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1. Dynamics of Entangled cis-1,4-Polyisoprene Confined to Nanoporous Alumina

Author:
Politidis, Christos,   et al.   ; Alexandris, Stelios; Sakellariou, Georgios; Steinhart, Martin; Floudas, George;     Show all 5 Authors
Source:
Macromolecules 2019 v.52 no.11 pp. 4185-4195
ISSN:
1520-5835
Subject:
adsorption; aluminum oxide; annealing; cooling; desorption; dielectric spectroscopy; differential scanning calorimetry; electric field; energy; geometry; glass; heat; molecular weight; nanopores; polymers; temperature
Abstract:
... The dynamics of a series of entangled cis-1,4-polyisoprenes located within self-ordered nanoporous alumina templates are studied as a function of the degree of confinement, 2Rg/d (Rg is the radius of gyration and d is the pore diameter) with dielectric spectroscopy and temperature-modulated differential scanning calorimetry. For the higher molecular weights, the segmental dynamics obtained on cool ...
DOI:
10.1021/acs.macromol.9b00523