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Highly efficient synthesis of triazolo[1,2-a]indazole-triones and novel spiro triazolo[1,2-a]indazole-tetraones under solvent-free conditions

Author:
Hasaninejad, Alireza, Zare, Abdolkarim, Shekouhy, Mohsen
Source:
Tetrahedron 2011 v.67 no.2 pp. 390-400
ISSN:
0040-4020
Subject:
chemical reactions, polyethylene glycol, synthesis, aldehydes
Abstract:
A new, convenient, and high yielding procedure for the synthesis of triazolo[1,2-a]indazole-triones by the condensation reaction between dimedone, aryl aldehydes, and ueazoles in the presence of a catalytic amount of sulfonated polyethylene glycol (PEG-SO₃H) as a highly stable and reusable eco-friendly degradable polymeric catalyst is described under solvent-free conditions. This procedure has also been applied successfully for the synthesis of novel spiro triazolo[1,2-a]indazole-tetraones.
Agid:
1093340