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1. Allylation of aldehydes by dual photoredox and nickel catalysis

Author:
Marchini, Marianna,   et al.   ; Gualandi, Andrea; Rodeghiero, Giacomo; Faraone, Adriana; Patuzzo, Filippo; Calogero, Francesco; Perciaccante, Rossana; Jansen, Thomas Paul; Ceroni, Paola; Cozzi, Pier Giorgio;     Show all 10 Authors
Source:
Chemical communications 2019 v.55 no.48 pp. 6838-6841
ISSN:
1364-548X
Subject:
alcohols; aldehydes; allylation; catalysts; catalytic activity; heterocyclic compounds; irradiation; nickel; redox reactions; ruthenium
Abstract:
... Here we report the application of dual nickel/photoredox catalysis to the allylation of aliphatic, aromatic and heteroaromatic aldehydes by using commercially available reagents. The process utilizes the combination of a Ni(ii) complex, [Ru(bpy)₃]²⁺ as a photoredox catalyst, and allylacetate under blue LED irradiation, and allows the synthesis of a large variety of homoallylic alcohols. ...
DOI:
10.1039/c9cc03344k