KMS-1 (KLa), Ca-modified KMS-1 (KCa) and Mg-modified KMS-1 (KMg) were comparatively characterized using X-ray diffraction, BET surface area, zeta potential and scanning electron microscopy, respectively. It was found that the adsorption capacity of KLa was ...
- DOI:
- 10.1016/j.colsurfa.2018.10.026
- https://dx.doi.org/10.1016/j.colsurfa.2018.10.026
64. Polycarboxylic magnetic polydopamine sub-microspheres for effective adsorption of malachite green
- Author:
- Pan, Xihao; Zuo, Gancheng; Su, Ting; Cheng, Siyao; Gu, Yufan; Qi, Xiaoliang; Dong, Wei
- Source:
- Colloids and surfaces 2019 v.560 pp. 106-113
- ISSN:
- 0927-7757
- Subject:
- Fourier transform infrared spectroscopy; adsorbents; adsorption; chemical structure; coatings; colloids; iron oxides; kinetics; magnetism; malachite green; models; nanocrystals; pH; particle size distribution; sorption isotherms; transmission electron microscopy
- Abstract:
- ... Magnetic particle is a promising class of materials to absorb harmful contaminants for their easy collecting property with magnetic response. Here, we report a novel kind of polycarboxylic magnetic polydopamine sub-microspheres (Fe3O4@PDA-COOH) facilely synthesized by coating polydopamine (PDA) onto the surface of magnetic nanocrystal clusters (Fe3O4). Then the sub-microspheres were modified with ...
- DOI:
- 10.1016/j.colsurfa.2018.10.014
- http://dx.doi.org/10.1016/j.colsurfa.2018.10.014
- Author:
- Wang, Xudong; Chen, Zhangjun; Li, Ke; Wei, Xiaodong; Chen, Zhenbin; Ruso, Juan M.; Tang, Zhenghua; Liu, Zhen
- Source:
- Colloids and surfaces 2019 v.560 pp. 298-305
- ISSN:
- 0927-7757
- Subject:
- Fourier transform infrared spectroscopy; colloids; enzyme activity; ethanol; glutaraldehyde; pH; particle size; penicillin amidase; temperature; titanium dioxide; ultraviolet-visible spectroscopy
- Abstract:
- ... In this work, titanium dioxide particle was firstly modified with glutaraldehyde, and modification conditions, i.e. particle size (d), active temperature (Ta), modification temperature (Tm), modification time (tm), pH value, aldehyde ethanol ratio (Ra) and ethanol ratio (Re), were studied and optimized adopting grafting rate (Gr) as the optimizing index, the ultraviolet-visible spectrophotometry a ...
- DOI:
- 10.1016/j.colsurfa.2018.10.001
- https://dx.doi.org/10.1016/j.colsurfa.2018.10.001
- Author:
- Xu, Zixuan; Zhao, Yonglu; Wang, Peiyu; Yan, Xinqi; Cai, Miaomiao; Yang, Ying
- Source:
- Industrial & engineering chemistry process design and development 2019 v.58 no.5 pp. 1779-1786
- ISSN:
- 1520-5045
- Subject:
- Fourier transform infrared spectroscopy; cadmium; chromium; cobalt; copper; ionic liquids; manganese; metal ions; nickel; pH; palladium; platinum; polymers; process design; scanning electron microscopy; temperature; thiourea
- Abstract:
- ... As an excellent separation material to recover platinum group metals (PGMs), imidazolium-based task-specific polymeric ionic liquid (CP-AMIN) was successfully synthesized and characterized by SEM and FT-IR. The effects of temperature, pH, reaction time, CP-AMIN amount, and concentration of chloride ion were discussed during the process of extraction of Pt(IV), Pt(II), and Pd(II) from acidic chlori ...
- DOI:
- 10.1021/acs.iecr.8b03408
- http://dx.doi.org/10.1021/acs.iecr.8b03408
- Author:
- Zbair, Mohamed; Anfar, Zakaria; Ait Ahsaine, Hassan; Khallok, Hamza
- Source:
- RSC advances 2019 v.9 no.2 pp. 1084-1094
- ISSN:
- 2046-2069
- Subject:
- Fourier transform infrared spectroscopy; Raman spectroscopy; X-ray photoelectron spectroscopy; Ziziphus; adsorbents; adsorption; aqueous solutions; cost analysis; energy; models; nitrogen; pH; paraquat; response surface methodology; scanning electron microscopy; thermogravimetry
- Abstract:
- ... This paper reports the removal of paraquat from an aqueous solution using prepared carbonated jujube seed (JS/HSO-700). JS/HSO-700 was characterized by XPS, TGA, FTIR, N₂ physisorption, SEM, and Raman techniques. FTIR revealed the presence of active species on the JS/HSO-700 surface. The removal rate of paraquat was investigated as a function of multiple operational factors such as contact time, a ...
- DOI:
- 10.1039/c8ra09337g
- http://dx.doi.org/10.1039/c8ra09337g
- Author:
- Eskandari, Parisa; Farhadian, Mehrdad; Solaimany Nazar, Ali Reza; Jeon, Byong-Hun
- Source:
- Industrial & engineering chemistry process design and development 2019 v.58 no.5 pp. 2099-2112
- ISSN:
- 1520-5045
- Subject:
- Fourier transform infrared spectroscopy; X-ray diffraction; X-ray fluorescence spectroscopy; activated carbon; adsorption; cyanides; energy-dispersive X-ray analysis; irradiation; models; nanomaterials; pH; photocatalysis; photocatalysts; photolysis; prediction; process design; response surface methodology; scanning electron microscopy; transmission electron microscopy; zeolites
- Abstract:
- ... The synthesized TiO₂/Fe₂O₃ nanostructures supported on powder-activated carbon (PAC) and zeolite at different mole ratios of Fe³⁺/TiO₂ were characterized by XRD, XRF, FESEM, EDX, TEM, FTIR, BET, and, PL analyses and their cyanide photodegradation mechanism was thoroughly discussed. The results confirmed not only TiO₂/Fe₂O₃/PAC had higher photocatalytic and adsorption capability but also better str ...
- DOI:
- 10.1021/acs.iecr.8b05073
- http://dx.doi.org/10.1021/acs.iecr.8b05073
- Author:
- Su, Mei; Fang, Yili; Li, Bing; Yin, Weizhao; Gu, Jingjing; Liang, Hao; Li, Ping; Wu, Jinhua
- Source:
- The Science of the total environment 2019 v.647 pp. 47-56
- ISSN:
- 0048-9697
- Subject:
- Fourier transform infrared spectroscopy; X-ray diffraction; X-ray photoelectron spectroscopy; activated carbon; adsorption; aqueous solutions; chromium; cost effectiveness; goethite; hydrochloric acid; hydroxides; iron oxyhydroxides; models; pH; scanning electron microscopes; scanning electron microscopy; water treatment
- Abstract:
- ... In this study, activated carbon (AC) was modified with micro-sized geothite (mFeOOH) using a facile and cost-effective impregnation method for enhanced Cr(VI) removal from aqueous solutions. X-ray diffraction (XRD) and scanning electron microscope (SEM) analysis showed that FeOOH particles with a diameter of 0.1–1 μm were dispersed homogeneously on the surfaces and pores of the AC. Fourier transfo ...
- DOI:
- 10.1016/j.scitotenv.2018.07.372
- https://dx.doi.org/10.1016/j.scitotenv.2018.07.372
- Author:
- Vyavahare, Govind; Jadhav, Pooja; Jadhav, Jyoti; Patil, Ravishankar; Aware, Chetan; Patil, Devashree; Gophane, Anna; Yang, Yung-Hun; Gurav, Ranjit
- Source:
- Journal of cleaner production 2019 v.207 pp. 296-305
- ISSN:
- 0959-6526
- Subject:
- Fourier transform infrared spectroscopy; Mangifera indica; X-ray diffraction; analysis of variance; atomic absorption spectrometry; biochar; biomass; experimental design; fabrics; fish; gentian violet; gills; histology; leaves; mangoes; models; pH; response surface methodology; scanning electron microscopy; seed germination; sorption; temperature; total organic carbon; toxicity; wastewater
- Abstract:
- ... The present study aimed to determine the sorption behaviour of crystal violet (CV) dye on mango leaves biochar (MLBC) prepared at 400 °C, 600 °C and 800 °C. Response surface methodology (RSM) was executed to evaluate the interactive effect of four process variables on the sorption of CV dye using Box-Behnken design. The quadratic model showed significance of model for the responses which were vali ...
- DOI:
- 10.1016/j.jclepro.2018.09.193
- https://dx.doi.org/10.1016/j.jclepro.2018.09.193
- Author:
- Alharthi, Sarah; El Rassi, Ziad
- Source:
- Talanta 2019 v.192 pp. 534-544
- ISSN:
- 0039-9140
- Subject:
- Fourier transform infrared spectroscopy; Raman spectroscopy; acids; aniline; capillary electrophoresis; carbon nanotubes; carboxylation; chromatography; coatings; electrolytes; hydroxylation; nanoparticles; nucleobases; nucleosides; pH; sodium dodecyl sulfate; solutes
- Abstract:
- ... In this study, multi-walled carbon nanotubes (MWCNTs) in either unmodified, hydroxylated (MWCNT-OH), carboxylated (MWCNT-COOH) or sulfonated (MWCNT-SO3H) forms were incorporated into the running electrolytes in capillary electrophoresis (CE) to play the role of pseudo-stationary phases (PSPs) and perform nanoparticle electrokinetic capillary chromatography (NPEKC). MWCNT-COOH and MWCNT-SO3H were d ...
- DOI:
- 10.1016/j.talanta.2018.09.045
- https://dx.doi.org/10.1016/j.talanta.2018.09.045
- Author:
- Al-Amoudi, Rami H.; Taylan, Osman; Kutlu, Gozde; Can, Asli Muslu; Sagdic, Osman; Dertli, Enes; Yilmaz, Mustafa Tahsin
- Source:
- Food chemistry 2019 v.271 pp. 650-662
- ISSN:
- 0308-8146
- Subject:
- Fourier transform infrared spectroscopy; Mespilus germanica; X-ray diffraction; arabinose; chemical structure; differential scanning calorimetry; endothermy; experimental design; fruits; fuzzy logic; galactose; glucose; heat production; nuclear magnetic resonance spectroscopy; pH; pectins; response surface methodology; rhamnose; thermogravimetry; viscoelasticity
- Abstract:
- ... In this work, response surface methodology and adaptive neuro-fuzzy inference system approaches were used to predict and model effect of extraction conditions of pectin from medlar fruit (Mespilus germanica L.). The pectin extracted at optimized conditions (89 °C, 4.83 h and 4.2 pH) could be classified as high methoxyl pectin. Sugar composition analysis showed that pectin was mainly composed of D- ...
- DOI:
- 10.1016/j.foodchem.2018.07.211
- https://dx.doi.org/10.1016/j.foodchem.2018.07.211
- Author:
- Campos, Alex Fabiano Cortez; de Oliveira, Helena Augusta Lisboa; da Silva, Fabiana Narciso; da Silva, Franciscarlos Gomes; Coppola, Priscilla; Aquino, Renata; Mezzi, Alessio; Depeyrot, Jerome
- Source:
- Journal of hazardous materials 2019 v.362 pp. 82-91
- ISSN:
- 0304-3894
- Subject:
- Fourier transform infrared spectroscopy; X-ray diffraction; X-ray photoelectron spectroscopy; adsorption; aqueous solutions; chromium; endothermy; ions; magnetism; models; nanoparticles; pH; pollutants; separation; sorbents; sorption isotherms; surface area; temperature; transmission electron microscopy; water pollution
- Abstract:
- ... Novel nanoadsorbents based on core-shell bimagnetic nanoparticles (CoFe2O4@ɣ-Fe2O3) with two different mean sizes were elaborated, characterized and applied as potential sorbents for Cr(VI) removal from aqueous solutions through magnetically assisted chemical separation. The nanoadsorbents were characterized by XRD, TEM, FTIR, XPS, potentiometric-conductometric titrations, BET and vibrating sample ...
- DOI:
- 10.1016/j.jhazmat.2018.09.008
- https://dx.doi.org/10.1016/j.jhazmat.2018.09.008
- Author:
- Zeng, Liang; Xiao, Ling; Shi, Xiaowen; Wei, Mingyu; Cao, Jinying; Long, Yangke
- Source:
- Journal of colloid and interface science 2019 v.534 pp. 586-594
- ISSN:
- 0021-9797
- Subject:
- Fourier transform infrared spectroscopy; X-ray diffraction; X-ray photoelectron spectroscopy; catalysts; catalytic activity; coatings; cobalt; electron paramagnetic resonance spectroscopy; inorganic salts; ions; leaching; nanoparticles; pH; remediation; rhodamines; scanning electron microscopy; temperature; thermogravimetry; transmission electron microscopy; water pollution
- Abstract:
- ... Herein, Prussian blue analogues@poly(m-phenylenediamine) nanoparticles (PBA@PmPDs) with well-defined core-shell structure were synthesized. The successful coating of poly(m-phenylenediamine) (PmPD) on the surface of FeyCo3-y [Co(CN)6]2 (Fe-Co-Co PBA) was confirmed by SEM, TEM, XRD, TGA, FT-IR and XPS. The catalytic performance of Fe-Co-Co PBA@PmPDs was evaluated by activation of peroxymonosulfate ...
- DOI:
- 10.1016/j.jcis.2018.09.074
- https://dx.doi.org/10.1016/j.jcis.2018.09.074
- Author:
- Ken, Bhupendra Singh; Nandi, Barun Kumar
- Source:
- Powder technology 2019 v.342 pp. 690-697
- ISSN:
- 0032-5910
- Subject:
- Fourier transform infrared spectroscopy; agitation; carbon; coal; desulfurization; hydrocarbons; hydrogen; linseed oil; minerals; oxygen; pH; particle size; powders; product quality; pulp; scanning electron microscopes; scanning electron microscopy; sulfur
- Abstract:
- ... This paper presents the results of experimental studies on desulfurization of high sulfur Indian coal by oil agglomeration using linseed oil. During experimental studies, various operating parameters like effect of pH, particle size, pulp density, agglomeration time, agitation rate and linseed oil dose were studied to find their impact on clean coal properties like sulfur reduction ratio (S/So), a ...
- DOI:
- 10.1016/j.powtec.2018.10.045
- https://dx.doi.org/10.1016/j.powtec.2018.10.045
- Author:
- Mohamed, Essam A.; Selim, Ali Q.; Zayed, Ahmed M.; Komarneni, Sridhar; Mobarak, Mohamed; Seliem, Moaaz K.
- Source:
- Journal of colloid and interface science 2019 v.534 pp. 408-419
- ISSN:
- 0021-9797
- Subject:
- Bacillariophyceae; Fourier transform infrared spectroscopy; X-ray diffraction; X-ray fluorescence spectroscopy; active sites; adsorbents; adsorption; diatomaceous earth; endothermy; light microscopy; methylene blue; models; pH; scanning electron microscopy; silica; sorption isotherms; temperature; thermodynamics
- Abstract:
- ... In the current study, calcination and thermo-chemical methods were applied in treatment of the processed diatomite fraction (<45 μm), which containing nearly 82.6 wt.% of the raw Egyptian diatomaceous earth. The untreated and modified diatomite fractions were characterized by optical microscopy (OM), X-ray fluorescence (XRF), X-ray diffraction (XRD), scanning electron microscopy (SEM) and Fourier ...
- DOI:
- 10.1016/j.jcis.2018.09.024
- https://dx.doi.org/10.1016/j.jcis.2018.09.024
- Author:
- Naeem, Hina; Ajmal, Muhammad; Qureshi, Raheela Beenish; Muntha, Sedra Tul; Farooq, Muhammad; Siddiq, Muhammad
- Source:
- Journal of environmental management 2019 v.230 pp. 199-211
- ISSN:
- 0301-4797
- Subject:
- Escherichia coli; Fourier transform infrared spectroscopy; Gram-negative bacteria; Gram-positive bacteria; Staphylococcus aureus; X-radiation; X-ray diffraction; adsorbents; adsorption; antibacterial properties; antibiotics; catalysts; catalytic activity; chemical reduction; decontamination; energy-dispersive X-ray analysis; graphene; ions; kinetics; malachite green; models; nanocomposites; nanosilver; nitroanilines; pH; pathogens; pollutants; scanning electron microscopy; silver; sorption isotherms; temperature; thermogravimetry; toxicity; transmission electron microscopy; wastewater
- Abstract:
- ... Here in, we presented a facile one-step method for the synthesis of Graphene oxide–silver (GO–Ag) nanocomposite and its applications as a sorbent for the elimination of some toxic pollutants from aqueous medium, as an efficient catalyst in the individual as well as simultaneous reduction reactions of multiple compounds, and as an antibacterial agent for the destruction of some harmful microorganis ...
- DOI:
- 10.1016/j.jenvman.2018.09.061
- http://dx.doi.org/10.1016/j.jenvman.2018.09.061
- Author:
- Guo, Zanru; Gu, Hongjian; Chen, Qiang; He, Zhanfeng; Xu, Wenyuan; Zhang, Jiali; Liu, Yongxin; Xiong, Leyan; Zheng, Longzhen; Feng, Yujun
- Source:
- Journal of colloid and interface science 2019 v.534 pp. 183-194
- ISSN:
- 0021-9797
- Subject:
- Fourier transform infrared spectroscopy; absorbents; absorption; adsorption; centrifugation; combustion; contact angle; desorption; ecosystems; emulsions; nitrogen; oils; pH; petroleum; polymerization; porous media; scanning electron microscopy; solvents; wettability
- Abstract:
- ... The effective separation and recovery of oils from water is important for the protections of ecosystems and the environment. Polymeric porous monoliths have been demonstrated as attractive absorbents for oil/water separation. However, the recyclability was mainly realized by squeezing, combustion, or centrifugation, which may restrict in elastic materials, destroy the adsorbates or need special ap ...
- DOI:
- 10.1016/j.jcis.2018.09.021
- https://dx.doi.org/10.1016/j.jcis.2018.09.021
- Author:
- Özdemir, Sadin; Mohamedsaid, Siham Abdullah; Kılınç, Ersin; Soylak, Mustafa
- Source:
- Food chemistry 2019 v.271 pp. 232-238
- ISSN:
- 0308-8146
- Subject:
- Fourier transform infrared spectroscopy; biosorption; biotechnology; cobalt; energy-dispersive X-ray analysis; ferric oxide; ions; maghemite; magnetism; mercury; nanoparticles; pH; scanning electron microscopy; sorbents
- Abstract:
- ... A new bio-MSPE sorbent based on the use of C. micaceus and γ-Fe2O3 magnetic nanoparticle was prepared for the preconcentrations of Co(II) and Hg(II). Critical parameters including pH, flow rate, quantity of C. micaceus, quantity of γ-Fe2O3 magnetic nanoparticle, eluent (type, concentration and volume), sample volume, and foreign ions were examined. Surface structure and variations after interactio ...
- DOI:
- 10.1016/j.foodchem.2018.07.067
- https://dx.doi.org/10.1016/j.foodchem.2018.07.067
- Author:
- Vaidya, Bhuvaneshwar; Shukla, Snehal K.; Kolluru, Srikanth; Huen, Melanie; Mulla, Nihal; Mehra, Neelesh; Kanabar, Dipti; Palakurthi, Srinath; Ayehunie, Seyoum; Muth, Aaron; Gupta, Vivek
- Source:
- Carbohydrate polymers 2019 v.204 pp. 68-77
- ISSN:
- 0144-8617
- Subject:
- Fourier transform infrared spectroscopy; P-glycoproteins; X-ray diffraction; beta-cyclodextrin; bioactive properties; collagen; differential scanning calorimetry; fibroblasts; intestines; lungs; molecular models; nuclear magnetic resonance spectroscopy; pH; permeability; solubility
- Abstract:
- ... Cyclodextrin complex of nintedanib was prepared aiming for increased bio-activity and improved transport across intestinal membrane with reduced p-glycoprotein (p-gp) efflux. Based on preliminary phase solubility studies and molecular modeling, sulfobutyl ether derivative of β-cyclodextrin (SBE-β-CD, Captisol®) was selected to prepare inclusion complex. Complexation was confirmed using FTIR, 1H NM ...
- DOI:
- 10.1016/j.carbpol.2018.09.080
- https://dx.doi.org/10.1016/j.carbpol.2018.09.080
- Author:
- Promphet, Nadtinan; Rattanawaleedirojn, Pranee; Siralertmukul, Krisana; Soatthiyanon, Niphaphun; Potiyaraj, Pranut; Thanawattano, Chusak; Hinestroza, Juan P.; Rodthongkum, Nadnudda
- Source:
- Talanta 2019 v.192 pp. 424-430
- ISSN:
- 0039-9140
- Subject:
- Fourier transform infrared spectroscopy; athletes; carboxymethylcellulose; cetyltrimethylammonium bromide; chitosan; color; colorimetry; cotton fabric; dyes; lactic acid; methyl orange; monitoring; pH; scanning electron microscopy; sports; sweat
- Abstract:
- ... A non-invasive textile-based colorimetric sensor for the simultaneous detection of sweat pH and lactate was created by depositing of three different layers onto a cotton fabric: 1.) chitosan, 2.) sodium carboxymethyl cellulose, and 3.) indicator dye or lactate assay. This sensor was characterized using field emission scanning electron microscopy and fourier transform infrared spectroscopy. Then, t ...
- DOI:
- 10.1016/j.talanta.2018.09.086
- https://dx.doi.org/10.1016/j.talanta.2018.09.086
- Author:
- Velusamy, Vijayalakshmi; Palanisamy, Selvakumar; Chen, Shih-Wei; Balu, Sridharan; Yang, Thomas C.K.; Banks, Craig E.
- Source:
- Talanta 2019 v.192 pp. 471-477
- ISSN:
- 0039-9140
- Subject:
- Fourier transform infrared spectroscopy; Raman spectroscopy; carbon electrodes; catalysts; cellulose; electrochemistry; electrosynthesis; fenitrothion; graphene; graphene oxide; pH; polymers; scanning electron microscopy
- Abstract:
- ... Over the past decades, the synthesis of carbohydrate polymers incorporated graphene or reduced graphene oxide has received greater attention in different disciplines owing to their unique physicochemical properties. In this context, we report a facile electrochemical synthesis of cellulose microfibers supported reduced graphene oxide and its application towards enhanced and lower potential electro ...
- DOI:
- 10.1016/j.talanta.2018.09.055
- https://dx.doi.org/10.1016/j.talanta.2018.09.055
- Author:
- Kazemi, Milad; Khodaiyan, Faramarz; Labbafi, Mohsen; Saeid Hosseini, Seyed; Hojjati, Mohammad
- Source:
- Food chemistry 2019 v.271 pp. 663-672
- ISSN:
- 0308-8146
- Subject:
- Fourier transform infrared spectroscopy; X-ray diffraction; arabinose; crystal structure; emulsifying; emulsifying properties; galactose; galacturonic acid; high performance liquid chromatography; irradiation; microwave treatment; molecular weight; nuclear magnetic resonance spectroscopy; pH; pectins; pistachios; rhamnose; xylose
- Abstract:
- ... The optimal microwave-assisted extraction conditions of pistachio green hull (PGH) pectin (extraction yield of 18.13%) were in microwave power of 700 W, irradiation time of 165 s, and pH of 1.5. The physico-chemical, structural and functional properties of pectin was examined and the results showed that PGH pectin under optimum conditions was low methoxyl (about 12.1%) with molecular weight of 1.6 ...
- DOI:
- 10.1016/j.foodchem.2018.07.212
- https://dx.doi.org/10.1016/j.foodchem.2018.07.212
- Author:
- Wang, Caili; Wang, Dong; Yang, Runquan; Wang, Huaifa
- Source:
- Powder technology 2019 v.342 pp. 397-403
- ISSN:
- 0032-5910
- Subject:
- Fourier transform infrared spectroscopy; X-ray diffraction; antimony; calcium silicate; coatings; electrical properties; energy-dispersive X-ray analysis; hydrolysis; nanoparticles; pH; powders; surface area; temperature; tin dioxide; transmission electron microscopy
- Abstract:
- ... Composite antistatic powders of wollastonite coated with antimony-doped tin oxide nanoparticles (Sb-SnO2/wollastonite, SSW) were prepared by heterogeneous nucleation method. The samples were characterized by X-ray diffraction (XRD), Fourier transform infrared (FTIR) spectroscopy, Scanning electronic microscopy (SEM), Transmission electron microscopy (TEM) and Energy-dispersive X-ray spectrometry ( ...
- DOI:
- 10.1016/j.powtec.2018.09.092
- https://dx.doi.org/10.1016/j.powtec.2018.09.092
85. Sacrificial template-based synthetic approach of polypyrrole hollow fibers for photothermal therapy
- Author:
- Bhattarai, Deval Prasad; Tiwari, Arjun Prasad; Maharjan, Bikendra; Tumurbaatar, Batgerel; Park, Chan Hee; Kim, Cheol Sang
- Source:
- Journal of colloid and interface science 2019 v.534 pp. 447-458
- ISSN:
- 0021-9797
- Subject:
- Fourier transform infrared spectroscopy; X-ray diffraction; X-ray photoelectron spectroscopy; coatings; cytotoxicity; differential scanning calorimetry; drugs; irradiation; nanofibers; nanoparticles; near-infrared spectroscopy; neoplasm cells; pH; phosphates; photothermotherapy; polymerization; polymers; pyrroles; scanning electron microscopy; thermogravimetry
- Abstract:
- ... In the present work, polypyrrole hollow fibers (PPy-HFs) were fabricated by sacrificial removal of soft templates of electrospun polycaprolactone (PCL) fibers with polypyrrole (PPy) coating through chemical polymerization of pyrrole monomer. Different physicochemical properties of as-fabricated PPy-HFs were then studied by Field emission scanning electron microscopy (FE-SEM), X-ray diffraction (XR ...
- DOI:
- 10.1016/j.jcis.2018.09.047
- https://dx.doi.org/10.1016/j.jcis.2018.09.047
- Author:
- Morosanu, Irina; Teodosiu, Carmen; Coroaba, Adina; Paduraru, Carmen
- Source:
- Journal of environmental management 2019 v.230 pp. 110-118
- ISSN:
- 0301-4797
- Subject:
- Fourier transform infrared spectroscopy; X-ray photoelectron spectroscopy; aqueous solutions; biosorption; desorption; dyes; effluents; kinetics; lead; metal ions; pH; rapeseed; response surface methodology; statistical models
- Abstract:
- ... Rapeseed (RS) waste was used for sequential biosorption from aqueous solutions of two target micropollutants: lead ions and Reactive blue 19 (Rb19) dye, through an integrated approach, combining experimental assessment and statistical modeling. In both cases of sequential biosorption, a pseudo-second order kinetic model fitted the biosorption data well. Intraparticle diffusion proved to be the rat ...
- DOI:
- 10.1016/j.jenvman.2018.09.075
- http://dx.doi.org/10.1016/j.jenvman.2018.09.075
- Author:
- Anirudhan, T.S.; Lekshmi, G.S.; Shainy, F.
- Source:
- Journal of colloid and interface science 2019 v.534 pp. 248-261
- ISSN:
- 0021-9797
- Subject:
- Fourier transform infrared spectroscopy; X-ray diffraction; X-ray photoelectron spectroscopy; adsorbents; adsorption; bentonite; chitosan; cross-linking reagents; energy-dispersive X-ray analysis; ethylene glycol; free radicals; hydrochloric acid; kinetics; models; pH; polymerization; potassium; potassium persulfate; scanning electron microscopy; seawater; surface area; uranium
- Abstract:
- ... A novel amidoxime functionalized adsorbent, poly(amidoxime)-grafted-chitosan/bentonite composite [P(AO)-g-CTS/BT] was prepared by in situ intercalative polymerization of acrylonitrile (AN) and 3-hexenedinitrile (3-HDN) onto chitosan/bentonite composite using ethylene glycol dimethacrylate (EGDMA) as cross linking agent and potassium peroxy disulphate (K2S2O8) as free radical initiator. The adsorbe ...
- DOI:
- 10.1016/j.jcis.2018.09.009
- https://dx.doi.org/10.1016/j.jcis.2018.09.009
- Author:
- Hojnik, Nataša; Modic, Martina; Ni, Yuan; Filipič, Gregor; Cvelbar, Uroš; Walsh, James L.
- Source:
- Environmental science & technology 2019 v.53 no.4 pp. 1893-1904
- ISSN:
- 1520-5851
- Subject:
- Aspergillus flavus; Fourier transform infrared spectroscopy; adverse effects; atmospheric pressure; decontamination; direct contact; disinfectants; disinfection; fungal spores; fungi; green chemistry; hydrogen peroxide; microbial contamination; nitrates; nitrites; nitrogen; nitrogen oxides; oxygen; ozone; pH; public health; toxicity
- Abstract:
- ... Fungal contamination of surfaces is a global burden, posing a major environmental and public health challenge. A wide variety of antifungal chemical agents are available; however, the side effects of the use of these disinfectants often result in the generation of toxic residues raising major environmental concerns. Herein, atmospheric pressure air plasma generated by a surface barrier discharge ( ...
- DOI:
- 10.1021/acs.est.8b05386
- http://dx.doi.org/10.1021/acs.est.8b05386
- Author:
- Tokarczyk, Karolina; Jachimska, Barbara
- Source:
- Colloids and surfaces 2019 v.561 pp. 357-363
- ISSN:
- 0927-7757
- Subject:
- Fourier transform infrared spectroscopy; bovine serum albumin; colloids; dendrimers; electrophoresis; electrostatic interactions; fluorouracil; hydrophobicity; light scattering; nanocarriers; nanoparticles; pH; quartz crystal microbalance; surface plasmon resonance
- Abstract:
- ... The success of novel therapeutic strategies relies strongly on the development of a reliable active agent delivery mechanism. In this work, we address the question of how G4 PAMAM dendrimers form complexes with a therapeutic agent, 5-fluorouracil (5-FU) and interact with bovine serum albumin (BSA). The analytical techniques, such as: UV–vis spectrophotometry, dynamic light scattering, electrophore ...
- DOI:
- 10.1016/j.colsurfa.2018.10.080
- https://dx.doi.org/10.1016/j.colsurfa.2018.10.080
- Author:
- Sivalingam, Sivamani; Kella, Tatinaidu; Maharana, Manisha; Sen, Sujit
- Source:
- Journal of cleaner production 2019 v.208 pp. 1241-1254
- ISSN:
- 0959-6526
- Subject:
- Fourier transform infrared spectroscopy; X-ray diffraction; X-ray fluorescence spectroscopy; adsorbents; adsorption; artificial colors; coal; desorption; fly ash; hot water treatment; kinetics; methylene blue; models; pH; protocols; response surface methodology; scanning electron microscopy; sonication; sorption isotherms; surface area; textile mill effluents; transmission electron microscopy; zeolites
- Abstract:
- ... Sono-assisted adsorptive elimination of dyes from industrial effluent is proved to be a fast, efficient and clean technique. Highly pure nanozeolite X (nFAZX) was synthesized from waste coal post-combustion fly ash (CFA) by pre-fusion hydrothermal method. Rapid sono-assisted adsorptive elimination of methylene blue (MB) dye from water solution was studied in presence nFAZX, CFA and commercial zeol ...
- DOI:
- 10.1016/j.jclepro.2018.10.200
- https://dx.doi.org/10.1016/j.jclepro.2018.10.200
- Author:
- Zhang, Bo; Liu, Wenwen; Sun, Dejun; Li, Yujiang; Wu, Tao
- Source:
- Colloids and surfaces 2019 v.561 pp. 244-253
- ISSN:
- 0927-7757
- Subject:
- 2,4-dichlorophenol; Fourier transform infrared spectroscopy; X-ray diffraction; X-ray photoelectron spectroscopy; adsorbents; adsorption; aqueous solutions; carbon; colloids; dispersibility; heat production; hydroxides; models; nanoparticles; nanospheres; oxides; pH; permeability; pollutants; porosity; porous media; scanning electron microscopy; sorption isotherms; surface area; transmission electron microscopy; zeta potential
- Abstract:
- ... The porous nanomaterials with hollow structure offers widespread potential applications due to its low density, strong dispersibility, rich porosity, high surface area, and good permeability. In this study, a hollow nanoshell of layered double oxides (LDOs) was synthesized using carbon nanospheres as a sacrificial template core and layer double hydroxides (LDHs) as shell-building precursors. The m ...
- DOI:
- 10.1016/j.colsurfa.2018.10.068
- https://dx.doi.org/10.1016/j.colsurfa.2018.10.068
- Author:
- Gasemloo, Sima; Khosravi, Morteza; Sohrabi, Mahmoud Reza; Dastmalchi, Siavoush; Gharbani, Parvin
- Source:
- Journal of cleaner production 2019 v.208 pp. 736-742
- ISSN:
- 0959-6526
- Subject:
- Fourier transform infrared spectroscopy; X-ray diffraction; aqueous solutions; carboxymethylcellulose; chromium; crosslinking; energy-dispersive X-ray analysis; ions; models; pH; response surface methodology; scanning electron microscopy; tanneries; wastewater
- Abstract:
- ... Sulfated carboxymethyl cellulose nanofilter membrane by crosslinking of glutaradehyde (GA) supported on polysulfone membrane (SCMC-GA-NF) was prepared and characterized by FTIR, XRD, SEM and EDS. The modeling of Cr (VI) removal from tannery industries wastewater by utilizing synthesized SCMC-GA-NF was studied by response surface methodology. The initial pH (4,8,12), pressure (2, 4, 6 bar) and SO3/ ...
- DOI:
- 10.1016/j.jclepro.2018.10.177
- https://dx.doi.org/10.1016/j.jclepro.2018.10.177
- Author:
- Ji, Haodong; Zhu, Yangmo; Liu, Wen; Bozack, Michael J.; Qian, Tianwei; Zhao, Dongye
- Source:
- Colloids and surfaces 2019 v.561 pp. 373-380
- ISSN:
- 0927-7757
- Subject:
- Fourier transform infrared spectroscopy; X-ray photoelectron spectroscopy; air; anaerobic conditions; calcium; carboxymethylcellulose; colloids; groundwater; humic acids; hydrochemistry; ions; iron; nanoparticles; pH; soil; technetium
- Abstract:
- ... Technetium (99Tc) typically exists as pertechnetate (TcO4−) and hydrated oxide (TcO2·nH2O) in soil and groundwater. While the former, Tc(VII), is very soluble and mobile in the environment, the latter is considered sparingly soluble and immobile. Consequently, immobilization of Tc(VII) can be achieved through conversion of Tc(VII) into Tc(IV). In this study, carboxymethyl cellulose (CMC) stabilize ...
- DOI:
- 10.1016/j.colsurfa.2018.10.048
- https://dx.doi.org/10.1016/j.colsurfa.2018.10.048
- Author:
- Hua, Mei; Lu, Jiaxi; DiQu,; Liu, Chang; Zhang, Lei; Li, Shanshan; Chen, Jianbo; Sun, Yinshi
- Source:
- Food chemistry 2019
- ISSN:
- 0308-8146
- Subject:
- Fourier transform infrared spectroscopy; Panax; X-ray diffraction; adsorption; cellulose; cholesterol; crystal structure; dietary fiber; food processing; glucose; hydrolysis; moieties; nitrites; pH; protein content; pyrolysis; scanning electron microscopes; sodium cholate; temperature; uronic acids; water holding capacity
- Abstract:
- ... The insoluble dietary fiber from ginseng residue (ginseng-IDF) was extracted using the AOAC (Association of Official Analytical Chemists) method with content of 68.61%. Ginseng-IDF had a polysaccharide content of 18.87%, uronic acid content of 7.85%, protein content of 6.52%, and had ideal water-holding capacity (17.66 g/g), swelling ability (15.05 mL/g), and oil-holding capacity (1.78 g/g). Scann ...
- DOI:
- 10.1016/j.foodchem.2019.01.114
- https://dx.doi.org/10.1016/j.foodchem.2019.01.114
- Author:
- Ma, Jie; Sun, Mengya; Zeng, Yulan; Liu, Zhenhua; Zhang, Manman; Xiao, Yao; Zhang, Shuping
- Source:
- RSC advances 2019 v.9 no.6 pp. 3337-3344
- ISSN:
- 2046-2069
- Subject:
- Fourier transform infrared spectroscopy; X-ray diffraction; X-ray photoelectron spectroscopy; absorption; adsorbents; adsorption; aqueous solutions; cadmium; carbon; chromium; copper; desorption; heavy metals; iron; kinetics; lead; magnetism; manganese; mercury; metal ions; microparticles; pH; scanning electron microscopy; transmission electron microscopy; zinc
- Abstract:
- ... Herein, Acac-C@Fe₃O₄, a magnetic carbon (C@Fe₃O₄) modified with acetylacetone (Acac), was first prepared and used as a solid-phase adsorbent for adsorbing some heavy metal ions from aqueous solution. The adsorbent was characterized by Fourier transform infrared spectroscopy (FTIR), X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), X-ray photoelect ...
- DOI:
- 10.1039/c8ra09830a
- http://dx.doi.org/10.1039/c8ra09830a
- Author:
- Abdolmohammad-Zadeh, Hossein; Ayazi, Zahra; Nezami, Kobra
- Source:
- Analytical methods 2019 v.11 no.4 pp. 462-471
- ISSN:
- 1759-9679
- Subject:
- Fourier transform infrared spectroscopy; X-ray diffraction; aqueous solutions; atomic absorption spectrometry; energy-dispersive X-ray analysis; ions; magnetism; magnetite; manganese; pH; permanganates; potassium; scanning electron microscopy; solid phase extraction; standard deviation
- Abstract:
- ... A novel magnetic solid-phase extraction (MSPE) method applying a nanosorbent based on an Ni–Al layered double hydroxide/magnetite nano-hybrid (Ni–Al LDH/Fe₃O₄) was developed for the preconcentration and speciation of Mn(vii)/Mn(ii) in aqueous solutions via flame atomic absorption spectrometry. The synthesized Ni–Al LDH/Fe₃O₄ nano-hybrid was characterized via X-ray diffraction, Fourier transform in ...
- DOI:
- 10.1039/c8ay02347f
- http://dx.doi.org/10.1039/c8ay02347f
- Author:
- Gacka, Ewelina; Wojcik, Aleksandra; Mazurkiewicz-Pawlicka, Marta; Malolepszy, Artur; Stobiński, Leszek; Kubas, Adam; Hug, Gordon L.; Marciniak, Bronislaw; Lewandowska-Andralojc, Anna
- Source:
- Journal of physical chemistry 2019 v.123 no.6 pp. 3368-3380
- ISSN:
- 1932-7455
- Subject:
- Fourier transform infrared spectroscopy; electron transfer; electrostatic interactions; fluorescence; graphene oxide; molecular models; nanohybrids; pH; physical chemistry; porphyrins; thermogravimetry
- Abstract:
- ... Noncovalent nanohybrids between meso-(p-hydroxyphenyl)porphyrin (TPPH) and graphene oxide (GO) sheets were studied as a function of pH. The overall charge of the TPPH molecule changes between negative (−4), neutral, and positive (+2) depending on the pH of the solution. Results of Fourier transform infrared spectroscopy, thermogravimetric analysis, and elemental analysis confirm successful noncova ...
- DOI:
- 10.1021/acs.jpcc.8b11374
- http://dx.doi.org/10.1021/acs.jpcc.8b11374
- Author:
- Akram, Muhammad; Khan, Binish; Imran, Muhammad; Ahmad, Iftikhar; Ajaz, Humayun; Tahir, Muhammad; Rabbani, Faiz; Kaleem, Imdad; Nadeem Akhtar, Muhammad; Ahmad, Naveed; Samad Shah, Noor
- Source:
- International journal of phytoremediation 2019 v.21 no.2 pp. 138-144
- ISSN:
- 1549-7879
- Subject:
- Fourier transform infrared spectroscopy; Gossypium hirsutum; adsorbents; biomass; biosorption; cotton; heavy metals; humans; ion exchange; lead; models; moieties; pH; phytoremediation; porosity; porous media; risk; scanning electron microscopy; sorption isotherms; surface area; temperature; toxicity; water pollution
- Abstract:
- ... Lead (Pb) is a toxic heavy metal causing serious health risks to humans and animals. In the present study, cotton (Gossypium hirsutum L.) shells powder was used as adsorbent for the treatment of synthetic Pb-contaminated water. The batch scale biosorption capacity of cotton shells powder was evaluated to study the effects of Pb concentrations, adsorbent doses and contact time at constant pH (6) an ...
- DOI:
- 10.1080/15226514.2018.1488810
- https://dx.doi.org/10.1080/15226514.2018.1488810
- Author:
- Ali, Imran; Peng, Changsheng; Naz, Iffat; Lin, Dichu; Saroj, Devendra P.; Ali, Mohsin
- Source:
- RSC advances 2019 v.9 no.7 pp. 3625-3646
- ISSN:
- 2046-2069
- Subject:
- Fourier transform infrared spectroscopy; X-ray diffraction; X-ray photoelectron spectroscopy; adsorbents; crosslinking; encapsulation; energy-dispersive X-ray analysis; hydrogen bonding; hydrophilicity; hysteresis; industrial applications; magnetism; malachite green; models; moieties; nanoparticles; oxidation; pH; pollutants; pollution control; polyvinyl alcohol; scanning electron microscopy; sodium alginate; thermogravimetry; washing; wastewater treatment
- Abstract:
- ... Novel bio-magnetic membrane capsules (BMMCs) were prepared by a simple two-step titration-gel cross-linking method using a polyvinyl alcohol (PVA) and sodium alginate (SA) matrix to control the disintegration of phytogenic magnetic nanoparticles (PMNPs) in an aqueous environment, and their performance was investigated for adsorbing cationic malachite green (MG) dye from water. The prepared BMMCs w ...
- DOI:
- 10.1039/c8ra09275c
- http://dx.doi.org/10.1039/c8ra09275c
- Author:
- Wang, Jingjing; Zhang, Wenhui; Wei, Jun
- Source:
- Journal of materials chemistry A 2019 v.7 no.5 pp. 2055-2065
- ISSN:
- 2050-7496
- Subject:
- Fourier transform infrared spectroscopy; X-ray diffraction; X-ray photoelectron spectroscopy; adsorbents; adsorption; beta-cyclodextrin; cadmium; electrostatic interactions; graphene oxide; heavy metals; hydrogen bonding; ionic strength; magnetic fields; metal ions; pH; pollutants; polymerization; scanning electron microscopy; sulfamethazine; transmission electron microscopy
- Abstract:
- ... In order to realize synergetic adsorption of heavy metal ions and organic pollutants, poly(β-cyclodextrin)-conjugated magnetic graphene oxide (MGO@poly(β-CD)) was designed and fabricated. The MGO@poly(β-CD) was characterized by Fourier transform infrared spectroscopy, X-ray photoelectron spectroscopy, scanning electron microscopy, transmission electron microscopy, X-ray diffraction and vibrating s ...
- DOI:
- 10.1039/c8ta09250h
- http://dx.doi.org/10.1039/c8ta09250h