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Development of porous and dispersed CRM
- Röhl-Kuhn, B., Meyer, K., Klobes, P., Fritz, T.
- Fresenius' journal of analytical chemistry 1998 v.360 no.3-4 pp. 393-397
- adsorption, aluminum oxide, certification, guidelines, porous media, silica, surface area
- Porous and finely dispersed certified reference materials (CRM) were certified using the gas adsorption method. The special certification procedure for IUPAC isotherm classification types I, II, and IV is presented for meso- and macroporous materials with special emphasis on specific surface area, specific pore volume and pore width according to standards DIN 66 131, 66 134, and 66 135. Four CRMs (SiO₂, α-Al₂O₃, two transition aluminas) with a macro- and mesopore range are presented. Certification was made on the basis of BCR guidelines in connection with interlaboratory tests (altogether 38 participating laboratories, 44 various gas adsorption apparatus).