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Influence of the synthesis methods on the particle size of the LiVMoO6 phase
- Milanova, Margarita, Iordanova, Reni, Dimitriev, Yanko, Kostov, Krassimir, Vassilev, Sasho
- Journal of materials science 2007 v.42 no.10 pp. 3349-3352
- X-ray photoelectron spectroscopy, melting, oxidation, particle size, powders, spectral analysis
- The lithiated transition metal oxide LiVMoO₆ has been synthesized by a novel melt quenching method that presents some advantages as compared to the classical solid-state reaction and soft-combustion synthesis. These are: the short preparation time and the possibility to control the grain size of LiVMoO₆ powders. The local structure of LiVMoO₆ samples prepared in different ways was characterized by IR spectral analysis. The oxidation state of Li, V, and Mo was determined by X-ray photoelectron spectroscopy.