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1. .A new urea adducts method for PUFA concentration using green food grade solvents and avoiding ethyl carbamate formation

Author:
Luis Vázquez; Mario Sánchez-Moyano; Lorena de la Iglesia; Guillermo Reglero; Carlos F. Torres
Source:
Food chemistry 2022 pp. 133197
ISSN:
0308-8146
Subject:
Echium plantagineum; ambient temperature; ethanol; ethyl carbamate; food chemistry; green chemistry; hexane; liquids; microalgae; oils; propionic acid; salmon; solvents; toxic substances; urea
Abstract:
... This study aimed to selectively enrich stearidonic acid (SDA) together with γ-linolenic acid (GLA) in Echium plantagineum oil by urea complexation. The complexation process at room temperature was carried out replacing common organic solvents, such as hexane and ethanol, by alternative compounds, included in Green Solvent and Food Grade categories, adapting this process towards the principles of G ...
DOI:
10.1016/j.foodchem.2022.133197

2. 1D Hypo-Crystals of Stereo-Irregular PMMA via Spray-Induced Rapid Solidification of Aqueous Solutions

Author:
Jae Hyun Sim; Yejin Kwon; Sangwon Eom; Myoungsoon Hwang; Soyoung Park; Hyorin Choi; Hoeil Chung; Daewon Sohn; Youngjong Kang
Source:
Macromolecules 2022 v.55 no.5 pp. 1700-1708
ISSN:
1520-5835
Subject:
X-ray diffraction; benzoic acid; ethanol; hydrogen; solidification; solubility
Abstract:
... Synergistic solubility enhancement of poly(methyl methacrylate) (PMMA) in ethanol/water mixtures is observed in the presence of benzoic acid (BA). SAXS and 2D correlation Raman experiments show that PMMA chains strongly interact with BA molecules in PMMA/BA/ethanol/water quaternary solutions via hydrogen bonding and dispersion interactions, which leads to the spontaneous extension of PMMA chains. ...
DOI:
10.1021/acs.macromol.1c02304

3. 3D printing of crude lignocellulosic biomass extracts containing hemicellulose and lignin

Author:
E. Gokce Bahcegul; Erinc Bahcegul; Necati Ozkan
Source:
Industrial crops and products 2022 pp. 115234
ISSN:
0926-6690
Subject:
ambient temperature; biodegradability; biomass; biopolymers; cellulose; corn; ethanol; evaporation; gels; hemicellulose; lignin; lignocellulose; water content
Abstract:
... Using lignocellulosic biomass, which is composed mainly of cellulose, hemicellulose and lignin, as a biopolymer resource in various polymeric material applications is an attractive option due to its abundance, biodegradability and renewability. Cellulose is the most popular member of the biopolymer trio for material applications, but despite constituting around half of a lignocellulosic biomass, a ...
DOI:
10.1016/j.indcrop.2022.115234

4. A Comparative Assessment on the Recovery of Pectin and Phenolic Fractions from Aqueous and DES Extracts Obtained from Melon Peels

Author:
Xiana Rico; Beatriz Gullón; Remedios Yáñez
Source:
Food and bioprocess technology 2022 v.15 no.6 pp. 1406-1421
ISSN:
1935-5130
Subject:
adsorption; amberlite; antioxidant activity; autohydrolysis; bioprocessing; desorption; ethanol; galacturonic acid; liquids; melons; naringenin; oligosaccharides; pH; pectins; sodium acetate; solvents; urea; water solubility
Abstract:
... This work evaluates the purification of melon peel extracts obtained by two eco-friendly methods: autohydrolysis and sodium acetate/urea/water extraction (1:3:1.6), an alkaline deep eutectic solvent (DES). For that, sequential ethanol precipitation and resin adsorption/desorption stages were proposed for the separate recovery of the pectic and phenolic fractions. In order to screen the optimal pur ...
DOI:
10.1007/s11947-022-02823-2

5. A Coupling Process of Distillation with Vapor Permeation and Adsorption for Production of Fuel Ethanol: A Comparative Analysis on Energy Consumption

Author:
Jiacheng Wang; Jiaqi Zhang; Zhou Hong; Xuechao Gao; Xuehong Gu
Source:
Industrial & engineering chemistry process design and development 2022 v.61 no.2 pp. 1167-1178
ISSN:
1520-5045
Subject:
adsorption; culture media; distillation; energy efficiency; ethanol; ethanol fuels; permeability; process design; solvents; steam; zeolites
Abstract:
... To efficiently produce fuel ethanol from fermentation broth, the distillation column was coupled with vapor permeation (VP) of a NaA zeolite membrane instead of using the adsorption technique to remove solvent water. The comparative analysis indicated that the energy efficiency was consistently higher for distillation-VP coupling, using a single-column distillation and three-column distillation, r ...
DOI:
10.1021/acs.iecr.1c01978

6. A Descriptive Chemical Composition of Concentrated Bud Macerates through an Optimized SPE-HPLC-UV-MS2 Method—Application to Alnus glutinosa, Ribes nigrum, Rosa canina, Rosmarinus officinalis and Tilia tomentosa

Author:
Thomas Charpentier; Séverine Boisard; Anne-Marie Le Ray; Dimitri Bréard; Amélie Chabrier; Hélène Esselin; David Guilet; Christophe Ripoll; Pascal Richomme
Source:
Plants 2022 v.11 no.2 pp. -
ISSN:
2223-7747
Subject:
Alnus glutinosa; Ribes nigrum; Rosa canina; Rosmarinus officinalis; Tilia tomentosa; antioxidants; chemical composition; ethanol; glycerol; glycosylation; high performance liquid chromatography; maceration; meristems; nucleosides; quality control; rutin; solid phase extraction; solvents
Abstract:
... Concentrated bud macerates (CBMs) are obtained from meristematic tissues such as buds and young shoots by maceration in a solvent composed of glycerin, water and ethanol (1/1/1/, v/v). Their traditional utilization in gemmotherapy has gained interest in the past years, and the knowledge of their chemical characterization can provide commercial arguments, particularly to secure their quality contro ...
DOI:
10.3390/plants11020144

7. A First Report on the Effects of Nanoscale Nutrients on Fermentation Process and Bio-Ethanol Production from Bio-Fortified Sweet Sorghum

Author:
R. Naseeruddin; V. Sumathi; T. N. V. K. V. Prasad; P. Sudhakar; V. Chadrika; B. Ravindra Reddy; C. V. Ratnavathi
Source:
Sugar tech 2022 v.24 no.3 pp. 870-881
ISSN:
0972-1525
Subject:
calcium; calcium oxide; clean energy; ethanol; ethanol production; fermentation; field experimentation; juices; magnesium; sugars; sweet sorghum; zinc
Abstract:
... Often, clean energy concept is tagged with the bio-ethanol production from the agricultural sources. Herein, we are first to report on use of nanoscale materials (nano-CaO and nano-MgO) in fermentation process for bio-ethanol production from nanoscale materials (zinc, calcium and magnesium)-driven bio-fortified sweet sorghum. A field experiment was conducted during 2014 and 2015, and nanoscale mat ...
DOI:
10.1007/s12355-022-01137-z

8. A Hybrid RSM-ANN-GA Approach on Optimization of Ultrasound-Assisted Extraction Conditions for Bioactive Component-Rich Stevia rebaudiana (Bertoni) Leaves Extract

Author:
Kashif Ameer; Saqib Ameer; Young-Min Kim; Muhammad Nadeem; Mi-Kyung Park; Mian Anjum Murtaza; Muhammad Asif Khan; Muhammad Adnan Nasir; Ghulam Mueen-ud-Din; Shahid Mahmood; Tusneem Kausar; Muhammad Abubakar
Source:
Foods 2022 v.11 no.6 pp. -
ISSN:
2304-8158
Subject:
Stevia rebaudiana; algorithms; carbon dioxide; ethanol; glycosides; hybrids; maceration; neural networks; response surface methodology; sonication; statistical analysis; steviol; stevioside; sucrose; sustainable technology; ultrasonic treatment
Abstract:
... Stevia rebaudiana (Bertoni) leaves consist of dietetically important diterpene steviol glycosides (SGs): stevioside (ST) and rebaudioside-A (Reb-A). ST and Reb-A are key sweetening compounds exhibiting a sweetening potential of 100 to 300 times more intense than that of table sucrose. Ultrasound-assisted extraction (UAE) of SGs was optimized by effective process optimization techniques, such as re ...
DOI:
10.3390/foods11060883

9. A Meta-Analysis of the Effects of a Chemical Additive on the Fermentation and Aerobic Stability of Whole-Plant Maize Silage

Author:
Érica Benjamim da Silva; Limin Kung
Source:
Agriculture (Basel) 2022 v.12 no.2 pp. -
ISSN:
2077-0472
Subject:
additive effect; agriculture; ammonium nitrogen; corn silage; ethanol; fermentation; forage; lactic acid; meta-analysis; pH; potassium sorbate; sodium benzoate; sodium nitrite
Abstract:
... Our objective was to conduct a meta-analysis on the effects of a chemical additive containing sodium benzoate, potassium sorbate, and sodium nitrite on the fermentation and aerobic stability of whole-plant maize silage. We used data from 28 experiments, with 56 untreated to treated comparisons, carried out over a 9-year period. The influence of dry matter (DM) content and length of ensiling on the ...
DOI:
10.3390/agriculture12020132

10. A New Ecological RP-HPLC Method for the Determination of Pitavastatin, Fenofibrate and Their Impurities in a Novel Fixed Dose Combination

Author:
T. S. S. Jagan Mohan; Hitesh A. Jogia; Khagga Mukkanti
Source:
Chromatographia 2022 v.85 no.2 pp. 177-191
ISSN:
0009-5893
Subject:
acetic acid; analytical chemistry; environmental assessment; ethanol; fenofibrate; solvents; thermal degradation; wavelengths
Abstract:
... We developed a simple, rapid, ecological RP-HPLC method for the estimation of Pitavastatin (PIT), Fenofibrate (FEN), and their impurities in a novel fixed dose combination. We achieved an efficient chromatographic separation in gradient elution mode using Hypersil BDS C18 (100 × 4.6 mm, 3.0 μm) column. The mobile phase A consisted of 0.1% glacial acetic acid buffer and mobile phase B consisted of ...
DOI:
10.1007/s10337-021-04119-7

11. A Novel Method to Extract Juglone from Juglans mandshurica Waste Branches Using a Water-in-Oil Microemulsion

Author:
Chunying Li; Xianming Meng; Mengfei Tian; Shen Li; Yao Tian; Tingting Wang; Chunjian Zhao
Source:
Waste and biomass valorization 2022 v.13 no.3 pp. 1547-1563
ISSN:
1877-2641
Subject:
Juglans mandshurica; biomass; emulsions; ethanol; juglone; microwave treatment; pH; temperature; wastes
Abstract:
... Pruning of Juglans mandshurica produces many branches, which are potentially a rich source of juglone although they are usually discarded as waste. Herein, we describe a water-in-oil microemulsion-based microwave-assisted extraction (MBMAE) method to isolate the juglone found in waste branches from J. mandshurica. In our experiment, J. mandshurica waste branch powder was added to the MBMAE system. ...
DOI:
10.1007/s12649-021-01611-x

12. A Pt/SnO₂/rGO interface more capable of converting ethanol to CO₂ in ethanol electro-oxidation: a detailed experimental/DFT study

Author:
Peiwen Xu; Shafei Zhao; Tingting Wang; Weijie Ji; Zhaoxu Chen; Chak-Tong Au
Source:
Journal of materials chemistry A 2022 v.10 no.18 pp. 10150-10161
ISSN:
2050-7496
Subject:
carbon dioxide; durability; energy efficiency; ethanol; graphene; oxidation
Abstract:
... In this study, we developed hierarchically structured Pt/SnO₂/rGO electrocatalysts through a “layer-by-layer” synthetic strategy. Particularly, a morphologically controlled synthesis was adopted to obtain regularly shaped SnO₂ crystallites comprising the specific facets of (101), (110), (111), and (221). Then the Pt nanoparticles of ca. 3 nm were uniformly deposited onto the different facets of Sn ...
DOI:
10.1039/d2ta00178k

13. A Simple Alcohol-based Method of Oocyst Inactivation for Use in the Development of Detection Assays for Cryptosporidium

Author:
Biniam Hagos; Robert E. Molestina
Source:
Food and Waterborne Parasitology 2022 v.27 pp. e00163
ISSN:
2405-6766
Subject:
ammonia; cell lines; diarrhea; disinfection; ethanol; excystation; fluorescent antibody technique; formaldehyde; genes; heat; light microscopy; methanol; oocysts; ozone; parasites; parasitology; propidium; quantitative polymerase chain reaction; sodium hypochlorite; sporozoites; toxicity; ultraviolet radiation; viability
Abstract:
... Cryptosporidium spp. are obligate, intracellular parasites that cause life-threatening diarrhea among children and immunocompromised adults. Transmission occurs by the fecal-oral route following ingestion of thick-walled oocysts that can contaminate, persist, and resist disinfection in water and food. Sodium hypochlorite, peroxides, ozone, formaldehyde, and ammonia are suitable disinfectants again ...
DOI:
10.1016/j.fawpar.2022.e00163

14. A barcoding pipeline for mosquito surveillance in Nepal, a biodiverse dengue-endemic country

Author:
Juliane Hartke; Friederike Reuss; Isabelle Marie Kramer; Axel Magdeburg; Isra Deblauwe; Reshma Tuladhar; Ishan Gautam; Meghnath Dhimal; Ruth Müller
Source:
Parasites & vectors 2022 v.15 no.1 pp. 145
ISSN:
1756-3305
Subject:
Culicidae; DNA; barcoding; climate change; cost effectiveness; dengue; ethanol; indigenous species; monitoring; nanopores; vector-borne diseases; Nepal
Abstract:
... BACKGROUND: Vector-borne diseases are on the rise on a global scale, which is anticipated to further accelerate because of anthropogenic climate change. Resource-limited regions are especially hard hit by this increment with the currently implemented surveillance programs being inadequate for the observed expansion of potential vector species. Cost-effective methods that can be easily implemented ...
DOI:
10.1186/s13071-022-05255-1

15. A biodegradable composite filter made from electrospun zein fibers underlaid on the cellulose paper towel

Author:
Jing Hu; Zhenjun Xiong; Yuqing Liu; Jinyou Lin
Source:
International journal of biological macromolecules 2022 v.204 pp. 419-428
ISSN:
0141-8130
Subject:
air; biodegradability; cellulose; commercialization; ethanol; filtration; petroleum; pollution; polymers; prices; solvents; tissue paper; zein
Abstract:
... Conventional petroleum-based synthetic polymeric fiber filter materials for separation may cause secondary pollution to the environment due to their non-degradable properties. Herein, we report a facile method of preparation of a biodegradable composite filter that can achieve filtration for air by underlaying the commercialized cellulose paper towel under electrospun zein fibers. The morphology o ...
DOI:
10.1016/j.ijbiomac.2022.02.029

16. A branched galactoglucan with flexible chains from the basidioma of Macrolepiota albuminosa (Berk.) Pegler

Author:
Yu-Xiao Wang; Yue Xin; Xiao-Jun Huang; Jun-Yi Yin; Shao-Ping Nie
Source:
Food chemistry 2022 v.367 pp. 130738
ISSN:
0308-8146
Subject:
Macrolepiota; X-ray diffraction; aqueous solutions; basidiomata; ethanol; food chemistry; glucose; molecular weight; polysaccharides; steady flow
Abstract:
... A homogeneous galactoglucan was purified from the alkali-extracted polysaccharides from the basidioma of Macrolepiota albuminosa by gradient ethanol precipitation, whose proposed structure was given for the first time. Results showed it had a molecular weight of 210 kDa, and mainly consisted of glucose and galactose. There were abundant filaments, randomly distributed sheet-like and flaky appearan ...
DOI:
10.1016/j.foodchem.2021.130738

17. A clean in-frame knockout system for gene deletion in Acetobacterium woodii

Author:
Jonathan P. Baker; Javier Sáez-Sáez; Sheila I. Jensen; Alex T. Nielsen; Nigel P. Minton
Source:
Journal of biotechnology 2022 v.353 pp. 9-18
ISSN:
0168-1656
Subject:
Acetobacterium woodii; Clostridium acetobutylicum; Clostridium difficile; acetates; acetogens; auxotrophs; biotechnology; carbon dioxide; ethanol; fructose; gene deletion; genes; glucose; greenhouse gases; plasmids; replicon
Abstract:
... Acetogenic bacteria produce acetate following the fixation of CO₂ via the Wood-Ljungdahl pathway. As such, they represent excellent process organisms for the production of novel chemicals and fuels from this waste greenhouse gas. Acetobacterium woodii is the model acetogen and numerous studies have been conducted investigating its biochemistry, gas consumption and use as a production chassis. Howe ...
DOI:
10.1016/j.jbiotec.2022.05.013

18. A combination of deep eutectic solvent and ethanol pretreatment for synergistic delignification and enhanced enzymatic hydrolysis for biorefinary process

Author:
Lan Yao; Pingping Cui; Xiong Chen; Chang Geun Yoo; Qianting Liu; Xianzhi Meng; Long Xiong; Arthur J. Ragauskas; Haitao Yang
Source:
Bioresource technology 2022 v.350 pp. 126885
ISSN:
0960-8524
Subject:
Broussonetia papyrifera; antioxidants; biomass; cellulose; corn stover; delignification; digestibility; enzymatic hydrolysis; ethanol; glucose; lignin; solubilization; solvents
Abstract:
... A novel pretreatment system containing deep eutectic solvents and ethanol (DES-E) for synergistic carbohydrate conversion and delignification was reported in this study. The DES-E pretreatment resulted in an enhanced glucose yield compared to individual DES and ethanol pretreatment for the three tested biomass, including Broussonetia papyrifera, corn stover and pine. To further explore the deligni ...
DOI:
10.1016/j.biortech.2022.126885

19. A comparative analysis of saponin-enriched fraction from Silene vulgaris (Moench) Garcke, Sapindus mukorossi (Gaertn) and Chlorophytum borivilianum (Santapau and Fernandes): an in vitro hemolytic and cytotoxicity evaluation

Author:
Rahul Singh; Rinku Sharma; Gorakh Mal; Rajat Varshney
Source:
Animal biotechnology 2022 v.33 no.1 pp. 193-199
ISSN:
1532-2378
Subject:
Chlorophytum borivilianum; Sapindus mukorossi; Silene vulgaris; biotechnology; cell lines; cytotoxicity; ethanol; hemolysis; saponins; sheep; sulfuric acid
Abstract:
... To explore the newer saponin resources, in vitro toxicity of saponin-enriched fraction (SEF) extracted from Silene vulgaris(SV) was evaluated for first time and compared with in vitro toxicity of SEF extracted from Sapindus mukorossi (SM) and Chlorophytum borivilianum (CV). All extracted SEF from diverse resources were characterized by immersing TLC plates in 0.5% RBC suspension method, by ethanol ...
DOI:
10.1080/10495398.2020.1775627

20. A comparison of the solvent liquefaction of lignin in ethanol and 1,4-butanediol

Author:
Charles A. Mullen; Gary D. Strahan; Yaseen Elkasabi
Source:
Journal of analytical and applied pyrolysis 2022 v.164 pp. 105522
ISSN:
0165-2370
Subject:
biofuels; crosslinking; depolymerization; ethanol; ethyl acetate; feedstocks; formic acid; lignin; liquefaction; methanol; molecular weight; pyrolysis; solubility; solvents
Abstract:
... This study compares the depolymerization of soda lignin via solvent liquefaction in ethanol and 1,4-butanediol (BD). The commercial soda lignin was fractionated based on solubility in ethyl acetate and methanol providing three fractions (F1 – soluble in ethyl acetate and methanol, F2 - insoluble in ethyl acetate and soluble methanol, F3 – insoluble in either) which varied mostly based on their mol ...
Handle:
10113/7730887
DOI:
10.1016/j.jaap.2022.105522