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An integrated total neutron scattering – NMR approach for the study of heterogeneous catalysis
- LeutzschThese authors contributed equally to this work., Markus, Falkowska, Marta, Hughes, Terri-Louise, Sederman, Andrew J., Gladden, Lynn F., Mantle, Michael D., Youngs, Tristan G. A., Bowron, Daniel, Manyar, Haresh, Hardacre, Christopher
- Chemical communications 2018 v.54 no.72 pp. 10191-10194
- catalytic activity, chemical compounds, chemical reactions, liquids, neutron diffraction, nuclear magnetic resonance spectroscopy
- Nuclear magnetic resonance (NMR) and total neutron scattering techniques are established methods for the characterisation of liquid phases in confined pore spaces during chemical reactions. Herein, we describe the first combined total neutron scattering – NMR setup as a probe for the catalytic heterogeneous reduction of benzene-d₆ with D₂ in 3 wt% Pt/MCM-41.