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- Author:
- Bettina Baumgartner; Stephan Freitag; Bernhard Lendl
- Source:
- Analytical chemistry 2020 v.92 no.7 pp. 4736-4741
- ISSN:
- 1520-6882
- Subject:
- Escherichia coli; Fourier transform infrared spectroscopy; bovine serum albumin; cost effectiveness; crystals; epoxides; germanium; optical equipment; polymerization; silicon; spectrometers; temperature; three-dimensional printing; wafers
- Abstract:
- ... In this work, we present a fully 3D-printed module for attenuated total reflection Fourier transform infrared (ATR-FTIR) spectroscopy ready for use in commercial FTIR spectrometers. The developed setup stands out in terms of robustness and ease of sample application. Rapid prototyping paired with theoretical considerations were employed to design and fabricate the module. Cost-efficient commercial ...
- DOI:
- 10.1021/acs.analchem.9b04043
- https://doi.org/10.1021/acs.analchem.9b04043
- Author:
- Laura Bergamonti; Marianna Potenza; Azar Haghighi Poshtiri; Andrea Lorenzi; Anna Maria Sanangelantoni; Laura Lazzarini; Pier Paolo Lottici; Claudia Graiff
- Source:
- Carbohydrate polymers 2020 v.231 pp. 115773
- ISSN:
- 0144-8617
- Subject:
- Aspergillus niger; Bacillus subtilis; Escherichia coli; Fourier transform infrared spectroscopy; Raman spectroscopy; X-ray diffraction; acid hydrolysis; aesthetics; cellulose; coatings; cotton; crystal structure; fungi; mechanical testing; minimum inhibitory concentration; nanocrystals; nanosilver; silver; sulfuric acid; transmission electron microscopy; waste paper
- Abstract:
- ... Waste paper is an environmentally friendly source of cellulosic material. Here we propose a new treatment based on nanocrystalline cellulose (CNC) for paper preservation and consolidation. Suspensions of CNC were prepared by sulfuric acid hydrolysis using waste paper as cellulose source (CNCWP) and compared with CNC from cotton linter (CNCCL). Both CNCs were obtained with good yield, showing high ...
- DOI:
- 10.1016/j.carbpol.2019.115773
- https://doi.org/10.1016/j.carbpol.2019.115773
- Author:
- Huimin Sun; Shuai Li; Shanshan Chen; Chunying Wang; Di Liu; Xinxin Li
- Source:
- International journal of biological macromolecules 2020 v.159 pp. 696-703
- ISSN:
- 0141-8130
- Subject:
- Bacillus subtilis; Escherichia coli; Fourier transform infrared spectroscopy; Staphylococcus aureus; antimicrobial properties; antioxidants; biodegradability; cinnamon; corn; corn oil; emulsions; encapsulation; essential oils; microstructure; oxygen; particle size distribution; permeability; polymers; sodium; starch; tensile strength; water vapor
- Abstract:
- ... This study aimed to determine the potential of sodium starch octenylsuccinate (SSOS)-based Pickering emulsions incorporated with cinnamon essential oil (CEO) as a vehicle for delivering active biodegradable films to improve their antimicrobial and antioxidant activites. This study explored the combined effects of mixed oils (CEO and corn oils). Particle size distribution, mean drop size, ζ-potenti ...
- DOI:
- 10.1016/j.ijbiomac.2020.05.118
- https://doi.org/10.1016/j.ijbiomac.2020.05.118
- Author:
- Zunaira Habib; Sher Jamal Khan; Nasir Mehmood Ahmad; Hafiz Muhammad Aamir Shahzad; Yousuf Jamal; Imran Hashmi
- Source:
- Environmental technology 2020 v.41 no.28 pp. 3657-3669
- ISSN:
- 1479-487X
- Subject:
- Bacillus subtilis; Escherichia coli; Fourier transform infrared spectroscopy; antibacterial properties; antifouling activities; atomic force microscopy; bacterial growth; biofilm; contact angle; energy-dispersive X-ray analysis; environmental technology; nanofiltration; permeability; polyamides; silver
- Abstract:
- ... Modification of active membrane surface is an auspicious way to enhance the membrane performance. In our study, a commercially available composite polyamide Nanofiltration (NF) membrane was modified by immobilizing silver doped TiO₂ (Ag–TiO₂) nanoparticles. Ag–TiO₂ with different nanoparticles concentration (0.05, 0.1, and 0.5 wt. %) were coated on the surface of the membrane by a dip coating meth ...
- DOI:
- 10.1080/09593330.2019.1617355
- https://doi.org/10.1080/09593330.2019.1617355
- Author:
- L.M. Dwivedi; K. Baranwal; S. Gupta; M. Mishra; S. Sundaram; V. Singh
- Source:
- International journal of biological macromolecules 2020 v.149 pp. 1323-1330
- ISSN:
- 0141-8130
- Subject:
- Bacillus subtilis; Cellulosimicrobium cellulans; Escherichia coli; Fourier transform infrared spectroscopy; Staphylococcus; X-ray diffraction; antibiotics; bioactive properties; guar gum; nanocomposites; nanomaterials; oxidation; particle size; scanning electron microscopy; sodium; sodium alginate; transmission electron microscopy; zinc oxide
- Abstract:
- ... The present study describes synthesis, characterization and antibacterial application of oxidized sodium alginate (OSA)-zinc oxide (ZnO) hybrid nanostructures (OSA-ZnO). In continuation to our previous study on oxidized guar gum (OGG)-ZnO (OGG-ZnO) nanocomposite, in the present study we have chosen OSA to understand the role of polysaccharide charge type in designing the antibacterial material. Th ...
- DOI:
- 10.1016/j.ijbiomac.2020.02.011
- https://doi.org/10.1016/j.ijbiomac.2020.02.011
- Author:
- Liduo Rong; Xin Shen; Bijia Wang; Zhiping Mao; Xueling Feng; Xiaofeng Sui
- Source:
- International journal of biological macromolecules 2020 v.147 pp. 18-23
- ISSN:
- 0141-8130
- Subject:
- Escherichia coli; Fourier transform infrared spectroscopy; Staphylococcus aureus; acetoacetic acid; antibacterial properties; biopolymers; cellulose; chitosan; cross-linking reagents; crosslinking; droplets; emulsifiers; emulsions; enamines; gels; ingredients; rheology; thyme; viscosity
- Abstract:
- ... Organo-hydrogels are widely used in various fields, due to functional organic ingredients immobilized by the gel network or stored and protected by the gels. Herein, cellulose acetoacetate (CAA) served as reactive natural polymer emulsifier to stabilize thyme oil-in-water (O/W) emulsions. Hydroxypropyl chitosan (HPCS) was added to the continuous phase in emulsions to achieve the organo-hydrogel vi ...
- DOI:
- 10.1016/j.ijbiomac.2020.01.052
- https://doi.org/10.1016/j.ijbiomac.2020.01.052
- Author:
- Betül Yılmaz Öztürk; Bükay Yenice Gürsu; İlknur Dağ
- Source:
- Process biochemistry 2020 v.89 pp. 208-219
- ISSN:
- 1359-5113
- Subject:
- Candida albicans; Escherichia coli; Fourier transform infrared spectroscopy; Gelidium; X-ray diffraction; antimicrobial properties; bacteria; biofilm; crystal structure; geometry; minimum inhibitory concentration; moieties; nanoparticles; nanosilver; reducing agents; sustainable technology; therapeutics; transmission electron microscopy; ultraviolet-visible spectroscopy; yeasts
- Abstract:
- ... In our study, green synthesis of silver nanoparticles was carried out using a red algae Gelidium corneum extract as reducing agent. The obtained silver nanoparticles were characterized by UV–vis, TEM, XRD, FTIR and ICP-MS measurements. FTIR measurements indicated the possible functional groups responsible for the stabilization and reduction of nanoparticles, while XRD analysis results explained th ...
- DOI:
- 10.1016/j.procbio.2019.10.027
- https://doi.org/10.1016/j.procbio.2019.10.027
- Author:
- Sania Naz; Saira Tabassum; Nelson Freitas Fernandes; Mohammad Mujahid; Muhammad Zia; Esperanza J. Carcache de Blanco
- Source:
- Natural product research 2020 v.34 no.5 pp. 720-725
- ISSN:
- 1478-6427
- Subject:
- Bacillus subtilis; Escherichia coli; Fourier transform infrared spectroscopy; Rhus; X-radiation; X-ray diffraction; animal models; antibacterial properties; antineoplastic agents; cupric oxide; cytotoxicity; drug development; energy-dispersive X-ray analysis; geometry; heat; inhibitory concentration 50; nanoparticles; neoplasm cells; particle size; prostatic neoplasms; protein kinases; reducing agents; scanning electron microscopy; thermal analysis; transcription factor NF-kappa B; transmission electron microscopy
- Abstract:
- ... The present study reports ecofriendly synthesis of CuO nanoparticles (NPs) using an extract of Rhus punjabensis as a reducing agent. NPs structural and composition analysis are evaluated by X-rays diffraction (XRD), Fourier transform infrared, Energy dispersive spectroscopy, Scanning electron microscopy, Transmission electron microscopy, and Thermal analysis. The NPs have pure single phase monocli ...
- DOI:
- 10.1080/14786419.2018.1495633
- https://doi.org/10.1080/14786419.2018.1495633
- Author:
- Yupei Li; Jiameng Li; Zhenqiang Shi; Yilin Wang; Xin Song; Liya Wang; Mei Han; Heyue Du; Chao He; Weifeng Zhao; Baihai Su; Changsheng Zhao
- Source:
- Carbohydrate polymers 2020 v.243 pp. 116470
- ISSN:
- 0144-8617
- Subject:
- Escherichia coli; Fourier transform infrared spectroscopy; Staphylococcus aureus; X-ray photoelectron spectroscopy; adsorption; anticoagulant activity; anticoagulants; bacteria; blood; chemical composition; chitosan; complement; crosslinking; endotoxins; hemolysis; hydrogels; patients; platelet activation; scanning electron microscopy; sorbents
- Abstract:
- ... Here, we describe a green approach to fabricate genipin crosslinked chitosan-kappa-carrageenan composite hydrogels (C-K hydrogels) aiming at reducing endotoxin level and bacteria burden in septic blood synchronously. The chemical compositions and morphologies of the developed C-K hydrogels were characterized by Fourier transform infrared spectroscopy, X-ray photoelectron spectroscopy and scanning ...
- DOI:
- 10.1016/j.carbpol.2020.116470
- https://doi.org/10.1016/j.carbpol.2020.116470
10. Anticoagulant dialyzer with enhanced Ca2+ chelation and hydrophilicity for heparin free hemodialysis
- Author:
- Yang Liu; Guiliang Li; Qiu Han; Haibo Lin; Qiang Li; Jing Hua; Fu Liu
- Source:
- Journal of membrane science 2020 v.604 pp. 118082
- ISSN:
- 0376-7388
- Subject:
- Escherichia coli; Fourier transform infrared spectroscopy; adhesion; adsorption; anticoagulants; antifouling activities; aqueous solutions; artificial membranes; atomic force microscopy; biocompatibility; blood platelets; calcium; carbon; chelation; complement; contact angle; creatine; crosslinking; dialysis; hemodialysis; hemolysis; heparin; hydrogels; hydrophilicity; nuclear magnetic resonance spectroscopy; phosphorus; proteins; scanning electron microscopy; sodium; stable isotopes; swine; thrombosis; toxins; urea
- Abstract:
- ... Inhibiting thrombosis in extracorporeal dialyzer is predominantly determined by the compatible interface design. It is challenging to develop anticoagulant dialyzers for clinical heparin free dialysis. Herein, we develop an environmentally friendly approach to construct a hydrogel skin composed of poly (sodium alginate-acrylic acid) P (SA-AA) network on polysulfone (PSf) membranes via pre-seeding ...
- DOI:
- 10.1016/j.memsci.2020.118082
- https://doi.org/10.1016/j.memsci.2020.118082
- Author:
- C. Vijilvani; M.R. Bindhu; F.C. Frincy; Mohamad S. AlSalhi; S. Sabitha; K. Saravanakumar; Sandhanasamy Devanesan; M. Umadevi; Mamduh J. Aljaafreh; Muhammad Atif
- Source:
- Journal of photochemistry and photobiology 2020 v.202 pp. 111713
- ISSN:
- 1011-1344
- Subject:
- Escherichia coli; Fourier transform infrared spectroscopy; Solanum nigrum; X-ray diffraction; aminophenols; antioxidants; biosynthesis; catalysts; catalytic activity; energy-dispersive X-ray analysis; gold; leaves; nanobiotechnology; nanogold; nanomedicine; nanoparticles; nanosilver; p-nitrophenol; palladium; physicochemical properties; polyphenols; silver; sodium borohydride; transmission electron microscopy
- Abstract:
- ... The field of nanobiotechnology and nanomedicine paves way for the use of several nanoparticles. Especially, in biomedical applications, the silver nanoparticles (AgNPs), gold nanoparticles (AuNPs) and palladium nanoparticles (PdNPs) are found most vital and promising, among other nanoparticles. The biomedical activities of these particles mostly depend on their shape, size and distribution. Prepar ...
- DOI:
- 10.1016/j.jphotobiol.2019.111713
- https://doi.org/10.1016/j.jphotobiol.2019.111713
- Author:
- Vivek Kumar Pandey; Siddh Nath Upadhyay; Keshavan Niranjan; Pradeep Kumar Mishra
- Source:
- International journal of biological macromolecules 2020 v.157 pp. 212-219
- ISSN:
- 0141-8130
- Subject:
- Escherichia coli; Fourier transform infrared spectroscopy; Listeria monocytogenes; X-ray diffraction; anti-infective agents; antimicrobial properties; biodegradability; biodegradation; chitosan; contact angle; crystal structure; food packaging; hydrophobicity; light scattering; meat; nanocomposites; nanosilver; packaging materials; polyvinyl alcohol; scanning electron microscopy; shelf life; ultraviolet-visible spectroscopy
- Abstract:
- ... Stable silver nanoparticles (AgNPs) of size 80 ± 11 nm produced by chitosan (CH) mediated green synthesis were blended with polyvinyl alcohol (PVA) to form electrospun fibrous composite nano-layers (FCNLs). The chitosan acted as the stabilising as well as an antimicrobial agent in combination with the AgNPs which were characterised using UV–visible spectrophotometry, dynamic light scattering (DLS) ...
- DOI:
- 10.1016/j.ijbiomac.2020.04.149
- https://doi.org/10.1016/j.ijbiomac.2020.04.149
- Author:
- Nasser A. Al-Tayyar; Ahmed M. Youssef; Rashad R. Al-Hindi
- Source:
- Food packaging and shelf life 2020 v.25 pp. 100523
- ISSN:
- 2214-2894
- Subject:
- Escherichia coli; Fourier transform infrared spectroscopy; Gram-negative bacteria; Gram-positive bacteria; Staphylococcus aureus; X-ray diffraction; antibacterial properties; antimicrobial packaging; breads; chitosan; contact angle; ecological footprint; food packaging; food pathogens; mechanical properties; nanocomposites; nanoparticles; packaging materials; permeability; polyvinyl alcohol; scanning electron microscopy; shelf life; silica; water vapor; zinc oxide; Iraq
- Abstract:
- ... In the current work, antimicrobial bionanocomposite films were fabricated based on chitosan (CS), poly (vinyl alcohol) (PVA) and nanocomposites comprised of silicon dioxide nanoparticles doped with zinc oxide nanoparticles (ZnO-SiO₂). The ZnO-SiO₂ nanocomposite was prepared and incorporated into a PVA/CS blend at different ratios (0.50, 1.0, 3.0 and 5.0 %) to generate the PVA/CS/ZnO-SiO₂ bionanoco ...
- DOI:
- 10.1016/j.fpsl.2020.100523
- https://doi.org/10.1016/j.fpsl.2020.100523
- Author:
- M. Amirul Islam; Walid M. Hassen; Azam F. Tayabali; Jan J. Dubowski
- Source:
- Biochemical engineering journal 2020 v.154 pp. 107435
- ISSN:
- 1369-703X
- Subject:
- Bacillus subtilis; Escherichia coli; Fourier transform infrared spectroscopy; Legionella pneumophila; Legionnaires' disease; antibodies; antimicrobial peptides; bacteria; binding capacity; biosensors; chemical bonding; culture media; fluorescence microscopy; mammals; prediction
- Abstract:
- ... Detection of pathogenic Legionella pneumophila by culture-based methods is not efficient in predicting outbreaks of the Legionnaires’ disease. The main problem is the relatively slow time-to-result and the inability of some culture media to support the growth of viable bacteria. One strategy to alleviate these issues is developing biosensors functionalized with mammalian antibodies designed to cap ...
- DOI:
- 10.1016/j.bej.2019.107435
- https://doi.org/10.1016/j.bej.2019.107435
- Author:
- Amr Fouda; Saad El-Din Hassan; Abdullah M. Abdo; Mamdouh S. El-Gamal
- Source:
- Biological trace element research 2020 v.195 no.2 pp. 707-724
- ISSN:
- 0163-4984
- Subject:
- Alternaria alternata; Aspergillus niger; Culex pipiens; Escherichia coli; Fourier transform infrared spectroscopy; Fusarium oxysporum; Gram-negative bacteria; Gram-positive bacteria; Musca domestica; Pseudomonas aeruginosa; Pythium ultimum; Streptomyces capillispiralis; Streptomyces pseudogriseolus; Streptomyces zaomyceticus; X-ray diffraction; anti-infective agents; antimicrobial properties; antioxidant activity; bioactive compounds; biocatalysts; biosynthesis; endophytes; energy-dispersive X-ray analysis; filtrates; hydrogen peroxide; in vitro studies; iron; larvicides; metabolites; nanoparticles; nanosilver; particle size; plant pathogenic fungi; scanning electron microscopy; surface plasmon resonance; transmission electron microscopy; ultraviolet-visible spectroscopy
- Abstract:
- ... In this study, metabolites involved in the free-biomass filtrates for three endophytic actinomycetes of Streptomyces capillispiralis Ca-1, Streptomyces zaomyceticus Oc-5, and Streptomyces pseudogriseolus Acv-11 were used as biocatalysts for green synthesis of silver nanoparticles (Ag-NPs). Characterization of biosynthesized Ag-NPs was accomplished using UV-Vis spectroscopy, X-ray diffraction patte ...
- DOI:
- 10.1007/s12011-019-01883-4
- https://doi.org/10.1007/s12011-019-01883-4
- Author:
- Nina Alizadeh; Shokufeh Malakzadeh
- Source:
- International journal of biological macromolecules 2020 v.147 pp. 778-791
- ISSN:
- 0141-8130
- Subject:
- 2,2-diphenyl-1-picrylhydrazyl; Escherichia coli; Fourier transform infrared spectroscopy; Staphylococcus aureus; X-ray diffraction; antibacterial properties; antineoplastic activity; antioxidant activity; antioxidants; bacteria; biodegradability; cell lines; chitosan; curcumin; cytotoxicity; encapsulation; gamma-cyclodextrin; hydrophobicity; inhibitory concentration 50; nanoparticles; polyphenols; scanning electron microscopy; ultraviolet-visible spectroscopy
- Abstract:
- ... Curcumin, as a naturally occurring polyphenol, has been extensively used as anticancer and antioxidant agent due to its ability to protect cells from oxidative damage. In the present study, we have prepared highly soluble CUR-β-cyclodextrin (β-CD) and γ-cyclodextrin (γ-CD) hollow spheres. UV–Vis method was employed to approve the successful formation of the inclusion complex where the aromatic rin ...
- DOI:
- 10.1016/j.ijbiomac.2020.01.206
- https://doi.org/10.1016/j.ijbiomac.2020.01.206
17. Application of Glycyrrhiza glabra L. Root as a Natural Antibacterial Agent in Finishing of Textile
- Author:
- Fazlıhan YILMAZ
- Source:
- Industrial crops and products 2020 v.157 pp. 112899
- ISSN:
- 0926-6690
- Subject:
- Escherichia coli; Fourier transform infrared spectroscopy; Glycyrrhiza glabra; Staphylococcus aureus; alum; aluminum sulfate; ambient temperature; antibacterial properties; antibiotics; atomic absorption spectrometry; bacteria; color; copper; copper sulfate; dyeing; ferrous sulfate; iron; lighting; potassium; scanning electron microscopy; textile finishes; tin; washing; woolen fabric; zinc chloride
- Abstract:
- ... The use of plant resources in different areas is increasing day by day. One of the uses of these resources is textile dyeing. In this study, Glycyrrhiza glabra L. roots were used for dyeing woolen fabrics. It is also aimed to give these dyed fabrics naturally antibacterial properties. In the dyeing process, copper (II) sulfate, tin chloride, iron (II) sulfate, zinc chloride and potassium aluminum ...
- DOI:
- 10.1016/j.indcrop.2020.112899
- https://doi.org/10.1016/j.indcrop.2020.112899
- Author:
- Ruyue Wang; Jinfeng Li; Dongya Dang; Jiong Hu; Yafang Hu; Jun Fan
- Source:
- Enzyme and microbial technology 2020 v.137 pp. 109547
- ISSN:
- 0141-0229
- Subject:
- Escherichia coli; Fourier transform infrared spectroscopy; cellulose; corn; enantiomers; humans; proteolysis; recombinant proteins; serine; serine racemase; technology; trypsin
- Abstract:
- ... Recombinant protein overexpressed in Escherichia coli is often less folded, leading to form the insoluble aggregates also called as inclusion bodies (IBs). IBs are classified as active and inactive ones, and enzyme produced as active IBs is the novel carrier-free immobilized material. In this study, we determined that His6-tagged serine racemase (SR) from maize or human produced as partially activ ...
- DOI:
- 10.1016/j.enzmictec.2020.109547
- https://doi.org/10.1016/j.enzmictec.2020.109547
- Author:
- Mohamed S. Aref; Salem S. Salem
- Source:
- Biocatalysis and agricultural biotechnology 2020 v.27 pp. 101689
- ISSN:
- 1878-8181
- Subject:
- Bacillus subtilis; Cinnamomum camphora; Escherichia coli; Fourier transform infrared spectroscopy; Pseudomonas aeruginosa; Staphylococcus aureus; X-ray diffraction; antibacterial properties; biomass; biotechnology; callus; callus culture; energy-dispersive X-ray analysis; nanoparticles; nanosilver; plant extracts; scanning electron microscopy; tissue culture; transmission electron microscopy; ultraviolet-visible spectroscopy; wavelengths
- Abstract:
- ... Plant tissue culture is considered as a basic and fundamental component of plant biotechnology and is considered a good approach for green synthesis of nanoparticles (NPs) because it is safe, eco-friendly and clean method. In the current study, callus extract of Cinnamonum camphora was utilized to the synthesis of silver nanoparticles (Ag-NPs) for the first time. Callus culture of C. camphora was ...
- DOI:
- 10.1016/j.bcab.2020.101689
- https://doi.org/10.1016/j.bcab.2020.101689
- Author:
- Devaraj Bharathi; Selvaraj Preethi; Kalimuthu Abarna; Manjunathan Nithyasri; Palaniswamy Kishore; Kathirvel Deepika
- Source:
- Biocatalysis and agricultural biotechnology 2020 v.27 pp. 101698
- ISSN:
- 1878-8181
- Subject:
- Escherichia coli; Fourier transform infrared spectroscopy; Solanum lycopersicum; acridine orange; antibacterial properties; antineoplastic activity; apoptosis; biosynthesis; color; energy-dispersive X-ray analysis; ethidium; fluorescence; fluorescence microscopy; human cell lines; human diseases; inhibitory concentration 50; iron; iron oxides; leaf extracts; light scattering; lung neoplasms; magnetism; nanoparticles; neoplasm cells; phytochemicals; scanning electron microscopy; staining; ultraviolet-visible spectroscopy
- Abstract:
- ... The synthesis of iron based magnetic nanoparticles is an expanding research area due to their potential applications in the development of novel technologies. The present study reports an eco-friendly synthesis of iron oxide nanoparticles (FeONPs) using Solanum lycopersicum leaf extract by a bio-inspired method. Synthesized FeONPs were characterized by using UV–visible spectroscopy, fourier transf ...
- DOI:
- 10.1016/j.bcab.2020.101698
- https://doi.org/10.1016/j.bcab.2020.101698